花岗闪长岩和大理岩Kaiser效应研究之比较

通过比较花岗闪长岩和大理岩在低载阶段声发射信号特点以及Ｋａｉｓｅｒ效应记忆先前应力、应变的能力,证明了Ｋａｉｓｅｒ效应的机理在于对先前损伤的记忆。     

岩石单轴压缩试验Kaiser效应实质的研究

岩石 Kaiser效应具有记忆先前应力、纵向应变和横向应变的能力 ,记忆的准确程度随加载阶段不同而不同。为了解 Kaiser效应的记忆实质 ,通过岩石单轴压缩试验确定 Kaiser效应对体积应变、弹性模量和泊松比三项物性参数的记忆能力。结果表明 ,岩石 Kaiser效应具有记忆先前物性参数的能力 ,其中尤以对弹性模量的记忆能力表现为最好 ,而且受时间因素影响不大 ,说明岩石 Kaiser效应的实质是对其内部物理特性的记忆     

以声发射估计岩石试样先存应力的新方法

利用声发射话动的凯塞（Kaiser）效应测定岩石先存最大应力已成为声发射技术的重要应用领域。目前,判断岩石凯塞效应对应应力的方法仍被重视。作者在研究岩石在单轴压缩条件下的声发射话动时发现:除了通过凯塞效应可测定岩石的先存最大应力之外,还可根据重复加载时声发射话动的某些特点推断出加载前的先存最大应力,从而进一步验证和提高了利用凯塞效应测定先存最大应力的可靠性。重复加载时声发射话动在一定技术条件下会出现这样的特点:在应力达到第一次加载的最大应力值时出现凯塞效应;而在此之前,当应力达到加载前岩石的先存最大应力值时,声发射话动相对其前后有所特殊。作者认为,这种现象可能反映了材料对先前经历过的损伤的记忆能力。本文初步探讨了这一现象的物理基础。     

时间延迟对劈裂试验条件下岩石凯塞效应的影响

验证了粗晶花岗岩在劈裂试验条件下凯塞效应的存在性。进行了循环加卸载时间间隔分别为2、15d和45d时岩石的声发射试验,讨论了时间延迟对花岗岩凯塞效应的影响。研究结果表明,前期荷载越接近极限强度,岩石的凯塞效应越不明显;凯塞效应随再次加载时间延迟的增加而削弱,在对花岗岩的声发射试验中观察到15d以后岩石的凯塞效应仍然很显著,45d后凯塞效应基本消失。文中同时对试件与加载设备之间的接触状态对声发射试验结果的影响作了初步的定性分析。     

基于大直径霍普金森压杆数值试验的非均匀介质动态破坏过程分析

基于细观损伤力学基础而开发的动态岩石破裂过程分析系统RFPA2D代替大直径SHPB试验技术对非均匀介质的动态破坏过程和动态性能进行数值模拟,分析了加载波形和介质的非均匀性对数值试样的动态性能,如应力-时间曲线、应变-时间曲线、应力-应变曲线和应变率-时间曲线的影响。分析表明,大直径SHPB弥散效应对试验结果的影响较大,选择合适的加载波形可以减小SHPB装置中应力波的弥散效应,得到较准确的试验结果,其中三角形波加载可以有效降低大直径SHPB动态测试中的应力波弥散,是岩石等非均匀材料SHPB动态测试的较理想加载波形;在相同加载条件下,岩石的非均匀性对波的弥散效应影响不大,但非均匀岩石的试验曲线比均匀岩石的曲线在波峰后都出现较大的振荡,这主要是由于不同均质度的岩石其单元具有不同的破坏分布造成的,不是波形弥散造成的。     

