Constraints of archaeomagnetic dating and field intensity determinations in three ancient tile kilns in Belgium

The aim of this study is to date by the archaeomagnetic method the last heatingcooling cycle of one Roman and two Medieval tile kilns, discovered in Belgium. The investigation demonstrates the limitations when well-documented local directional secular variation curves of the geomagnetic field in the past are used for dating and the difficulties when trying to determine field intensities from “in situ” baked clays from the kilns. The three kilns yielded very well defined ancient field directions but two possible dating solutions for each of them when no a priori time constraints are taken into account, due to field direction recurrence. As an increase of the dating accuracy and reduction of the number of dating solutions can be expected using the full field vector information, also field intensity determinations on burnt clays from the kilns were attempted. Field intensities from samples of the Roman and of one of the Medieval kilns are quite scattered. On the other hand, results obtained applying the Thellier-Thellier method and the modified method developed by Dekkers and Böhnel on sister samples from the Roman kiln agree fairly well. Rock magnetic properties reveal high variance in the kilns that point to varying spatial heating and cooling conditions in the kilns. Even well burnt material from the kilns shows irreversible changes when heated in air in the laboratory. Reliable field intensities on “in situ” baked materials from kilns themselves can therefore only be obtained when measuring sufficient number of samples from different parts of the kiln, taking into account the spatial-temporal conditions during kiln operation and cooling history. More reference intensity data is needed in our regions in order to improve dating based on directional reference data only.     

Preliminary Archaeomagnetic Results from a Floor Sequence of a Bread Kiln in Lübeck (Germany)

A sequence of 25 bread-kiln floors was sampled for archaeomagnetic measurements in a bakehouse in the old town of Lübeck, Germany. Due to archaeological dating this kiln floor sequence has been built up presumably from the late 13 ^th to the 18 ^th century. The primary magnetisation component is carried by magnetite (maghemite) and is very stable. Small viscous magnetisation components could be removed easily. The preliminary results of characteristic remanent magnetisation for 23 of the kiln-floor layers show clearly the trend of the geomagnetic secular variation expected for that time interval. By comparison with French and British master curves, the kiln-floor sequence started around 1425 and lasted until 1775 AD. Presently, confidence circles are relatively large and need refineing by measuring more samples, which have already been collected. Together with ¹⁴ C dating that can be determined from the charcoals found in the lowest layers and thermoluminescence dating of the layers, we expect to obtain, for the first time, a secular variation curve for Northern Germany covering the time interval from 1400 to 1800 years AD.     

Archaeomagnetic secular variation in the UK during the past 4000 years and its application to archaeomagnetic dating

This paper examines the limitations and deficiencies of the current British archaeomagnetic calibration curve and applies several mathematical approaches in an attempt to produce an improved secular variation curve for the UK for use in archaeomagnetic dating. The dataset compiled is the most complete available in the UK, incorporating published results, PhD theses and unpublished laboratory reports. It comprises 620 archaeomagnetic (directional) data and 238 direct observations of the geomagnetic field, and includes all relevant information available about the site, the archaeomagnetic direction and the archaeological age. A thorough examination of the data was performed to assess their quality and reliability. Various techniques were employed in order to use the data to construct a secular variation (SV) record: moving window with averaging and median, as well as Bayesian statistical modelling. The SV reference curve obtained for the past 4000 years is very similar to that from France, most differences occurring during the early medieval period (or Dark Ages). Two examples of dating of archaeological structures, medieval and pre-Roman, are presented based on the new SV curve for the UK and the implications for archaeomagnetic dating are discussed.     

Palaeomagnetism of silurian lavas of Somerset and Gloucestershire,England

Detailed alternating field demagnetisation of Upper Llandovery volcanics of the Mendip Hills and Gloucestershire has isolated remanence directions interpreted as primary from each of five sites. Well-defined high-coercivity secondary magnetisation is present in six samples of one site and low-coercivity secondary remanence is present in all samples from another site; the former component was apparently acquired in Permo-Triassic times. Primary directions of magnetisation show marked improvement in precision after correction for penecontemporaneous folding, and show a late Llandovery reversal in the sense R → N.The group mean directions of magnetisation isD = 243.5°,I = 47.5° (precision parameterk = 29). Petrographic examination confirms observations from magnetic properties that relict titanomagnetite (oxidation classes 3 to 5) is the remanence carrier in most samples. Hematite, probably mostly late magmatic in origin, is widely developed in all samples, but only the principal remanence carrier where it has thoroughly replaced the titanomagnetite. Low-coercivity remanence is apparently caused by weathering effects but there is no clear visible cause for secondary high-coercivity remanence carried by some samples.The mean virtual geomagnetic pole position is close to Upper Silurian/Lower Devonian pole positions from other parts of Britain and defines a minimum apparent polar shift of 60° between late Ordovician and Upper Llandovery times. Reference to absolute age dates suggests that this shift took place between ca. 447 and 434 m.y. followed by slight polar movement between ca. 434 and 394 m.y.     

