Optically stimulated luminescence dating of a Holocene beach ridge plain in Northern Jutland, Denmark

This study presents results from 20 optically stimulated luminescence (OSL) ages from one of the world's largest beach ridge plains, the Jerup beach ridge plain at the base of the Skagen Spit in the northernmost part of Jutland, Denmark. The OSL ages were obtained using quartz and a SAR protocol, and used to establish a chronology for the beach ridge plain and for the underlying coastal plain. The accuracy of the chronology is tested both by laboratory tests (recuperation, recycling ratio and dose recovery) and by comparison with independent age controls, e.g. previously reported radiocarbon dates, map sources, anecdotal evidence and settlement names. It is concluded that the OSL signals are internally consistent, and that the derived OSL ages are in good agreement with a large range of independent age controls. The ridge plain is shown to cover a time span from 1000 to 2700 years ago; this chronology is more detailed and precise than those previously available, and gives an average beach ridge formation rate of 15 yr/ridge and an average lateral migration rate of 2.0 m/yr. This study adds to the growing knowledge that OSL dating has a large potential for establishing detailed and precise chronologies in coastal marine sediments, including beach ridges.     

Quartz OSL dating of late Holocene beach ridges from the Magdalen Islands (Quebec,Canada)

Quartz optically stimulated luminescence (OSL) dating has been applied to sandy beach ridge systems from the Magdalen Islands in the center of the Gulf of St. Lawrence (Quebec, Canada) to provide the first chronological framework for these features. Nineteen beach ridges (22 samples) from four different sites throughout the archipelago were investigated. At one of the sites, samples were taken at 9 m and 7.5 m depth using a vibracore. The quartz is dominated by the fast OSL component and a single-aliquot regenerative-dose (SAR) protocol was used to measure the equivalent doses; a low preheat (180°C/10 s) was chosen to avoid the influence of thermal transfer. The average dose recovery ratio of all samples is 1.02 ± 0.02 (n = 130) suggesting that the SAR protocol works satisfactorily on this material. The OSL ages are internally consistent and supported by independent age control (radiocarbon). The OSL ages indicate that the ridges were built between 2.6 ± 0.2 ka and 0.40 ± 0.10 ka, i.e. during a period of sea level rise. This rise eroded adjacent sandstone cliffs, which contributed a significant sediment supply to the littoral drift and beaches. Some low-lying coasts in the archipelago are still prograding, despite a relative sea level increase of ∼1.6 mm/a over the last 600 years. The late Holocene ages obtained in this study indicate that these processes have been active for at least the past two thousand years. This study demonstrates for the first time that OSL dating using quartz has great potential in this area, and is an appropriate method for establishing precise chronologies for coastal sediments in this region of the Gulf of St. Lawrence.     

Characteristics of the burial environment related to quartz SAR-OSL dating at St. Vincent Island, NW Florida, USA

St. Vincent Island, on the northwest Gulf coast of Florida, USA, preserves a well-developed beach ridge plain that began to form 4000 years ago based on inferred ages of pottery artefact assemblages. Seven vibra cores up to 2.88 m in length (uncompacted sediment) were retrieved from six ridges across the island. The single-aliquot regenerative-dose (SAR) procedure was used to obtain two optically stimulated luminescence (OSL) ages per core at different depths within each core.

The geographically youngest ridges gave ages of 370±50–1900±300 years, yielding an inter-ridge accumulation time of 150 years assuming uniform sediment accumulation. The oldest ridge sets yielded ages of 2700±400–2800±300 years. Dating results are evaluated in terms of equivalent dose (D_E) distributions and other characteristics in relation to aspects of the burial environment, including pedogenesis.     

