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等离子体直读光谱法同时测定岩石中15个痕量稀土元素
引用本文:袁玄晖,阙松娇,伍新宇,殷宁万.等离子体直读光谱法同时测定岩石中15个痕量稀土元素[J].岩石矿物学杂志,1983,2(2):127-130.
作者姓名:袁玄晖  阙松娇  伍新宇  殷宁万
作者单位:中国地质科学院岩矿测试技术研究所 (袁玄晖,阙松娇,伍新宇),中国地质科学院岩矿测试技术研究所(殷宁万)
摘    要:近年来,着地质学科的研究需要,稀土元素的分析手段不断向深度发展。为了制作稀土球粒陨石标准化分布型武图,要求准确测定痕量稀土元素,同时还由于各种岩石的基体变化不一,造岩元素所产生的谱线干扰以及可变的背景干扰都给痕量稀土元素的测定带来困难,所以,一般都需要进行预处理,将岩石的主元素分离,并使稀土元素相对浓缩。


THE SIMULTANEOUS DETERMINATION OF 15 TRACE RARE EARTFI ELEMENTS IN ROCKS BY PLASMA ATOMCOMP DIRECT READING SPECTROMETER SYSTEM
Abstract:A method for the determination of rare earth elements at chondritic abundance levels is described. Dissolution of rock samples is accomplished by sodium peroxide fusion. Rare earth elements are separated from matrix concomitants and pzeconcentrated by canon exchange employing No. 1 resin. The analysis of the samples is performed on a Jarrell-Ash model 1160 Atom- Comp spectrometer with 60 channels. A DEC PDP 11/23 minicomputer controls the ICAP spectrometer and is interfaced to a LA-120 DECwriter for data reporting. A precision of 1-5.5%(RSD) was attained. Analyses of several hun- dreds of rock samples showed that the method is well suited to the routine simultaneous determination of 15 rare earth elements.
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