箕状断陷湖盆缓坡带层序地层格架内成岩特征研究——以东营凹陷南部缓坡带沙河街组为例

东营凹陷在沙河街组沉积期为北陡南缓的箕状断陷湖盆。通过钻井岩心、测井、薄片及扫描电镜分析,在断陷湖盆的南缓坡带古近系沙河街组中识别出了冲积扇、河流、三角洲和湖？白沉积体系,以及滨浅湖砂坝和缓坡远端浊积扇沉积相。建立了东营凹陷南部缓坡带层序地层格架及层序演化模式。在此基础上,详细研究了层序地层格架内的成岩作用特征。层序地层格架内主要成岩作用类型有压实作用、压溶作用、溶解作用等,成岩阶段为早成岩A、B期,晚成岩A、B期。层序地层格架内发育了碳酸盐胶结、石英次生加大、高岭石胶结和泥岩压实四种成岩相。     

连续运行GPS定位服务系统的探讨

介绍了连续运行GPS定位服务的概念、实现模式及其在测绘行业中的应用。     

GPS RTK校准检测试验场建设的研究

叙述了GPSRTK接收机校准检测试验场建设的方法,介绍了GPSRTK接收机校准检测的步骤,提出了GPSRTK校准检测的项目和结果判定方法,为未来的GPSRTK国家检定规程的出台做了有益地探索。     

Zircon M257 ‐ a Homogeneous Natural Reference Material for the Ion Microprobe U‐Pb Analysis of Zircon

We introduce and propose zircon M257 as a future reference material for the determination of zircon U‐Pb ages by means of secondary ion mass spectrometry. This light brownish, flawless, cut gemstone specimen from Sri Lanka weighed 5.14 g (25.7 carats). Zircon M257 has TIMS‐determined, mean isotopic ratios (2s uncertainties) of 0.09100 ± 0.00003 for ²⁰⁶pb/²³⁸U and 0.7392 ± 0.0003 for ²⁰⁷pb/²³⁵U. Its ²⁰⁶pb/²³⁸U age is 561.3 ± 0.3 Ma (unweighted mean, uncertainty quoted at the 95% confidence level); the U‐Pb system is concordant within uncertainty of decay constants. Zircon M257 contains ～ 840 μg g^?1 U (Th/U ～ 0.27). The material exhibits remarkably low heterogeneity, with a virtual absence of any internal textures even in cathodoluminescence images. The uniform, moderate degree of radiation damage (estimated from the expansion of unit‐cell parameters, broadening of Raman spectral parameters and density) corresponds well, within the “Sri Lankan trends”, with actinide concentrations, U‐Pb age, and the calculated alpha fluence of 1.66 × 10¹⁸ g^?1. This, and a (U+Th)/He age of 419 ± 9 Ma (2s), enables us to exclude any unusual thermal history or heat treatment, which could potentially have affected the retention of radiogenic Pb. The oxygen isotope ratio of this zircon is 13.9%o VSMOW suggesting a metamorphic genesis in a marble or calc‐silicate skarn.     

Composition-Induced Variations in SIMS Instrumental Mass Fractionation during Boron Isotope Ratio Measurements of Silicate Glasses

An analytical artefact is reported here related to differences in instrumental mass fractionation between NIST SRM glasses and natural geological glasses during SIMS boron isotope determinations. The data presented demonstrated an average 3.4‰ difference between the NIST glasses and natural basaltic to rhyolitic glasses mainly in terms of their sputtering-induced fractionation of boron isotopes. As no matrix effect was found among basaltic to rhyolitic glasses, instrumental mass fractionation of most natural glass samples can be corrected by using appropriate glass reference materials. In order to confirm the existence of the compositionally induced variations in boron SIMS instrumental mass bias, the observed offset in SIMS instrumental mass bias has been independently reproduced in two laboratories and the phenomenon has been found to be stable over a period of more than one year. This study highlights the need for a close match between the chemical composition of the reference material and the samples being investigated.     

Recommended Values of 239Pu, 240Pu and 239+240Pu Concentrations in Reference Material IAEA-315 (Marine Sediment) Estimated by Thermal Ionisation Mass Spectrometry, Inductively Coupled Plasma-Mass Spectrometry and Alpha Spectrometry