Analysis of water quality and circulation of four recreational Miami beaches through the use of Lagrangian Coherent Structures

Four popular, recreational beaches in Miami, FL are Hobie Beach, Virginia Key Beach, Crandon Park Beach, and Bill Baggs Cape Florida State Park. While all of the beaches are within a few miles of each other in Biscayne Bay, they have greatly differing water qualities, as determined by the testing for fecal indicator bacteria performed by the Florida Department of Health. Using the geodesic theory of transport barriers, we identify Lagrangian Coherent Structures (LCSs) in each area. We show how these material curves, which shape circulation and mixing patterns, can be used to explain the incongruous states of the water at beaches that should be comparable. The LCSs are computed using a hydrodynamic model and verified through field experimentation at each beach.     

Numerical analysis of coastal cliff failure along the Pembrokeshire Coast National Park,Wales, UK

Cliff stability within the Pembrokeshire Coast National Park was evaluated using a numerical model applied at four sites representative of rock mass failure phenomena and major sedimentary geological sequences. The sites were: Mill Bay, (Old Red Sandstone); St Govan's Head, Carboniferous Limestone (Dinantian); Druidston, Millstone Grit (Namurian) and Lower Coal Measures (Westphalian); and Wiseman's Bridge, Lower Coal Measures (Westphalian). The study integrated a range of geotechnical parameters, measured in the field and laboratory, into a model to predict the likely failure mechanisms. The model is based on the existence of rock prisms delineated by structural parameters, i.e. joints, bedding planes and critical tension fractures behind the cliff face. An iterative approach is used to define the dip of the most probable, stepped failure surface at the base of any potentially unstable multiblock system and to calculate the sliding and toppling forces for each block in the cliff mass. Prediction compared favourably with field observations at three of the four selected sites, i.e. Druidston, St Govan's Head and Wiseman's Bridge. At Druidston sliding is predicted and dominates in the basal blocks, whilst toppling is confined to the upper cliff and is dependent on movement of the lower structural units. St Govan-s Head is shown to have a low risk of toppling and sliding and this was predicted except where basal undercutting reaches a depth of 1·0 m or lateral forces exceed 100 kN m⁻² when failure could occur. Copyright © 1998 John Wiley & Sons, Ltd.     

An OSL, radiocarbon and tephra isochron-based chronology for Birdlings Flat loess at Ahuriri Quarry, Banks Peninsula, Canterbury, New Zealand

OSL, radiocarbon dating of pedogenic carbonate and tephrochronology have been used in an attempt to provide a detailed and reliable chronology for Birdlings Flat loess, a thick, proximal loess found on the lower flanks of Banks Peninsula, Canterbury, New Zealand. In a ca 15 m thick section at Ahuriri Quarry the Kawakawa tephra isochron of 26,500 cal. yr BP is identified at a depth of ca. 1.35 m on the basis of glass counting and electron microprobe fingerprinting. Radiocarbon ages of filamentous or root pseudomorph carbonate increase down section from ca. 10,000 cal. yr BP at 2.80 m to ca. 30,000 ¹⁴C yr BP at 10.90 m. Ages from carbonate lining cracks are often out of sequence, indicating deep percolation by bypass flow down preferential flow paths. OSL ages show reversals with respect to each other, carbonate radiocarbon ages, and with the position and accepted age of Kawakawa tephra. Coincident radiocarbon and OSL ages at 3.85 m depth indicate that OSL ages are underestimates by at least 20%. Before OSL can be deemed a high accuracy dating method of the quatzo-feldspathic loess of South Island, New Zealand, more research into the causes of age underestimation and age reversals must be carried out. The last major episode of loess accumulation on the flanks of Banks Peninsula in Canterbury began before ca. 30,000 ¹⁴C yr BP (ca. 35,000 cal. yr BP) and possibly before 43,000 yr based on OSL.     

