微焦X射线扫描成像技术在岩石物性特征研究的现状

微焦X射线扫描成像技术是在微米—纳米级尺度上对储层岩石物性特征的重构及透视表征,是目前国际范围内较为先进的储层定性定量研究技术。在系统文献资料研究基础上,对微焦X射线扫描成像技术的原理及研究主要内容进行归纳总结,指出该技术是为研究岩石基质及赋存于不同岩石孔隙空间之中的流体而开发建立的不断成熟起来的油气储层定性定量研究技术。可以实现岩石整体、岩石骨架和孔隙三维重构,能够以透视岩心成像的方式直观清晰地观察分析岩石内部三维孔隙空间的分布、大小及其连通性。通过阈值分割,可对孔隙三维组构、孔隙网络中流体流动、天然气水合物生成与分解等特征进行建模分析,达到四维研究的水平。分析探讨了原理及前人研究实例,对其在油气和天然气水合物实际勘探开发运用中的现状及前景做出展望。     

X射线衍射全岩录井技术在渤海油田的应用

渤海油田的勘探中深层的快速发展、PDC钻头大量使用、大位移井等新技术的应用等,造成现场岩屑细碎,依靠传统的岩性识别方法进行岩性识别越来越困难,进而影响到中深层地层界面的准确判断,不能满足目前随钻岩性识别和实时建立地质岩性剖面的要求。为了解决细碎岩屑的岩性识别以及地层界面识别的问题,渤海油田引入了X射线衍射全岩录井技术(以下简称XRD),该技术主要分析岩石中所含矿物成分以及相对含量,通过特征指示矿物含量的变化,进行岩性识别,根据不同沉积环境的矿物含量的变化趋势来进行地层划分,为现场岩性快速识别及地层界面识别提供了有力支持。     

利用单飞秒激光脉冲驱动类氖钛X射线激光的研究

提出了一种利用单飞秒激光脉冲驱动类氖钛X射线激光的物理方案.利用自相似方法研究了不同脉冲前沿的单飞秒激光辐照钛平板靶产生的类氖钛X射线激光等离子体的特性,得到了电子温度、电子密度和定标长度三者的定标律,讨论了给定输入参数下各定标律曲线的特性.研究表明,利用单个飞秒激光能够实现X射线激光的产生,而且脉冲前沿强度随时间增长平缓的飞秒激光有利于驱动X射线激光.本研究为实验上实现单飞秒激光脉冲驱动X射线激光提供了一种新的方案.     

高电荷态Ar17+离子在表面以下过程中发射X射线分支比及各分支能量的研究

对低速高电荷态Ar¹⁷⁺离子在与不同金属靶相互作用过程中放出的Ar离子K壳X射线的Kβ/Kα分支比及各分支K线平均能量进行了理论研究.在文献 的基础上,通过对实验数据的分析,得到了0.3—0.8玻尔速度之间的Ar¹⁷⁺离子与Be,Al,Ni,Mo,Au等金属相互作用过程中入射离子发出的X射线分支比及各分支平均能量.理论上,基于导带电子俘获模型和级联跃迁模型,建立耦合方程组,以解释实验主要结果,理论结果与实验符合较     

129Xeq+激发Mo表面产生的X射线谱

研究了高电荷态离子¹²⁹Xe^q+(q=25,26,27)入射金属Mo表面产生的特征X射线谱.实验结果表明,在束流强度小于120 nA条件下, 高电荷态离子¹²⁹Xe^q+可以激发Mo的L壳层特征X射线谱.单离子X射线相对产额可达10^-8量级,特征X射线的相对产额随入射离子的动能和电荷态(势能)的增加而增加.通过Mo原子的Lα相似文献   

单细胞藻吸收Cu2+,Zn2+,Se4+,Cd2+的扫描电镜X射线能谱分析

青岛大扁藻（Ｐｔａｔｙｔｈｏｎａ。ｈｅｉｇｏｈｎｄｌｃａ。ａ,ｔｓ。ｎｇｉｇｏ。ｓ;ｓＴｓｅｎｇｅｔＴ．Ｊ．Ｃｈａｎｇ）、。角褐指藻（Ｐｈａ。ｄａｅｔｙｌ。。ｔ,。。－ｎ。加。Ｂｏｈｌｉｎ）、湛ｕ叉鞭藻（一ｃ,ａ──ａ。切ｎｊ。ｎｇ。ｓ。Ｈｕ）、路氏巴夫藻＿Ｐａ。ｉｃ。ａｌ。ｔｉｅｒ（ＤｒｏｏＰ）Ｇｒｅｅｎｊ等单细胞藻类,是养殖对虾、扇贝、鲍、牡赈、河蟹等人工育苗中幼体的活饵料,它们的质量决定养殖动物幼体的成活率、生长速度以及抗病能力。所以单细胞藻类的营养成分、生活状态、密度是培育出具优良性状动…     