The recommended concentrations of ²³⁹Pu, ²⁴⁰Pu and ^239+240Pu in reference material IAEA‐315 (marine sediment) were estimated by three analytical methods: isotope dilution thermal ionisation mass spectrometry (TIMS), isotope dilution inductively coupled plasma‐mass spectrometry (ICP‐MS) and alpha spectrometry. The determination of ²³⁹Pu and ²⁴⁰Pu (^239+240Pu by alpha spectrometry) was carried out with samples from randomly selected bottles using each method. Plutonium‐238 was also measured by alpha spectrometry. A plutonium‐242 reference material was used as a spike for the quantitative analysis. The influence of ²⁴²Pu in the samples was therefore calculated; however, this contribution was less than the range of uncertainty and did not influence the final results. The obtained data were statistically analysed using variance component analysis and paired comparison. The combined standard uncertainties from “method/measurement”, “bottle” and “sub‐sample” were in the order of 3 to 6%. The main contributions to the uncertainty were from the material heterogeneity and from systematic differences between methods. Based on this study with twenty‐seven analyses using 10–14 g sample mass, concentrations of (38 ± 3) Bq kg^?1, (28 ± 3) Bq kg^?1 and (66 ± 4) Bq kg^?1 are proposed as recommended values for ²³⁹Pu, ²⁴⁰Pu and ^239+240Pu, respectively, and (9.5 ± 0.4) Bq kg^?1 for ²³⁸Pu as an information value in reference material IAEA‐315. In mass concentration units, these amount to (16.4 ± 1.2) ng kg^?1, (3.3 ± 0.4) ng kg^?1 and (0.015 ± 0.003) ng kg^?1 for ²³⁹Pu, ²⁴⁰Pu and ²³⁸Pu, respectively. The certified reference materials NIST 4350B and NIST 4354 were also analysed by TIMS for quality assurance of the method used in this study.     

自动化监测技术在我国首条大型电力隧道中的应用

通过自动化监测在超大工程项目中的应用,利用现有技术手段,对工程进行有效管理,逐渐将对工程的安全、预判起到越来越重要的作用,它可以在为工程节约大量资金情况下,提高预判安全施工的能力,是提高工程管理的重要手段。     

GGR Critical Review of Analytical Developments in 2004–2005

In 2005 Geostandards and Geoanalytical Research embarked upon a new initiative for its readers. Key researchers in various fields of geoanalytical technique development and their application were identified and invited to provide reviews pertinent to their expertise. As noted in the first of these publications "…instead of revisiting the historical context or decades of development in each analytical technique, the goal here has been to capture a snapshot of "hot topics" across a range of fields as represented in the… literature" (Hergt et al . 2005). Rather than prepare an annual review, a decision was taken earlier this year to provide a biennial summary of progress and accomplishments, in this case for the years 2004–2005. The principal techniques employed in Earth and environmental sciences are covered here, and include laser ablation and multicollector ICP-MS, ICP-AES, thermal ionisation and secondary ion mass spectrometry, as well as neutron activation analysis, X-ray fluorescence and atomic absorption spectrometry. A comprehensive review of the development of reference materials, often essential to these techniques, is also provided. The contributions assembled serve both to keep readers informed of advances they may be unfamiliar with, but also as a means of showcasing examples of the breadth and depth of work being conducted in these fields.     

Reference Materials in Geoanalytical Research -Review for 2004 and 2005

This review gives an overview of the use and development of reference materials of geochemical and environmental interest in the literature of the years 2004 and 2005. In these years the performance of existing methods has been improved and new geochemical applications using new techniques have been developed. Accordingly, there was an increasing need for new reference materials, especially for in situ microanalysis and for precise stable isotope measurements. In addition, there was a notable trend for further characterisation of existing reference materials, mainly for the platinum-group elements. This review focuses on five topics: reference materials for platinum-group elements, reference glasses for in situ microanalysis, zircon reference materials, isotopic reference materials, and the development and certification of reference materials.     

湿地功能快速评价中的若干理论问题

针对目前湿地功能快速评价中存在的不足之处,分析了产生这些不足的原因及湿地功能快速评价过程中存在的一些基本理论问题。分析表明:湿地功能快速评价方法是为了达到“湿地功能无净损失”目的,是在需要评价的湿地如此之多而从事湿地功能评价的专业人员又极其缺乏的情况下发展起来的。它对于湿地恢复与重建以及湿地受人类活动干扰程度的评价是非常有效的;在湿地功能快速评价过程中,把相对未受人类干扰的参照湿地的功能指数规定为1,这就使得快速评价方法不能对参照湿地的功能进行评价,而目前最需要评价其功能的湿地往往就是这些相对未受人类活动干扰的湿地;在相同水文地貌的湿地类型内评价湿地功能之间的差异,这使得快速评价方法不能评价湿地的水文地貌功能;由于快速评价的结果都是相对的功能指数,并不能说明湿地所提供的功能量是否满足人们的需求,因而在决策中不能单独使用;快速评价都是“一次调查就获得结果”,同时由于快速评价过程中指标选择的主观性、指标赋值的主观性、采样点空间设置的主观性以及采样时间的主观性,对于具有时空变化特征的湿地功能的评价结果的可重复性和科学性是很低的。为了使湿地功能评价的结果对管理和决策具有指导意义,基于湿地功能量计算的、定量的评价湿地功能的方法必须开发出来。针对不同的评价目的,湿地功能评价可采用双重参照标准:一是以自然为参照来评价湿地功能受人类活动影响的程度以及湿地恢复与重建成功与否;二是以人类需要为标准来评价湿地提供的功能量是否满足了我们的期望,以便采取措施改进湿地功能来满足人类的需求。