OSL dating of the AD 869 Jogan tsunami deposit,northeastern Japan

Sediments deposited by the AD 869 Jogan tsunami offer an opportunity to test the reliability of optically stimulated luminescence (OSL) dating of relatively old historical tsunami deposits. We collected a geoslicer sample from sand deposited on the Sendai Plain, northeastern Japan, by the Jogan tsunami and applied quartz OSL dating to it. We then compared the OSL ages with the known age of the tsunami event. In ascending order, the sedimentary sequence in the geoslicer sample consists of the beach–dune sand, lower peat, Jogan tsunami deposit, upper peat, pre-2011 paddy soil, and the 2011 tsunami deposit. To obtain equivalent dose (D_e,bulk), a standard single-aliquot renegerative-dose (SAR) protocol was applied to large aliquots of the 180–250 μm fraction of two samples from the beach–dune sand, and four samples from differing levels of the Jogan tsunami deposit. The OSL decay curves were dominated by the medium component; thus, for two samples from the Jogan deposit the fast-component OSL signal was isolated and used to determine the equivalent dose (D_e,fast). Using D_e,bulk, OSL ages of the tsunami deposit were underestimated by ∼40%, and even the beach–dune sand was dated younger than AD 869. In contrast, D_e,fast provided a robust age estimate with only slight underestimation. A pulse annealing test showed that the bulk and medium-component OSL signals were thermally unstable. The medium component in the natural OSL was clearly truncated in comparison to the regenerated OSL; the medium component is thus considered to be the main cause of the underestimated ages. Similar effects of a dominant medium-component OSL have been reported in tectonically active regions, which are also prone to tsunamis. The effect of this dominance should be carefully considered in quartz OSL dating of tsunami deposits.     

Influence of topography on wind speed over a coastal dune and blowout system at Jockey's Ridge,NC, USA

This study examines the spatial distribution of wind speed across a coastal dune system located at Jockey's Ridge State Park, North Carolina. The study area consists of a trough blowout through a foredune ridge, and the landforms that have developed behind the foredune. Wind speed and direction were measured simultaneously with single sensors placed at a fixed height in 13 locations across the blowout/dune complex. Fractional wind speed‐up is computed for sampling stations using data from a mast located on the beach as the reference. Results show that wind speeds were generally accelerated across the study site. The highest speeds were recorded on the foredune ridges adjacent to the blowout. Wind was accelerated through the center of the blowout throat and along the downwind lateral wall. Further into the blowout, at the base of the ramp to the depositional lobe, higher wind speeds shifted to the upwind lateral wall and continued to accelerate up the ramp as air exited to the rear. Significant variations in the wind speed‐up pattern were associated with different wind approach angles, with greater speed‐up occurring when the winds were aligned normal to the dune system. The speed‐up decreased as the angle of approach became increasingly oblique to the ridge. The patterns of wind speed‐up across the site point to the influence of topography on airflow. To quantify the relationship, measures of several topographic variables were obtained along sample transects running upwind from each sample station along flow lines representing different wind approach angles. Examination of correlation coefficients between wind speed‐up and topographic variables suggests that for groups of stations with similar topographic characteristics, 30–50% of the variations in speed‐up may be explained by the upwind topographic variability. Copyright © 2014 John Wiley & Sons, Ltd.     

Tsunami generation by pyroclastic flow during the 3500-year B.P. caldera-forming eruption of Aniakchak Volcano, Alaska

 A discontinuous pumiceous sand, a few centimeters to tens of centimeters thick, is located up to 15 m above mean high tide within Holocene peat along the northern Bristol Bay coastline of Alaska. The bed consists of fine-to-coarse, poorly to moderately well-sorted, pumice-bearing sand near the top of a 2-m-thick peat sequence. The sand bed contains rip-up clasts of peat and tephra and is unique in the peat sequence. Major element compositions of juvenile glass from the deposit and radiocarbon dating of enclosing peat support correlation of the pumiceous sand with the caldera-forming eruption of Aniakchak Volcano. The distribution of the sand and its sedimentary characteristics are consistent with emplacement by tsunami. The pumiceous sand most likely represents redeposition by tsunami of climactic fallout tephra and beach sand during the approximately 3.5 ka Aniakchak caldera-forming eruption on the Alaska Peninsula. We propose that a tsunami was generated by the sudden entrance of a rapidly moving, voluminous pyroclastic flow from Aniakchak into Bristol Bay. A seismic trigger for the tsunami is unlikely, because tectonic structures suitable for tsunami generation are present only south of the Alaska Peninsula. The pumiceous sand in coastal peat of northern Bristol Bay is the first documented geologic evidence of a tsunami initiated by a volcanic eruption in Alaska. Received: 3 December 1997 / Accepted: 11 April 1998     

