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1.
本文研究了在HCl介质中,D401(EDTA)螯合树脂对铂、钯的吸附性能。实验表明,在pH=2~4范围内,树脂对钯有良好的吸附性能,饱和吸附量70.5mgPd(Ⅱ)/g—R。PH≥4时对铂不吸附;钯的负载柱可用[0.1molTu(硫脲)+0.5molHCl]/L混合液定量洗脱,洗脱率为99.2%、获得了pH=4盐酸溶液中树脂柱分离铂、钯的方法。  相似文献   

2.
本文研究了D_001大孔阳离子强酸树脂从H_2SO_4-CS(NH_2)_2溶液中,富集及分离Au(I)、Ag(I)的性能。表明在pH=2.0左右,树脂对Au(Tu) ̄+_2、Ag(Tu) ̄+_2(Tu=硫脲)有良好的吸附性能,Au和Ag的吸附容量分别为61.18mg/g-Resin和99.11mg/g—Resin。负载柱上的Au、Ag可分别用NaCN—NaOH和H_3BO_3-NaOH-Na_2S_2O_3定量洗脱。可进行一定程度的Au、Ag分离。  相似文献   

3.
本矿床是我国金红石矿床重要的成因及工业类型,为具有特定化学成分的岩石在特定变质条件下形成的。本文通过对大量数据的处理,查明了化学成分与成矿的关系:高Al2O3、MgO、Fe2O3+FeO、K2O、P2O5、H2O+、MnO,低SiO2、CaO、Na2O、CO2、S等,利于钛富集;高TiO2、MgO、P2O5、S,低SiO2、CaO、K2O、Al2O3、Fe2O3/FeO,利于金红石形成;高Sc、Zr、Ni、Zn及La/Yb,低Y、Nb、Th、Cd、Ba、Be、ΣREE,利于金红石纯度提高。对研究矿床成因及寻找新的同类矿床等有重要意义  相似文献   

4.
沙虫干呈味及功能性成分研究   总被引:2,自引:1,他引:1  
对沙虫干抽提物成分的组成进行的研究结果表明:游离氨基酸含量w为10.3%,占抽提物含氮物质的77.9%。抽提物组成中呈甘味的Gly(3.2%)、Ala(2.5%)和呈鲜味的IMP(0.27%)、Glu(0.25%)、琥珀酸(0.35%)等成分同沙虫干独特的风味有关,Na^+、Cl^+等无机离子同其呈味相关,此外,牛磺酸含量w高达3.2%,是富含牛磺酸的一种海洋生物;精氨酸的含量w亦较高,为1.2%  相似文献   

5.
着重研究了红海湾养殖区底质水中NO3^--N、NO2^--N、NH4^+-N、PO4^3--P、有机质及c(NO3^--N)/cp和∑cn/cp(∑cn=c(NO2^-)+c(NO3^-)+c(NH4^+)比值的分布特征,并对该湾低质水中氮、磷及有机质的季节变化及其它们之间的相互关系作了讨论,结果表明:在春、夏、;冬三个季节中,NH4^+-N的浓度比NO2^--N及NO3^--N高,春季NH4^+-N平均浓度为92.60μmol/L,占总无机氮80.57%;夏季浓度为47.04μmol/L,占总无机氮61.64%;冬季NH4^+-N的浓度最低,为9.60μmol/L,占总无机氮45.76%;而夏季PL4^3--P浓度及有机质的含量比春、冬季高,分别为53.68μmol/L和1.362%。分析指出该湾底质水中无机  相似文献   

6.
大孔树脂纯化菠萝皮黄酮类化合物的研究   总被引:1,自引:0,他引:1  
通过静态吸附与解吸实验,比较7种树脂对菠萝皮黄酮类化合物的吸附和解吸特性,筛选出较优的菠萝皮黄酮类化合物吸附剂,并检测吸附流速、上样液浓度、pH值、洗脱流速、洗脱剂体积分数等动态吸附性能。结果表明:AB-8树脂具有较好的吸附和解吸效果,吸附流速1mL/min、上样液浓度2.25mg/mL、pH值6、洗脱流速0.5mL/min、洗脱剂体积分数90%条件下,AB-8型大孔树脂可用于菠萝皮黄酮类化合物的分离纯化。  相似文献   