三轴疲劳-卸围压条件下大理岩力学特性试验研究

为了揭示应力扰动和卸载围压作用下大理岩损伤破裂的物理过程和非线性力学行为,采用GCTS RTR-2000伺服加载岩石力学试验机进行了岩石疲劳卸围压试验,同时对破坏试样进行了压后裂纹形态CT扫描可视化分析。结果表明：周期性的加卸载作用对大理岩起到了主因损伤作用,卸围压的作用对大理岩起到了根本性的破坏作用。岩石疲劳循环形成滞回环,滞回环面积由疏变密,滞回环加载和卸载曲线接近重合,加卸载模量近似相等;岩石经过卸围压作用,岩石的轴向、径向和体积应变表现为不同程度增大,表明应变对围压降低具有强敏感性,敏感程度由高到低依次为体积应变、径向应变和轴向应变;由于疲劳循环的影响,卸围压作用产生的围压降幅随循环次数增多而降低,卸围压时长随循环次数增多而减少;量化宏观应变变形,求得应变损伤指数 、 、 ,疲劳循环次数越多,应变损伤指数越大;岩石破坏后细观CT扫描揭示了疲劳循环损伤对岩石破裂形态影响的内在机制。随疲劳循环次数的增加,裂纹密度和规模显著增加。研究成果可为地下工程疲劳活动规律和开挖卸荷问题提供理论和模型支撑。     

三轴疲劳-卸围压条件下大理岩力学特性试验研究

为了揭示应力扰动和卸载围压作用下大理岩损伤破裂的物理过程和非线性力学行为,采用GCTS RTR-2000伺服加载岩石力学试验机进行了岩石疲劳卸围压试验,同时对破坏试样进行了压后裂纹形态CT扫描可视化分析。结果表明：周期性的加卸载作用对大理岩起到了主因损伤作用,卸围压的作用对大理岩起到了根本性的破坏作用。岩石疲劳循环形成滞回环,滞回环面积由疏变密,滞回环加载和卸载曲线接近重合,加卸载模量近似相等;岩石经过卸围压作用,岩石的轴向、径向和体积应变表现为不同程度增大,表明应变对围压降低具有强敏感性,敏感程度由高到低依次为体积应变、径向应变和轴向应变;由于疲劳循环的影响,卸围压作用产生的围压降幅随循环次数增多而降低,卸围压时长随循环次数增多而减少;量化宏观应变变形,求得应变损伤指数Da,Dr和Dv,疲劳循环次数越多,应变损伤指数越大;岩石破坏后细观CT扫描揭示了疲劳循环损伤对岩石破裂形态影响的内在机制,随疲劳循环次数的增加裂纹密度和规模显著增加。研究成果可为地下工程疲劳活动规律和开挖卸荷问题提供理论和模型支撑。     

利用岩石声发射凯塞效应测定岩体地应力

将砂岩在整个变形阶段的声发射信号特征可划分为加载初期、压密阶段、裂纹稳定扩展阶段、裂纹非稳定扩展阶段、砂岩破坏阶段5部分。利用岩样声发射信号的特征,确定出岩石的凯塞效应点与其裂纹稳定扩展阶段的起始点相对应,并进一步得出岩石凯塞效应点的上限为裂纹稳定扩展阶段的终点,裂纹非稳定扩展阶段的起始点。凯塞效应点受岩样两端面的平行度、压机加载速率等有关,岩样端面不平整,在加载初期会有强烈的声发射信号;压机加载速率过大,声发射信号可能显示不出来或被后续更强的声发射信号所掩盖。计算出深度为670m处巷道周围天然应力3个主应力的大小和方向,与在现场用应力解除法和水压致裂法测得的天然应力相比,其数值基本一致,但方向存在一定的偏差。     