Historical measurements of the Earth's magnetic field compared with remanence directions from lava flows in Italy over the last four centuries

Direct measurements of the Earth's magnetic field in Italy since 1640 a.d. have been used to check the remanence directions derived from historically dated volcanic rocks of Etna and Vesuvius. Direct measurements consist of the records of L’Aquila and Pola geomagnetic observatories, the repeat stations of the Italian Magnetic Network and the data base of the Historical Italian Geomagnetic Data Catalogue. All have been relocated to the same reference site (Viterbo — lat. 42.45°N, long. 12.03°E) in order to draw a reference secular variation (SV) curve. The direction of the Earth's field at Viterbo has also been calculated from the historical records (2000-1600) of ref. [Jackson, A., Jonkers, A.R.T., Walker, M.R., 2000. Four centuries of geomagnetic secular variation from historical records. Phil. Trans. R. Soc. London, Ser. A 358, 957-990] database. The remanence directions from Etna show a general agreement with the trend of the SV curve, although their inclination is usually lower than that from the direct measurement. The directions from Vesuvius are more scattered. Large discrepancies occur at both volcanoes and in some cases have been ascribed in the literature to poor geographic information, making it difficult to identify the flows actually emplaced during the eruptions reported in the chronicles. Closer examination shows that the great majority of the best-defined remanence directions (semi-angle of confidence α₉₅ < 2.5°) deviate significantly from the geomagnetic direction measured at the time of the emplacement, the angle between the two directions being larger than the α₉₅ value. The value of 2.5-3.0° can thus be regarded as a conservative evaluation of the error when dealing with dating Etna and Vesuvius lava flows older than 17th century, even when the accuracy attained in remanence measurements is higher. In default of a SV curve for Italy derived from archaeological artefacts, a further error in dating is introduced when reference is made to SV curves of other countries, even if well-established, as these are from regions too far from Italy (>600 km) to confidently relocate magnetic directions.     

Behaviour of the earth's magnetic field as recorded in the sediment of Loch Lomond

A palaeomagnetic record of geomagnetic secular variation during the last 7000 years has been obtained from the sediments of Loch Lomond, Scotland. The magnetic direction fluctuations repeat well between cores and show greater detail, especially over the last 5000 years, than other European records. A time scale has been derived from¹⁴C analyses on the Lomond sediment and comparison with other¹⁴C-dated sediments. Investigation of relative palaeointensity determination methods has shown that the widely used normalization parameter of partial ARM is insensitive to even small sediment grain size fluctuations.The new high-fidelity direction record and improved time scale show that geomagnetic field changes have not followed a simple oscillatory pattern during the last 7000 years. The record enhances the application of palaeomagnetism to dating recent sediments, as the main declination swings are now characterized by fine detail, and paired inclination data are also available. The problem of mismatching swings when correlating with other paired directional records is thus reduced.The palaeomagnetic record agrees well with some archaeomagnetic results. It confirms the period of anticlockwise motion of the geomagnetic field vector, between 1000 and 600 years B.P., which was first documented by English archaeomagnetic investigations. Clockwise motion is shown to predominate during the remainder of the last 5500 years. The VGP path does not correlate with that of Japanese archaeomagnetic results nor North American sediment data from 2000 to 0 years B.P. This suggests that the secular changes are dominated by local non-dipole sources rather than wobbling of the main geomagnetic dipole.     