7.
从北部海沿海采捕的日本鬼You(Inimicus japonicus)亲鱼,经暂养后进行催产,雌鱼每千克体重注射LRH-A310-μg+DOM5mg或HCG600~800IU+LRH-A330~40μg;雄鱼注射同样药物,剂量减半。共采卵109万粒,平均受精率89.0%,平均孵化率为90.0%,共培育出体长1.8~2.8cm的幼鱼26.8万尾,平均成活率30.7%。  相似文献   

8.
用乙醇提取螺旋藻中的叶绿素,再用5%NaOH溶液皂化、石油醚萃取,在酸性环境中用10%CuSO4溶液实现铜镁置换,沉淀物经丙配溶解后,加2%NaOH的乙醇溶液成盐,过滤,水洗,真空干燥,制成叶绿素铜钠盐.制品的质量达到GB3262-82的要求.提取率为64.7%,制品得率占藻粉1.1%。着重对铜镁置换的条件、制品耐酸、耐热、耐光等性能进行了对比试验,结果表明整个工艺是切实可行的.  相似文献   

9.
综合应用电子显微镜、扫描电镜、阴极发光、X衍射、稳定同位素分析和流体包裹体分析测试等技术,通过半定量化研究深入探讨了莺歌海盆地 XF13区块黄流组储层中富 CO2 和富烃类气两类气体充注对储层中碳酸盐胶结物形成的影响,结果表明:①靠近底辟的 XF13A、XF13B井受到了晚期富 CO2 热流体充注影响,促进了 溶 蚀作用(次生孔隙比例为39.9%~58.4%),但由于处于幕式半开放的封闭成岩体系中,溶蚀过程中形成的大量Ca2+ 、Mg2+ 、Fe2+ 等离子没有及时排出,这些离子重新化合沉淀形成大量晚期碳酸盐胶结物,使得碳酸盐胶结物体积分数(4.5%~13.5%)和类型增多,进而破坏孔隙喉道,形成中孔 低 渗 储 层;②远 离 底 辟 的 XF13E、XF13F等井黄流组储层主要是早期烃类气充注,溶蚀作用较弱(次生孔隙比例为7.2%~27.7%)且处于开放的酸性热液体系中,造成碳酸盐胶结物体积分数(1.0%~6.0%)和类型相对较少,形成中孔中渗储层。   相似文献   

10.
为查明有机质微生物降解过程对地下水系统中碘迁移富集的影响,以大同盆地为研究区,对区内22组地下水样品进行了水化学和生物标志物研究。水化学分析结果表明,地下水碘质量浓度为5~1212μg/L,其 中,56.52%的地下水样品中碘质量浓度超过饮用水标准限定值150μg/L。地下水样品生物标志物分析结果显示,可提取饱和烃中存在大量“未分辨组分(UCM)”;CPI1 和 CPI2 分别为0.38~1.03和0.27~1.19;低相对分子质量正构烷烃无明显奇偶优势。上述生物标志物特征表明,含水层中有机质经历了强烈的微生物降解。有机质微生物降解产生的 HCO-3 通过竞争吸附,导致沉积物中吸附态碘的解吸附并在地下水中富集。此外,有机质的微生物降解有利于迁移能力强的低相对分子质量有机质或有机胶体的形成,该类有机物通过吸附或螯合作用进一步促进碘在地下水中的富集。   相似文献   

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12.
Based on the hydrographic data in austral summer during the 22nd Antarctic Expedition of China(2005/2006),some features can be found about the northern margin of Emery ice shelf as follows.The heat content in the surface layer(0-50 m) at the eastern end and the western end of the ice-shelf margin is much higher than that at the middle.The upper mixing-layer depth and the seasonal thermocline depth at the middle of the ice-shelf northern margin are much shallower than those at the both ends.However there is much less difference between the middle and the ends in the bottom layer.The remote sensing photos show that the inhomogeneity in the surface-layer water is closely related to the spatial distribution of the floes and polynia in the area.  相似文献   