Generalised synchronisation of spatiotemporal chaos using feedback control method and phase compression

Coupled map lattices are taken as examples to study the synchronisation of spatiotemporal chaotic systems. First, a generalised synchronisation of two coupled map lattices is realised through selecting an appropriate feedback function and appropriate range of feedback parameter. Based on this method we use the phase compression method to extend the range of the parameter. So, we integrate the feedback control method with the phase compression method to implement the generalised synchronisation and obtain an exact range of feedback parameter. This technique is simple to implement in practice. Numerical simulations show the effectiveness and the feasibility of the proposed program.     

Experimental study on the phase transformation point of crushable and noncrushable soils

Two marine calcareous deposits as crushable soils and a siliceous sand as a noncrushable soil were used in this study to compare their monotonic response. Undrained monotonic triaxial tests were conducted on samples, which were prepared in different relative densities and consolidated under various confining pressures. The location of phase transformation point in undrained response of the sands in different initial conditions was evaluated. The effect of important parameters including relative density, confining pressure, particle shape, and particle breakage on phase transformation point was assessed. The input energy applied per unit volume of the soils was used to interpret the shearing response of crushable and noncrushable soils. The results showed that calcareous sands have more tendencies in contraction. Particle shape and breakage play a key role in engineering behavior of crushable soils.     

基于等离子体增强化学气相沉积技术的光电子器件多层抗反膜的设计和制作

针对光电子器件端面抗反镀膜的要求,研究了基于等离子体增强化学气相沉积(PECVD)技术的多层抗反膜的设计和制作.首先,对影响SiN_x折射率的因素进行了实验研究,确定了具有大折射率差的SiO₂/SiN_x材料的PECVD沉积条件.根据理论计算分析,设计了四层SiO₂/SiN_x抗反膜结构,能够在70 nm的波长范围内实现低于10^-4的反射率     

Localisation and phase transition of acoustic waves in a soft medium containing air bubbles

We study via numerical experiments the localisation property of an acoustic wave in a viscoelastic soft medium containing randomly-distributed air bubbles. The behaviours of the oscillation phases of bubbles are particularly investigated in various cases for distinguishing efficiently the acoustic localisation from the effects of acoustic absorption caused by the viscosity of medium. The numerical results reveal the phenomenon of `phase transition' characterized by an unusual collective oscillation of bubbles, which is an effective criterion to unambiguously identify the acoustic localisation in the presence of viscosity. Within the localisation region, the phenomenon of phase transition persists, and a remarkable decrease in the fluctuation of the oscillation phases of bubbles is observed. The localisation phenomenon will be impaired by the enhancement of the viscosity factors, and the extent to which the acoustic wave is localised may be determined by appropriately analyzing the values of the oscillation phases or the amount of reduction of the phase fluctuation. The results are particularly significant for the practical experiments in an attempt to observe the acoustic localisation in such a medium, which is in general subjected to the interference of the great ambiguity resulting from the effect of acoustic absorption.     

太平洋海山富钴结壳中铂族元素赋存状态与富集机理

通过选择性化学提取法,对太平洋采薇海山富钴结壳样品中铂族元素进行分级提取实验,利用电感耦合等离子体质谱仪(ICP-MS)测定了铂族元素含量。赋存状态结果显示,富钴结壳中铂族元素在各个化学相态中富集比例从大到小依次为:铁氧化物相、残渣态、锰氧化物相、碳酸盐相、吸附态,未磷酸盐化新壳层和磷酸盐化老壳层中铂族元素都主要赋存于铁氧化物相中,其富集比例为59.26%～82.19%,残渣态中磷酸盐对铂族元素具有一定的富集能力,其富集比例为17.23%～35.37%。不同类型地质体中铂族元素的赋存状态结果,也证实了富钴结壳和海山结核中铂族元素富集主要受到铁氧化物相和残渣态的影响。太平洋海山富钴结壳中铂族元素的富集机理推测为铁氧/氢氧化物胶体粒子的吸附作用,使海水中PtC l24-离子被吸附到铁氧化物相中,从而使富钴结壳中铂族元素富集。     

Dynamic characteristics of marine soft clay under variable phase difference and initial static shear stress