高水压条件下大理岩破坏机理试验研究

锦屏二级水电站深埋隧洞中大理岩洞段处于高水压力和高应力环境中, 该段在施工过程中多次发生严重突水灾害。对该段大理岩的高水压条件岩石力学试验表明, 高水压条件下, 岩石应力-应变曲线在峰值应力附近出现明显平缓段, 应力降大, 岩石峰值强度及脆性破坏后破碎程度随水压力升高而升高, 岩石试件以压致拉裂破坏为主。基于高水压条件下裂纹周边应力解析分析, 认为裂隙中高水压力存在降低了裂隙尖端附近高应力集中效应, 与加载方向一定小夹角范围内的微裂隙尖端附近最大拉应力集中程度接近, 这使得岩石中应变能可进一步积累、压致拉裂型微裂隙数量进一步增加, 岩石呈脆性破坏, 并且破碎程度明显增加。研究工作对深埋隧洞突水灾害防治及强降雨诱发高速滑坡灾害预防具有重要的理论和现实意义。     

一种基于弹性能释放率的岩石新型统计损伤本构模型

为了揭示岩石变形的破坏机理以及岩石材料产生损伤的本质原因,文章对岩石材料变形规律和力学特性进行分析后,再以损伤变量作为影响岩石变形和力学性能变化的内变量,采用能量原理、有效应力原理和统计损伤理论构建了一种基于弹性能释放率的新型岩石统计损伤本构模型。该损伤模型进一步完善了岩石损伤本构模型的理论体系,弥补了传统损伤模型无法合理解释引发岩石破坏原因的不足。利用岩石试验数据对损伤模型的参数进行确定,并将损伤演化模型代入弹性能-应变模型中,分析在加载过程中岩石弹性能变化的规律。结果表明:模型曲线与试验曲线在峰前变形阶段几乎重合,说明损伤模型可以很好地反映岩石的变形特性;在初始加载阶段,岩石的损伤变量随着轴向应变的增大而增大,说明在荷载作用下,岩石内部裂隙逐渐发展发育,使得岩石材料的损伤逐步积累;在围压达到10 MPa以上时,损伤-应变曲线基本重合。同时,在初始加载时刻,损伤-应变曲线增长率急剧上升,大约在岩石应变为0.01%时,损伤-应变曲线趋于平稳变化状态;且由于岩石在峰值应力点附近损伤迅速累积,进而使得损伤变量在数值上快速增大到1,这说明了围压的增大使得岩石破坏极限得到显著的提升。     

Experimental verification of the Kaiser effect in rocks

Summary The Kaiser effect is a measure of damage developed in rock. It was investigated using 61 core specimens of eight types of rocks under uniaxial cyclic loading. The effects of the delay time between subsequent loading cycles and the holding time on the Kaiser effect were examined in granite specimens. The characteristics of AE occurring during unloading and holding were also studied. The experimental results showed that most of the rocks, with the exception of some iron ores, showed an obvious Kaiser effect before the load was very near the level of the strength. The delay and holding times did not strongly influence the Kaiser effect. Breakdown of the Kaiser effect was expressed by the felicity ratio that may be taken as a measure of the quality of rock. The onset of the continuously increasing AE in the first loading cycle can be taken as a measure of the damage in rock. The mechanism of the Kaiser effect was studied with the aid of a micromechanical model. An expression for the damage surface in the stress space was derived from the model. The theoretical expression was compared with the results of the Kaiser effect tests, which showed a satisfactory consistence.     

A new method for estimation of the crustal stress from cored rock samples: Laboratory study in the case of uniaxial compression

We present a new method by which the maximum previous stress in rocks can be estimated. The Kaiser effect in acoustic emission is often used for an estimation of the stress to which rocks have been subjected. However, there are cases in which the Kaiser effect is not clear. In such cases, estimation of the previous stress is difficult by the conventional method which is based on the acoustic emission activity during one stress cycle. Using a new method of cyclic loading, we can estimate the stress in cases where the conventional method does not work. In the new method, the difference of the acoustic emission activity between the first and second reloading begins to increase markedly at the previous maximum stress. Even if the Kaiser effect is not clear, we can estimate the previous stress by observation of this difference.Our new method may be applicable for estimating the crustal stress. In this paper, we study the influence of water and temperature under uniaxial compression, because rocks in the earth's crust are saturated and subjected to high temperatures and they are disturbed by water and temperature in the sampling process. The present experiment shows that the Kaiser effect is often masked by changes in water content and temperature. However, we can estimate the previous stress by the new method even after the rock has been disturbed by water and temperature. The accuracy in the stress estimation by this method is satisfactory for the ratio of the previously applied stress to the fracture strength of the rock less than 40%.     