13.
Phylogenetic analysis based on 16S rDNA of 8 strains of cultivable bacteria isolated from Arctic sea-ice was studied.The results showed that strain BJ1 belonged to genus Planococcus,which was a genus of low mole percent G C gram-positive bacteria;strain BJ6 belonged to genus Burkholderia of β-proteobacteria and the rest 6 strain all belonged to γ-proteobacteria,of which strain BJ8 was a species of Pseudoalteromonas,strain BJ2-BJ5 and BJ7 were members of genus Psychrobacter.Phylogenetic analysis also indicated that bacteria of genus Psychrobacter of the isolates formed a relatively independent phylogenetic cluster in comparison with other bacteria belonged to genus Psychrobacter.  相似文献   

14.
正1 Aims and Scope Advances in Polar Science(APS)is an international,peer-reviewed journal jointly sponsored by the Polar Research Institute of China and the Chinese Arctic and Antarctic Administration.APS is a comprchensive academic journal dedicated to presentation of multi-disciplinary achievements in Arctic and Antarctic expeditions and research.Its primary purpose is to publish achievements in fundamental research,applied  相似文献   

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16.
《山地科学学报》2014,(4):I0004-I0009
<正>AIMS AND SCOPE(Editorial Policy)The Journal of Mountain Science(JMS)is devoted to mountains and their surrounding lowlands-ecoregions of particular global importance,with a particular emphasis on the important highlands/mountains in the world,such as the Tibetan Plateau,the Himalayas,the Alps,the Andes,the Rockies and many other mountain ranges of our planet.  相似文献   

17.
<正>The Journal of Mountain Science(JMS),founded in2004,is an international English-language journal on mountain sciences.JMS is supervised by the Chinese Academy of Sciences(CAS),sponsored by the Chengdu Institute of Mountain Hazards and Environment,CAS,published by Science Press China,and distributed by Springer exclusively throughout the world(excluding Mainland China).The JMS is published bimonthly,fulltexted in SpringerLink and CNKI,indexed/abstracted by  相似文献   

18.
Using the NCEP/NCAR reanalysis monthly 500 hPa height data on a 2.5 latitude-longitude grid and 1°×1° sea ice data,the polar vortex area,intensity index and arctic sea ice area index are calculated respectively,and the meridional distribution,period variation and the abrupts in the long range trend are analyzed to study their relationship.The results show that the meridional distribution of sea ice and polar vortex h-ave distinctive difference,the relative positions of them are different in the eastern and western hemispheres,and exept they have periods of 4 months,quasi half year,quasi year,4-5 years and 10 years commonly,and each of them has its own respective variation as well.The sea ice area is decreasing apparently since 1980's,so is the polar vortex area,but their abrupt changge time are different totally.The area of sea ice and polar vortex has prominent positive correlation,but the relationship of sea ice intensity,polar vortex intensity,polar vortex area is complicated.  相似文献   

19.
The ability of cell to modulate the fluidity of plasma membrane was crucial to the survival of microorganism at low temperature. Plasma membrane proteins, fatty acids and carotenoids profiles of Antarctic psychrophilc yeast Rhodotorula sp. NJ298 were investigated at -3 ℃, 0 ℃ and 8 ℃. The results showed that plasma membrane protein content was greater at -3 ℃ than that at 8 ℃, and a unique membrane polypeptide composition with an apparent molecular mass of 94.7 kDa was newly synthesized with SDS-PAGE analysis; GC analysis showed that the main changes of fatty acids were the percentage of unsaturated fatty acids (C18∶ 1 and C18∶ 2) and shorter chain saturated fatty acid (C10∶ 0) increased along with the decrease of the culture temperature from 8 ℃ to -3 ℃; HPLC analysis indicated that astaxanthin was the major functional carotenoids of the plasma membrane, percentage of which increased from 54.6±1.5% at 8 ℃ to 81.9±2.1% at -3 ℃. However the fluidity of plasma membrane which was determined by measuring fluorescence anisotropy was similar at -3 ℃, 0 ℃ and 8 ℃. Hence these changes in plasma membrane's characteristics were involved in the cellular cold-adaptation by which NJ298 could maintain normal plasma membrane fluidity at near-freezing temperature.  相似文献   

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