Storm response of a mixed sand gravel beach ridge plain under falling relative sea levels: A stratigraphic investigation using ground penetrating radar

Beach ridge stratigraphy can provide an important record of both sustained coastal progradation and responses to events such as extreme storms, as well as evidence of earthquake induced sediment pulses. This study is a stratigraphic investigation of the late Holocene mixed sand gravel (MSG) beach ridge plain on the Canterbury coast, New Zealand. The subsurface was imaged along a 370 m shore-normal transect using 100 and 200 MHz ground penetrating radar (GPR) antennae, and cored to sample sediment textures. Results show that, seaward of a back-barrier lagoon, the Pegasus Bay beach ridge plain prograded almost uniformly, under conditions of relatively stable sea level. Nearshore sediment supply appears to have created a sustained sediment surplus, perhaps as a result of post-seismic sediment pulses, resulting in a flat, morphologically featureless beach ridge plain. Evidence of a high magnitude storm provides an exception, with an estimated event return period in excess of 100 years. Evidence from the GPR sequence combined with modern process observations from MSG beaches indicates that a palaeo-storm initially created a washover fan into the back-barrier lagoon, with a large amount of sediment simultaneously moved off the beach face into the nearshore. This erosion event resulted in a topographic depression still evident today. In the subsequent recovery period, sediment was reworked by swash onto the beach as a sequence of berm deposit laminations, creating an elevated beach ridge that also has a modern-day topographic signature. As sediment supply returned to normal, and under conditions of falling sea level, a beach ridge progradation sequence accumulated seaward of the storm feature out to the modern-day beach as a large flat, uniform progradation plain. This study highlights the importance of extreme storm events and earthquake pulses on MSG coastlines in triggering high volume beach ridge formation during the subsequent recovery period. © 2019 John Wiley & Sons, Ltd.     

OSL and IRSL dating of raised beach sand deposits along the southeastern coast of Norway

Raised beach sand deposits along the southeastern coast of Norway were dated by optical (OSL) and infrared stimulated luminescence (IRSL) and the quartz and K-feldspar luminescence characteristics were described. Due to the poor quartz luminescence characteristics, only a limited number of samples were suitable for OSL dating. More promising are the K-feldspar extracts, with typical K-feldspar luminescence characteristics and no sign of fading. For equivalent dose (D_e) determination, sand-size quartz and feldspar extracts were used, applying a single aliquot regenerative (SAR) protocol. Both, OSL and IRSL D_e estimates show a wide distribution, unexpected for beach deposits. The calculated OSL and IRSL age estimates were generally in good agreement and the correctness of the ages was confirmed by independent age control. Because only a limited number of the quartz samples were suitable for OSL dating, IRSL dating of the K-feldspar represents an alternative to OSL quartz dating.     

Constraining the age of rock art by dating a rockfall event using sediment and rock-surface luminescence dating techniques

Optically stimulated luminescence (OSL) is used to determine the age of a rockfall event that removed part of the pictograph figures at the Great Gallery rock art panel in Canyonlands National Park, Utah, USA. Analyses from the outer millimeter of the buried surface of a rockfall boulder and quartz grains from the underlying sediment both provide consistent ages that also agree with an AMS radiocarbon age of a cottonwood leaf found immediately between the clast and underlying sediment. Measurement of the OSL signals as a function of depth into the surface of the boulder clearly shows that there is no detectable increase in the OSL signal to a depth of at least 3 mm suggesting that the OSL signal was fully reset to this depth before burial. Consistent OSL and radiocarbon ages for this rockfall event provide a minimum age of ∼900 a for the Great Gallery, which is the type locality of Barrier Canyon Style rock art with a controversial and unknown origin.     

