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发射光谱法测定化探样品中的Cu、Pb、Zn、Co、Ag、Sn、Mo和B
引用本文:王清全,周玉香,王世东,刘祥.发射光谱法测定化探样品中的Cu、Pb、Zn、Co、Ag、Sn、Mo和B[J].吉林地质,2007,26(3):58-61.
作者姓名:王清全  周玉香  王世东  刘祥
作者单位:吉林省第五地质调查所实验室,吉林,九台,130500
摘    要:以Al2O3、K2S2O7、NaF、C作为缓冲剂与样品混匀,装入石墨电极中,以平头石墨电极为上电极,样品电极为下电极进行摄谱,由光电译谱仪测定谱线的黑度值,以锗为内标用内标法测定样品中Cu、Pb、Zn、Co、Ag、Sn、Mo和B的质量分数。

关 键 词:发射光谱  垂直电极  内标法定量
文章编号:1001-2427(2007)03-058-04
收稿时间:2006-07-24
修稿时间:2007-05-12

Determining Cu, Pb, Zn, Co, Ag, Sn, Mo and B in geochemical exploration samples by using optical emission spectrometry
WANG Qing-quan,ZHOU Yu-xiang,WANG Shi-dong,LIU Xiang.Determining Cu, Pb, Zn, Co, Ag, Sn, Mo and B in geochemical exploration samples by using optical emission spectrometry[J].Jilin Geology,2007,26(3):58-61.
Authors:WANG Qing-quan  ZHOU Yu-xiang  WANG Shi-dong  LIU Xiang
Institution:Laboratory, The Fifth Geologic Survey of Jilin Province, Jiutai 130500, China
Abstract:As buffer with Al2O3,K2S2O7,NaF and C,mix with samples,and put them into graphite electrode tube,the flat graphite electrode means the upper electrode,and sample electrode means the lower one to make spectral analysis;the blackness value of the spectral lines are determined by the photoelectric interpreting spectrometry.The Ge is as an intetrnal standard,the contents of Cu,Pb,Zn,Co,Ag,Sn,Mo and B in samples are determined by the internal standard technique.
Keywords:optical emission spectrometry  vertical electrode  determination by internal standard technique  
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