Geomagnetic secular variation from recent lake sediments,ancient fireplaces and historical measurements in southeastern Australia

Compilations of historical observations, archaeomagnetic data from ancient fireplaces and palaemagetic results from short cores of sediment from lakes in southeastern Australia, particularly Lake Keilambete, provide a detailed record of the geomagnetic secular variation during the last 3000 years. The independent sets of data are in good agreement if the radiocarbon time scale for the lacustrine record is about 450 years too old. The error is attributed to systematic incorporation of ancient carbon into the lake floor sediments, mainly through erosion of sediment on the crater walls at times of low water level. A significant lag between deposition and the acquisition of stable magnetic remanence is ruled out. Inclination has been abnormally steep during the last 500 years but remained fairly close to the axial dipole field value prior to that. During the last 1000 years the predominant sense of looping of the magnetic vector corresponds to westward drift of the nondipole field. Secular variations on a time scale of ～ 100 years can be resolved by the lacustrine record.     

Archaeomagnetic study and rehydroxylation dating of fired-clay ceramics

Archaeomagnetic study and rehydroxylation dating of fired-clay ceramics from Great Britain, Spain, and the Black Sea region is carried out in order to refine the dating of the material from the archaeological monuments used in the archaeomagnetic research for determination of the elements of the main magnetic field during the past few millennia. The archaeomagnetic analysis revealed the factors responsible for deviations of the rehydroxylation dating from the true values. They include the processes of weathering (magnetite transformation into hydroxides) and secondary magnetization (e.g., magnetization in a fire). In order to bring the dating closer to the true values, corrections for the influence of the distorting factors are suggested. The data on the geomagnetic field intensity derived from the magnetization of the studied material are used as independent criteria to validate the dating of the field. When applied to the fired clay material with reliable dating, the rehydroxylation method provides the estimates of the temperature in the region of archaeological monuments during the past.     

Geomagnetic Field Variations as Determined from Bulgarian Archaeomagnetic Data. Part II: The Last 8000 Years

The knowledge about past secular variations of the geomagnetic field is achieved on the basis of archaeomagnetic researches of which the Bulgarian studies form an extended data set. In Part I (Kovacheva and Toshkov, 1994), the methodology used in the Sofia palaeomagnetic laboratory was described and the secular variation curves for the last 2000 years were shown. In Part II (this paper), the basic characteristics of the prehistoric materials used in the archaeomagnetic studies are emphasised, particularly in the context of the rock magnetic studies used in connection with palaeointensity determinations. The results of magnetic anisotropy studies of the prehistoric ovens and other fired structures are summarised, including the anisotropy correction of the palaeointensity results for prehistoric materials, different from bricks and pottery. Curves of the direction and intensity of the geomagnetic field during the last 8000 years in Bulgaria are given. The available directional and intensity values have been used to calculate the variation curve of the virtual dipole moment (VDM) for the last 8000 years based on different time interval averages. The path of virtual geomagnetic pole (VGP) positions is discussed.     

Comparison of the Brunhes epoch geomagnetic secular variation recorded in the volcanic and sedimentary rocks

The results of numerical modeling of the geomagnetic secular variation by the method of the Giant Gaussian Process (GGP) are presented and compared with the information derived from the presentday databases for paleointensity. The variances of the positions of the virtual geomagnetic pole (VGP) calculated from the synthetic and experimental data (Brunhes epoch, effusive rocks) are nearly similar, which supports the validity of the theoretical model. The average value of the virtual axial geomagnetic dipole (VADM) calculated from the PINT world database on paleointensity and the Sint-2000 model is lower than VADM calculated by the GGP model; at the same time, the estimates based on the archaeomagnetic data give the VADM value slightly above the model prediction. The largest difference is observed in the variances of VADM, which is for all the three databases noticeably higher than the value calculated from the GGP model. Most probably, this is due to the contribution of the neglected measurement errors of VADM.     

中国四川地区地球磁场强度的长期变化

运用 Thellier 逐步热退磁法,主要测定了我国四川一些地区新石器时期至明、清各朝代的地球磁场总强度值。本文结果表明,在过去5000多年里,该地区地球磁场的总强度随时间呈较大幅度的变化。将该地区与我国其它相关地区地球磁场总强度的长期变化曲线进行对比研究的结果表明:变化的总趋势大致可比,但最高值出现的时间不同.从过去四千年间,新疆、四川、广东、福建及洛阳一些地区的地球磁场强度变化曲线中最高峰和跨时千余年的"M"型变化中低峰出现的时间推得的滞后速度在0.01°-0.03°/a 之间。     

Fluctuations of magnetic inclination and declination in Mexico during the last three millennia