Developments in optically stimulated luminescence age control for geoarchaeological sediments and hearths in western New South Wales,Australia

Research conducted by the Western New South Wales Archaeology Program (WNSWAP) provides the opportunity to assess the reliability of optically stimulated luminescence (OSL) dating of late Pleistocene and Holocene fluvial sediments and burnt stone samples from arid zone geoarchaeological contexts. A large number of radiocarbon age determinations of charcoal preserved in heat retainer hearths provides independent chronological control at these contexts. We describe a rapid OSL methodology for dating burnt hearth stones to complement previously applied radiocarbon methods, which we have tested using 37 samples from hearths with radiocarbon determinations. We propose a geoarchaeological model in which these hearths were constructed by people whose activity took place on an archaeological surface, formed by the earlier deposition of fluvial sediments. Here we demonstrate the veracity of this model by dating sediments lying stratigraphically below the hearths, and use the radiocarbon age control and chronological consistency to assess the accuracy and reliability of both small aliquot and single grain single aliquot regenerative-dose (SAR) OSL dating. While small aliquot age estimates are in most cases in agreement with independent control, the single grain determinations using a finite mixture model (FMM) appear to provide improved chronological resolution. Using single grains, we note some problems in the application of the FMM and in the dating of young samples in the range of 1–100 years. As many samples may have resided close to the surface since deposition, we have developed a mathematical function to describe gamma and cosmic dose rate contributions at burial depths down to 40 cm. These OSL age estimates allow us to reject the model of intensification of human activity as responsible for the observed pattern of archaeological radiocarbon determinations in this part of the Australian arid zone.     

OSL dating of individual quartz ‘supergrains’ from the Ancient Middle Palaeolithic site of Cuesta de la Bajada,Spain

Dose saturation represents a fundamental limitation for obtaining finite optically stimulated luminescence (OSL) quartz ages over Middle Pleistocene timescales. Single-grain OSL studies typically reveal significant intra- and inter-sample variability in quartz dose saturation properties at the individual grain level. This enhanced variability may offer the potential to obtain extended-range chronologies exceeding the traditional upper age limits of multiple-grain OSL dating. However, there have been relatively few detailed assessments of single-grain OSL properties over high dose ranges. In this study we investigate extended-range single-grain OSL dating potential at Cuesta de la Bajada, one of the most important Ancient Middle Palaeolithic sites in the Iberian Peninsula. The quartz samples from this site exhibit exceptional dose saturation properties and contain significant populations of individual ‘supergrains’ with bright OSL signals, very high characteristic saturation dose (D₀) limits of 200 to >600 Gy, and dose-response curves that closely conform to single saturating exponential functions. Assessments of OSL signal composition and the ability to successfully recover a known laboratory dose of 470 Gy support the potential for obtaining high equivalent dose (D_e) values with reasonable fitting uncertainties. A series of novel sensitivity tests are used to assess potential biases in supergrain D_e estimation over high dose ranges related to (i) thermally transferred signal contributions, (ii) choice of dose-response curve fitting function, and (iii) insufficient dose saturation properties of individual grains. The single-grain D_e values obtained using the standard quality assurance criteria and novel sensitivity tests are consistent at 2σ, and are in agreement with quartz Ti-centre ages obtained on two of three paired electron spin resonance (ESR) samples collected from Cuesta de la Bajada. These comparisons support the suitability of our single-grain OSL results and suggest there may be good potential for using quartz supergrains to establish extended-range chronologies at some Middle Pleistocene sites. Comparisons with other single-grain OSL studies across the Iberian central plains suggest that favourable dose saturation properties may be influenced by regional-scale geological controls. The importance of undertaking single-grain OSL dating at Cuesta de la Bajada is also demonstrated by the results of synthetic aliquot experiments, which reveal multiple-grain age offsets of 60–170 ka when unsuitable grain types are inadvertently included in the final age calculations. The single-grain OSL results indicate that the main archaeological horizon at Cuesta de la Bajada (unit CB3) accumulated between 264 ± 22 and 293 ± 24 ka. These ages are consistent with the chronologies of other key early Middle Palaeolithic sites in the region (Ambrona AS6 and Gran Dolina TD10) and indicate that the Ancient Middle Palaeolithic techno-complex likely spread across Iberia from at least Marine Isotope Stage 9 onwards.     