Marble bowing: comparative studies of three different public building facades

The veneer cladding of the Oeconomicum (OEC, Göttingen), the State Theatre of Darmstadt (STD, Darmstadt) and of the State and University Library (SUB, Göttingen) is characterised by pronounced bowing after a short time of exposure. Direct comparison of bowing data related to measurements from 2000 to 2003 at the SUB clearly show that the amplitude in bowing had significantly increased. The bowing is different in intensity and orientation (concave, convex). The cladding material (Peccia marble, Rosa Estremoz marble and Carrara marble) are different in lattice preferred orientation, grain size distribution and grain interlocking. Depending on the bowing, panels may show cracks mostly initiated at the dowels. The percentage of visible cracks and breakouts increases with the amplitude of bowing except for the STD. Repetitive heating–cooling under dry conditions leads to considerable inelastic residual strain only after the first or second thermal cycle. The residual strain continuously increases again if water is present, whereby the moisture content after a thermal cycle has a certain impact on the decay rate. The water-enhanced thermal dilatation strongly correlates with the deterioration rate obtained from the laboratory bow test. Detailed petrophysical investigations provide evidence that with increasing bowing a decrease of mechanical properties (flexural strength or breaking load at dowel hole) occur. Marble degradation is also connected with the increase in porosity and a general shift of the maximum pore radii to larger pore sizes. On-site damage analyses were combined with laboratory tests of the bowing potential to constrain factors that may influence the risk failure. The experimental bowing data clearly demonstrate that after 40 heating cycles combined with the effect of moisture a certain impact on the decay rate is observed. In the case of demounted panels the bowing tests show that already strongly deformed panels from the building exhibit a lower bowing potential than those with lower amplitudes of bowing. This is not the general case for all marble types. Finally, the artificial bowing causes a significant reduction of the flexural strength and the breaking load at the dowel hole. The strength loss of the experimentally aged claddings combined with on-site damage analyses led to conclusions concerning risk assessment and the predicted lifetime of the investigated marble claddings.     

Fatigue-Damage Evolution Characteristics of Interbeded Marble Subjected to Dynamic Uniaxial Cyclic Loads

In this work, uniaxial fatigue tests combined with post-test X-ray computed tomography (CT) scanning were conducted on marble samples with different interbed orientations, in order to reveal the anisotropic damage evolution characteristics during rock failure. The dynamic elastic modulus, damping ratio, fatigue deformation, damage evolution, accumulative damage modeling and crack pattern were systematically analyzed. The testing results indicate that the interbed structure in marble affects the damage evolution and the associated dynamic mechanical behaviors. The damage curve in “S” style indicates three-stage trend, namely, initial damage stage, steady damage stage and the accelerated damage stage. The damage index during cyclic deformation for marble presents obvious discrepancy. In addition, a fatigue damage prediction models was employed numerically as double-term power equations based on the experimental data. It is found that the selected damage model is suitable in modeling the rapid damage growth in the early and final stage of rock fatigue lifetime. Moreover, post-test CT scanning further reveals the anisotropic damage characteristics of marble, the crack pattern in the fractured sample is controlled by the interbed structure. What is more, the most striking founding is that the fracture degree is in consistent with the damage accumulation within the steady damage stage. Through a series of damage mechanical behavior analysis, the internal mechanism of the effect of interbed orientation on damage evolution of marble is firstly documented.