Revealing the evolution of the past geomagnetic field is of dual interest. It is crucial to estimate the conditions of the Earth's deep interiors, while it offers a reliable absolute dating tool of burned archaeological artifacts. Although a substantial effort was paid during the last decade to construct a reference archaeomagnetic curve for Mesoamerica, mostly absolute intensity variations are revealed for the previous three millennia. Here, we report an updated directional (inclination and declination) reference secular variation curve based on volcanic lava flows and archaeological artifacts carrying full thermoremanent magnetization. A bootstrap method with penalized cubic b-splines was used to develop the directional curve. Relocation error exercise and strict selection criteria allowed to use 82 well-defined palaeodirections. Both data distribution density and the firm relationship between the ages and samples, ensure the reliability of the curve for the dating purposes. The combination of directional data with available intensity variation highlights some sudden geomagnetic field fluctuations.     

Palaeomagnetic study of some charnockites of the Palni Hills

The intensity of natural remanence magnetisation (NRM) is measured along the three mutually-perpendicular directions using an astatic magnetometer. The intensity of induced magnetisation is measured using an apparatus fabricated in the laboratory. The Koenigsberger ratio has been calculated for all the samples and the ratio has been used to test the stability of NRM in the samples. The mean direction of magnetisation is determined from the three components of the NRM intensity. The palaeomagnetic pole position of the samples is determined using the direction of magnetisation and the site location. An attempt has been made to fix the geological age of the charnockites using palaeomagnetic methods.     

The characteristics,origins, and geodynamic settings of supergiant gold metallogenic provinces

An investigation of the rock magnetic properties using stepwise isothermal remanence (IRM) acquisition, thermomagnetic analysis and temperature-dependent susceptibility history, identifies magnetite as the carrier of the main fraction of the remanence, associated with maghemite and hematite in Malan loess (L1), Holocene soil (S0) and last-glacial paleosol (S1). The presence of short-lived direction fluctuations indicates that no significant smoothing occurs in L1 when its remanence is locked, and thus L1 is capable of recording the geomagnetic secular variation (PSV), while the PSV has been severely smoothed or wiped out by pedogenic processes during S1 formation. It has been suggested that the Mono Lake and Laschamp excursions are two independent geomagnetic events based on this study.     

新石器时代姜寨遗址的考古地磁研究

通过测量姜寨遗址窑灶烧土标本的剩余磁化方向,确定了公元前四千年左右该遗址所在临潼地区的地磁场方向（倾角和偏角）,采用逐步热退磁法,求出了当时、当地的地球磁场总强度值。由此,按照中心偶极模式算得了当时该地区所在的地磁纬度,以及该时期的虚地磁极位置和地球的虚偶极矩。     

A Regional Archaeomagnetic Model for the Palaeointensity in Europe for the last 2000 Years and its Implications for Climatic Change

The SCHA.DI.00 directional model for the geomagnetic field in Europe for the last 2000 years (Pavón–Carrasco et al., 2008) has been updated by modelling the palaeointensity. This model, SCHA.DI.00, was developed from available Bayesian European Palaeosecular Variation Curves using the regional Spherical Cap Harmonic Analysis technique. The comparison of the palaeosecular variation curves, given by the regional model, with available archaeomagnetic data not used in its development showed an improvement with respect to the fit obtained by global archaeomagnetic models. In this paper advantage is taken of recently published palaeointensity databases to develop a complete (direction and intensity) regional archaeomagnetic model for the last 2000 years valid for the European region: the SCHA.DI.00–F model. Not only does this complete model provide an improvement for example for archaeomagnetic data studies, but it is also shown that this new regional model can be used to study the recently proposed link between the centennial secular variation of the geomagnetic field and climate change. The pattern of the archaeosecular variation of the field intensity obtained by SCHA.DI.00–F seems to verify the hypothesis presented by Gallet et al. (2005) about a possible (causal) connection between changes in the geomagnetic field intensity and in climate parameters, opening the door for more discussions on this challenging subject.     