Mercury concentrations in red drum, Sciaenops ocellatus, from estuarine and offshore waters of Florida

Dorsal muscle tissue from 712 red drum, Sciaenops ocellatus, from Florida waters were analyzed for total mercury content. Mercury levels detected in these red drum varied but in most study areas were usually lower than regulatory threshold guidelines. Total mercury levels in individual fish from all study areas ranged from 0.020 to 3.6 ppm (wet weight). Total mercury levels detected in red drum from the Florida Keys-Florida Bay area were often higher than those in fish from all other estuarine study areas. Positive relationships between total mercury levels and fish size (length and weight) and fish age were observed in most Florida study areas, indicating that mercury levels tend to increase over time as red drum grow. The majority of large, mature red drum examined contained mercury levels greater than the 0.5-ppm threshold level set by the Florida Department of Health (DOH). Approximately 94% of all adult red drum from offshore waters adjacent to Tampa Bay contained mercury levels greater than or equal to the 0.5-ppm threshold level, and 64% contained levels greater than or equal to the DOH 1.5-ppm "no consumption" level. All fish from this area with mercury levels greater than 1.5 ppm were large individuals (670 mm SL). Eight percent of legal-size red drum from Florida waters contained total mercury levels greater than or equal to the 0.5-ppm threshold level. The majority (52%) of these legal-size fish greater than or equal to 0.5 ppm were from the Florida Keys-Florida Bay area. In the Florida recreational fishery, the current maximum size limit for this species is an effective filter that prevents humans from consuming those red drum with the greatest likelihood of containing high mercury levels.     

Detecting post-depositional sediment disturbance in sandy deposits using optical luminescence

Post-depositional mixing or exhumation is common in surficial sediments, yet may be unobservable from field evidence. However, any disturbance may have significant consquences in terms of establishing a reliable luminescence age determination. Optically stimulated luminescence (OSL) measurements, particularly measurements at the single grain level, can be used to gain an insight into both contemporary and past post-depositional processes.

This paper examines sites from Texas and Florida (USA) with independent chronological control to demonstrate the potential effects of varying degrees of bioturbation on OSL. Results show that contemporary soil forming processes clearly impact on the palaeodose (D_e) replicate distributions which are measured in order to derive an OSL age. Significant levels of scatter and apparently zero dose grains are observed in the upper-most sediments; declining with depth from the surface. D_e replicates from undisturbed and fully bleached sediments are unskewed, show low overdispersion (OD) and comparable single grain and single aliquot OSL ages. Bioturbated sediments, however, may show highly skewed multi-model D_e distributions with higher OD values, zero dose grains at depth, and significant diffences between single grain and single aliquot results. True burial ages may be derived from minimally bioturbated sediments through the application of statistical analysis such as finite mixture modelling to isolate D_e components. However, for significantly bioturbated sediments, the latter approach, even at the single grain level, produces inaccurate ages. In such cases we argue that additional evidence (both dating and contexual) may be required to identify with confidence the burial D_e population.     

Spatial and seasonal aspects of beach stability

Recent work at three contrasting sites in England and Wales has shown characteristics atypical of those frequently reported elsewhere. These differences are:

• (a) Taking each entire beach system there is no uniform trend of erosion or accretion, nor a progressive variation in beach elevation or volume alongshore, from one survey to the next. However, for Swansea Bay the ‘long-term’ (i. e. 18 months) range in profile height along that stretch of coast where the alignment of the beach is normal to the direction of wave approach, correlates well with computed wave energy derived from relevant offshore wave directions.
• (b) While beach variability is greatest during the ‘winter’ (i. e. storm) period there is no overall tendency for a drawdown of sediment from the intertidal zone at that time. Response times are relatively short. Thus high beach levels need not necessarily be associated with ‘summer’ conditions.
• (c) Although in Swansea Bay there is a tendency for the beach height to fluctuate least at mid-tide level this is not true of the other two sites. In no area does sediment eroded from the upper exposed part of the beach regularly appear to be deposited on the lower exposed part, or vice versa.