     

锦屏大理岩蠕变损伤演化细观力学特征的数值模拟研究

岩石的蠕变损伤和断裂是岩石流变效应的重要表现形式,但其损伤演化过程往往难以直观观测,为此,采用二维颗粒流数值模拟方法(PFC2D)对岩石的蠕变损伤和断裂的细观力学机制进行了分析。在锦屏大理岩室内试验基础上,利用颗粒流应力腐蚀模型(PSC),建立了能反映其短期和长期强度特征的柱状岩样数值模型,并开展了大量数值试验。结果表明,蠕变损伤的演化过程与暂态的损伤演化过程具有明显的差异。在岩样蠕变损伤过程中,其内部微裂纹多沿加载方向开裂且分布均匀,先快速增加再稳定扩展,最后则发生快速断裂。当荷载较小时,岩样宏观上呈现劈裂破坏特征,当荷载较大时,岩样呈现剪切破坏特征。在岩样蠕变损伤初始和稳定演化阶段的前期,荷载大小对岩样的损伤演化过程影响不大;在稳定演化阶段的后期至断裂过程中,低荷载下岩样的损伤增速比高荷载下快。     

液氮冻结对岩石抗拉及抗压强度影响试验研究

液氮温度极低（?195.8℃）,当与储层岩石接触时,能够改变岩石物性并对岩石结构产生损伤致裂,因此,可用于储层压裂改造。为了研究液氮压裂时低温对岩石力学性能的影响,分别对不同含水状态（干燥与饱和）的不同类型（大理岩、砂岩和花岗岩）岩石进行液氮冻结处理,并对冻结前、后岩样进行抗拉及单轴抗压强度对比测试。结果表明,经液氮冻结后,岩石的单轴抗压强度、抗拉强度和弹性模量都降低;岩石在干燥状态下,液氮冻结对大理石强度的影响大于对红砂岩的影响;岩石饱和水状态下,液氮冻结对红砂岩强度的影响大于对大理岩的影响;饱和水状态岩石经液氮冻结后,其应力-轴应变曲线在弹性变形阶段出现一个拐点;对于同种类型岩石,饱和水状态能加剧液氮冻结并对岩石损伤,岩石强度影响显著;对3种岩样微观结构进行了电镜扫描（以大理岩为例进行分析）,发现经液氮冻结后在矿物颗粒之间生成了微裂隙。研究结果可为进一步研究液氮压裂机制提供试验依据。     

Analysis of the surface of different marbles by X-ray photoelectron spectroscopy (XPS) to evaluate decay by SO2 attack

Atmospheric pollution is one of the main agents of decay in monuments and other works of art located in industrialised urban centres. SO₂ is a permanent and abundant component of air pollution and, although it does not have an immediate visual effect, after continuous exposure, it can cause irreversible damage to building materials. Marble is one of the most commonly used ornamental stones in historical monuments and its mineralogical composition makes it very susceptible to damage caused by exposure to SO₂. To measure the chemical reactions caused on marble by the action of atmosphere rich in SO₂, selected calcitic and dolomitic samples were altered by weathering accelerated test. For this, seven marble types (four calcitic and three dolomitic) were exposed to high concentration of sulphur dioxide for 24 h in a climate chamber under controlled temperature and humidity conditions (20 °C and > 90 % HR). Changes on marble surfaces caused by reactions of SO₂ with calcite and dolomite were studied using two non-destructive techniques: chromatic change by means of colorimetry and chemical analysis using X-ray photoelectron spectroscopy (XPS). The development of new mineral phases was also observed by scanning electron microscopy. Colorimetric analysis revealed a decrease in lightness and chromatic parameters suggesting that these changes were due to the development of new mineral phases in all marbles. The XPS technique, which is generally used in the analysis of metals, is relatively new in the field of stone deterioration. It enabled us to recognise the development of sulphites and sulphates on marble surfaces with high precision, after just 24 h of exposure to high SO₂ concentrations and to distinguish different decay paths for calcitic and dolomitic marbles.