Abstract

Under seismic loading, the soil layer is subjected to multidirectional cyclic shear stress with different amplitudes and frequencies because of the coupling of multiple shear waves and the soil element within a slope or behind a retaining wall is subjected to initial static shear stress before subjected to cyclic loading. Due to the complexity of seismic loading propagation, a phase difference exists between the initial static shear stress and cyclic shear stress. To investigate the influence of the phase difference and initial static shear stress on cyclic shear strain, cyclic modulus, and cyclic strength, a series of laboratory tests are performed on Wenzhou marine soft clay by multi-directional simple shear system, which can simulate the actual state better by controlling the horizontal cyclic stress in the x and y directions simultaneously. As the phase difference varies from 0° to 90°, the dynamic shear modulus increases and cyclic strain accumulation decreases with an increasing number of cycles. The shear strain increases with the initial shear stress.     

南海沉积物沉积有机态Fe与Fe限制的分析

Fe限制的研究对于探讨全球CO2变化及解决"温室效应"具有重要的意义.南海兼具开阔大洋和边缘海的特征,其古生产力的演变对区域及全球气候变化的研究具有重要作用.本文采用连续提取法对两个南海柱样沉积物中的Fe,Ba,Al等主要金属元素进行了形态分析,并将两个站位沉积物中沉积有机态Fe与Al/Ti比值、TOC、生源Ba等古生...     

南沙地块OBS2019-2测线数据处理与震相识别

为揭示南海南部陆缘的地壳结构,研究其张裂-破裂机制,开展共轭陆缘对比,我们在南沙地块礼乐西海槽附近的洋陆转换带上完成了OBS2019-2测线的探测工作。相较于北部陆缘,南部陆缘已有的海底地震仪(ocean bottom seismometer,OBS)测线较少,对深部地壳结构的研究也较少,因此OBS2019-2测线就尤为重要。文章重点阐述了OBS2019-2测线的数据处理工作,包括UKOOA文件制作、数据格式转换、位置校正、单个台站综合地震记录剖面的生成等,然后在剖面图中对各类深部震相(Pg、PcP、PmP、Pn)进行识别追踪,并建立初步的模型;使用Rayinvr软件进行走时试算工作,验证了震相识别的准确性。处理结果显示OBS2019-2测线的深部震相清晰,最远震相可以连续追踪到120km以外,数据整体质量良好,能为后续速度建模和构造解释等工作提供坚实基础。     

Quantifying the reefscape transformation of a coastal Caribbean coral reef during a phase shift and the associated coastal landscape change

Caribbean coral reefs are under strong natural and human pressures and many have undergone phase shifts as a result of local and global change. However few studies have quantified the extent of these phase shifts and the potential impacts that they have on coral reef communities. A temporal comparative analysis of several coral reefscape and landscape metrics was conducted for data from Mahahual, Quintana Roo, Mexico, between the years 2000 and 2006, when a phase shift occurred. Landscape metrics were calculated from coral reef and coastal cover maps obtained by multispectral satellite image classification using IKONOS satellite imagery. These metrics showed that the coastal landscape and reefscape of Mahahual lost 85 ha of vegetation cover and 43 ha of coral cover over 6 years, respectively. Coastal landscape transformation was induced by the construction of a cruise ship pier and multiple associated tourist developments along the coast, such as hotels and restaurants, meanwhile alteration of the reefscape may be associated with potential stressors such as coastal development, bleaching events and hurricanes.     

基于三维相空间法和稳健估算法的ADV流速数据后置处理效果研究

水流是影响藤壶、牡蛎、藻类等水生生物能否成功附着在渔业装备上的重要环境因素,水体流速的变化会改变藻类新陈代谢过程,制约藤壶与牡蛎幼虫大面积扩散。流速测量数据的准确性对研究渔业装备上附着生物的附着机制起到至关重要的作用。声学多普勒流速仪(ADV)是测量水体流速的重要设备。然而,水体中的气泡、大颗粒悬浮物等因素会影响ADV的相关系数和信噪比,从而导致流速数据中产生野点,降低了数据的准确性。本文基于国内外主流算法稳健估算法与三维相空间法,以ADV实际测量的流速数据为例,对比研究两种后置处理方法的检测效果。结果显示,稳健估算法平均检出率为4.95%,峰度系数平均下降77.71%,三维相空间法平均检出率为14.60%,峰度系数平均下降84.05%。综合分析,三维相空间法处理效果较好,其检测准确性高于稳健估算法,但存在过处理现象。建议在处理野点含量低于5%的数据时选用相空间法,而对于野点偏离样本平均值较远的数据时,可以选用稳健估算法。本文对减小流速数据误差,为准确定量研究水流对渔业装备附着生物的附着量与种类影响有着重要的意义。