Archaeomagnetic studies of materials from the Gorelyi Les and Ust-Khaita monuments (Eastern Siberia)

Archaeomagnetic studies of materials from archaeological monuments of the Irkutsk and Baikal regions provided new constraints on the geomagnetic intensity variation in Eastern Siberia for the interval from the 5th millennium BC through the 1st millennium AD. Material from the Gorelyi Les and Ust-Khaita multilayer archaeological monuments of the Irkutsk region is dated according to layer depths of deposits. Data on the geomagnetic intensity obtained from archaeomagnetic studies corroborate the validity of this method of dating. It is established that the average level of the geomagnetic intensity smoothly rose in the interval from the 5th millennium BC through the 1st millennium AD, with faster variations being superimposed on this trend. The pattern of the geomagnetic intensity variation is similar to those in other Eurasian regions.     

Note on the palaeomagnetism of the Sekondi series,Ghana

From a collection of 39 oriented hand-samples at 16 sites, total N.R.M. directions at 12 sites from the Elmina Sandstone (Devonian or possibly Carboniferous) of the Ghana coast fall in a group. Their in-situ mean (D = 334°, $\text{I = +11}\text{1}\text{2}\text{°}$) is significantly divergent from the local geomagnetic field, and does not correlate with expected Palaeozoic remanence directions. A bedding-tilt test suggests that the magnetisation is secondary, and comparison with other African data suggests a Mesozoic (possibly Cretaceous) age. The remanence is only partially stable against thermal demagnetisation. The observations are consistent with a remanence originating at the time of faulting, tilting and uplift which marked the beginning of rifting of South America from Africa.     

Secular variation study from non-welded pyroclastic deposits from Montagne Pelée volcano, Martinique (West Indies)

We present palaeomagnetic data obtained from large clasts collected in non-welded pyroclastic deposits from Montagne Pelée volcano (Martinique Island, West Indies). These deposits, dated by the ¹⁴C method from 5000 yr BP to the present, comprise block- and ash-flows, ash- and pumice-flows and pumice fallouts. Alternating fields treatment was as a routine chosen to demagnetise large samples for which the magnetisation was measured with a specially designed inductometer. The mean directions obtained from block- and ash-flow deposits of the 1902 and 1929 eruptions are in good agreement with the expected geomagnetic directions at these times in Martinique. The so-called P1 eruption (∼1345 AD), which is characterised by a rarely observed transition from a Peléean to a Plinian eruptive style, allows a direct comparison of the palaeomagnetic directions obtained from the three types of pyroclastic deposits. All deposits provide identical mean directions, which further demonstrates the suitability of the non-welded pyroclastic deposits for geomagnetic secular variation study with a very good accuracy and precision. The possibility of using pyroclastic deposits is promising for obtaining a wider distribution of sampling sites, which may better allow us to constrain our knowledge on the geomagnetic secular variation. We find that large geomagnetic changes occurred in Martinique during the last millennium, while the variations appear more limited prior to this period.     

First archaeomagnetic results and dating of Neolithic structures in northern Greece

Archaeomagnetism in Greece has continuously developed during the last decades. Numerous studies have provided high quality data and accurate secular variation curves for the direction and intensity of the geomagnetic field have been constructed. The Greek Secular Variation Curves (SVCs) cover the last 8 millennia for intensity and 6 millennia for direction. The coverage of the archaeological periods remains uneven, with several gaps, mostly in the directional dataset, with only two results for periods older than 2500 B.C. In the present contribution, the first archaeomagnetic results from Neolithic settlements in northern Greece are presented. For the present study, samples were collected from three different archaeological sites: burnt structures in Avgi (Kastoria) and Vasili (Farsala) and one oven from Sosandra (Aridaia). The natural remanent magnetization (NRM) grouping of all specimens indicated that the majority of the samples were burnt in situ, providing thus a reliable direction of the ancient field. Magnetic cleaning (both alternating-field and thermal) revealed the presence of one stable component of magnetisation. Rock magnetic experiments (acquisition of isothermal remanent magnetization (IRM), thermal demagnetisation of the IRM, thermomagnetic curves) have been performed on pilot samples indicating that low coercivity magnetic minerals such as magnetite or Timagnetite are prevailing. The mean directions (declination D, inclination I and parameters of the Fisherian statistics), which arose from the three sites are as follows: Sosandra: D = 343°, I = 55.6°, ??₉₅ = 4.8°; Avgi: D = 10.1°, I = 53.4°, ??₉₅ = 4.2° and Vasili: D = 357.5°, I = 43.1°, ??₉₅ = 4.1°. The obtained data are in a very good agreement with results from Neolithic Bulgaria. This study represents the beginning of an effort to fill the gaps of the Greek secular variation curves and their extension to the Neolithic period.