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离子色谱法检测土壤样品水溶态中的七种阴离子
引用本文:李庆霞,刘亚轩,陈卫明,肖细炼,张勤.离子色谱法检测土壤样品水溶态中的七种阴离子[J].物探与化探,2012,36(3):418-421.
作者姓名:李庆霞  刘亚轩  陈卫明  肖细炼  张勤
作者单位:中国地质科学院地球物理地球化学勘查研究所,河北廊坊,065000
基金项目:中央级公益性科研院所基本科研业务费专项资金资助(AS2009J06)
摘    要:采用离子色谱法测定土壤样品水溶态中的F^-、Cl^-、NO2^-、SO4^2-、Br^-、NO3^-、PO4^3-。通过优化提取条件,得出最优条件下7种阴离子的加标回收率为94.4%~102.5%,精密度为3.1%~4.6%。对实际样品进行测试,结果表明,该方法适用于土壤样品水溶态中7种阴离子的定性、定量分析。

关 键 词:离子色谱法  土壤样品测试  水溶态中阴离子

THE DETERMINATION OF SEVEN ANIONS IN WATER-EXTRACTABLE SOIL SAMPLES BY ION CHROMATOGRAPHY
LI Qing-xia , LIU Ya-xuan , CHEN Wei-ming , XIAO Xi-lian , ZHANG Qin.THE DETERMINATION OF SEVEN ANIONS IN WATER-EXTRACTABLE SOIL SAMPLES BY ION CHROMATOGRAPHY[J].Geophysical and Geochemical Exploration,2012,36(3):418-421.
Authors:LI Qing-xia  LIU Ya-xuan  CHEN Wei-ming  XIAO Xi-lian  ZHANG Qin
Institution:(Institute of Geophysical and Geochemical Exploration,Chinese Academy of Geological Sciences,Langfang 065000,China)
Abstract:The technology for determination of seven anions in water-extractable soil samples by ion chromatography was developed and the extraction conditions were optimized.Under the optimum condition,the recoveries of seven anions(F-,Cl-,NO-2,SO2-4,Br-,NO-3 and PO3-4) were 94.4%-102.5% and the precisions of seven anions were 3.1%-4.6%.The means has been applied to the determination of seven anions in water-extractable soil samples with satisfactory results.
Keywords:ion chromatography  soil sample analysis  anions of water-extractable state
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