     

Multi-residues of organic pollutants in surface sediments from littoral areas of the Yellow Sea, China

Concentrations of all studied organic pollutants, except for DDTs, were greatest at sites in Dalian Bay, where surface sediment concentrations of PHCs, PAHs, PCBs and DDTs exceeded the corresponding ERL values. The sum concentration of DDTs was greatest in Haizhou Bay exceeding the related ERM value. In terms of compositions of PAHs and PAEs, the predominant components were the MMW and HMW compounds, DBP and DEHP, respectively. The main degradation product of p,p'-DDT was p,p'-DDD at most sampling sites. The principal sources of PAHs and DDTs involved various pyrolytic processes (i.e., combustion of biomass and vehicle exhaust), and application of technical DDT (in the form of impurity or raw material), and a mixture of technical DDT and technical dicofol. Moreover, the coastal site with greatest potential ecological risk from total PAHs was located in Dalian Bay, while the littoral areas of Dalian Bay, two harbor cities (Yantai-Weihai), Jiaozhou Bay, and Haizhou Bay, had relatively high potential risk from DDTs, especially in Haizhou Bay.     

Optical dating of hydromagmatic volcanoes on the southwestern coast of Jeju Island, Korea

Jeju Island, the largest Quaternary volcanic island in Korea, has formed mostly since the early Pleistocene, but its latest chronology of volcanism and sedimentation is still poorly constrained. Here we report optically stimulated luminescence (OSL) ages for two hydromagmatic volcanoes on the southwestern coast of Jeju Island, i.e., the Songaksan and Suwolbong tuff rings. The basaltic tuffs of these volcanoes contain abundant quartz sands from underlying marine sedimentary sequences. Two samples collected from the middle part of the Songaksan Tuff yielded highly reproducible quartz single-aliquot regenerative-dose (SAR) OSL ages of 7.0±0.3 ka, providing the first direct age estimate of Holocene volcanism in Jeju Island. The quartz OSL age estimate of 5.1±0.3 ka for the younger reworked basaltic tuff (the Hamori Formation) is comparable with previous radiocarbon and U-series disequilibrium dating of fossil mollusk shells. Two samples from the Suwolbong Tuff show quartz OSL age estimates of 18.3±0.7 and 18.6±0.9 ka, which are identical within error ranges and younger than the quartz OSL age estimate of 23.2±1.0 ka for the underlying Gosan Formation. This study confirms that volcanism and attendant sedimentation were active in Jeju Island until very recently.     

Optical dating of perennially frozen deposits associated with preserved ancient plant and animal DNA in north-central Siberia

We present chronological constraints on a suite of permanently frozen fluvial deposits which contain ancient DNA (aDNA) from the Taimyr Peninsula of north-central Siberia. The luminescence phenomenology of these samples is first discussed, focusing on the optically stimulated luminescence (OSL) decay curve characteristics, thermoluminescence (TL) properties, and signal compositions of quartz from these previously unstudied deposits. Secondly, we assess the suitability of these samples for OSL dating and present the OSL chronologies obtained using both single-grain and multi-grain equivalent dose (D_e) measurements. The results of our analyses reveal a large amount of inter-aliquot variability in OSL decay curve shape that is directly related to differences in the size of the 280 °C TL peak and the associated slowly bleached ‘S2’ OSL component. Longer OSL stimulation durations are adopted in the D_e measurement procedure to prevent the progressive build-up of slowly bleached signal components throughout successive single-aliquot regenerative-dose (SAR) measurement cycles. The use of low preheat temperatures in the SAR procedure also reduces the deleterious effects of these slowly bleached signal components. The resultant single-grain and multi-grain OSL chronologies obtained using this approach are stratigraphically consistent and are in close agreement with independently established ¹⁴C ages at our sites. The findings of this research reveal the potential of OSL dating as a means of providing a reliable chronometric framework for sedimentary aDNA records in permafrost environments.