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冷蒸气原子荧光法测量地球化学样品中痕量汞
引用本文:邢飞,杜淑兰.冷蒸气原子荧光法测量地球化学样品中痕量汞[J].吉林地质,2011,30(1):113-115,150.
作者姓名:邢飞  杜淑兰
作者单位:吉林省地质科学研究所,吉林,长春,130012
摘    要:用冷蒸气原子荧光法测量地球化学样品中痕量汞,对载气流量、试液酸度、硼氢化钾浓度等进行了试验。工作曲线线性范围为0~4μg/L,方法检出限为0.002 3μg/g,精密度RSD%为1.1~5.0。方法用国家一级地球化学标准物质中汞的测定,结果与标准值一致。

关 键 词:冷蒸气  原子荧光  地球化学样品  

Determination of trace mercury in geochemical samples by cold vapor atomic fluorescence spectrometry
XING Fei,DU Shu-lan.Determination of trace mercury in geochemical samples by cold vapor atomic fluorescence spectrometry[J].Jilin Geology,2011,30(1):113-115,150.
Authors:XING Fei  DU Shu-lan
Institution:XING Fei,DU Shu-lan Jilin Institute of Geological Sciences,Changchun 130012,Jilin,China
Abstract:A method for trace mercury in geochemical samples by cold vapor generation—atomic fluorescence spectrometry.The experimental conditions that carrying gas flow amount,Aqua Regina concentration and KBH4 concentration etc.The detection limit of the method for mercury is 0.023ug/L,linear scope is 0-4.0 ug/L,precision is 1.1-5.0(RSD%) for mercury.This method is demonstrated accurate and reliable through testing of standard samples.
Keywords:cold vapor generation  atomic fluorescence spectrometry  geochemical sample  mercury  
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