纤维素接枝丙烯酰胺/高岭土高吸水性复合材料研究

在高岭土的存在下，以N，N－亚甲基双丙烯酰胺作交联剂，以硝酸铈铵为引发剂微晶纤维素与丙烯酰胺进行接枝共聚反应，合成接枝纤维素／高岭土高吸水性复合材料。研究了纤维素与单体的配比、高岭土添加量、交联剂用量、引发剂用量及反应温度对吸水率的影响。用红外光谱表征复合材料的结构，用电子显微镜观察复合材料的表面与界面。结果表明，高岭土在接枝聚合物中能较好分散，复合材料吸水率达1166，对生理盐水溶液的吸水率达86。     

白云鄂博群中两个重要不整合界面特征及区域对比

白云鄂博群尖山组顶部的钙质风化壳和比鲁特组顶部的铁质风化壳分别代表长城系与蓟县系及蓟县系与青白口系的分界,并具较大区域上的一致性和可对比性。不整合界面的重新厘定,必然导致白云鄂博群的解体或改为白云鄂博超群。     

Fitness-for-Purpose of Reference Material Reference Values in Relation to Traceability of Measurement, as Illustrated by USGS BCR-1, NIST SRM 610 and IAEA NBS28

As in all fields of sample analysis, reference materials play a large role in supporting measurements in the geosciences. While a rather large number of materials are in distribution (> 380), not all are equally effective or fit-for-purpose in supporting laboratory data quality and thereby assuring the desired comparability of measurements between laboratories. Equally important, reference values that are not fit-for-purpose cannot be used effectively to establish traceability links between laboratory measurements and national and international standards. The needed fitness-for-purpose is not achieved for reference values either when more than one reference value has been proposed and a consensus does not exist among users as to which should be used by all, or when reference value uncertainties are too large in comparison to those of routine laboratory measurements. The focus of this review will be, first to outline the current reality, and second to suggest ways in which certifications of RMs can be improved to provide reference values that are universally accepted and more fit-for-purpose in general laboratory use. The discussion will be illustrated largely by current uses of USGS BCR-1, NIST SRM 610 and IAEA NBS28, as these three materials are those for which the largest body of newly published data exists, according to recent bibliographies of the geoanalytical literature published annually in Geostandards Newsletter: The Journal of Geostandards and Geoanalysis.     

Preparation of a New Geological Survey of Japan Geochemical Reference Material: Coral JCp-1

A new geochemical reference material, coral Porites sp. JCp-1 has been prepared by the Geological Survey of Japan (GSJ). Provisional values for twenty one major, minor and trace elements are presented. The homogeneity tests showed that all elements studied are considered to be homogeneously distributed.     

某地平板玻璃原料用石英砂的提纯研究

某地石英矿砂通过磁选分离法、稀酸浸泡法处理后，矿砂不同程度地降低了铁、铝、钙镁的含量；采用磁选分离 稀酸浸泡法联合处理后，使该地石英砂的化学成分达到了优质的生产平板玻璃用硅质原料的国家标准。     

压电双晶片双向大幅振动的探讨

通过压电陶瓷的逆压电效应对压电陶瓷双晶片在自动生产送料线上的应用研究，得出在二元系Ph(Ni1／3Nb2／3)O3-PhTiO3-PhZrO3的基础上作调整制作的压电双晶片。经运用在振动料斗上，作调频调幅控制。达到了压电双晶片振子结构，振子谐振频率为300Hz，当外加电压达300V时，振子偏转位移量大于1．7mm，故可作为一种理想的振动源。     

夏塞地区银、锡多金属矿成矿规律新认识

夏塞地区是西南三江(金沙江、澜仓江、怒江)地区东缘的一个重要成矿带，带内银、锡矿产责源十分丰富。本文认为其成矿物质来源于花岗岩体和地层，构造和岩体是区内的主要控矿因素，地壳演化与成矿作用关系十分密切，矿床类型为分布于岩体内接触带的矽卡岩型矿床和分布于岩体外接触带的热液型矿床。     

兰坪白秧坪铜银多金属矿床成矿物质来源的铅和硫同位素示踪

白秧坪铜银多金属矿床主要产于白垩系下统景星组石英砂岩、粉砂岩中，矿石铅同位素组成特征与景星组砂岩的铅同位素组成比较接近，表明壳源物质参与了成矿作用。作ZartMan图解和△γ—△β图解表明，矿石铅属于壳幔混合来源。矿石铅μ值介于9．43—9．65之间，Th/U比值介于3．72—3．87之间，表明矿石铅为壳幔混合铅。该矿床硫同位素组成表明，硫来源于深部地幔硫遭受地壳硫的混入。该矿床的成矿作用发生于开放体系之中，成矿物质来源为深部幔源物质混合了壳源物质。     

地球深部物质的某些物性测量方法研究

文中介绍了地球深部物质实验室近 2 0年来开展高温高压下地球深部物质物性实验研究过程中 ,在测量方法方面的进步和应用情况。这些测量方法包括了高温、高压下弹性的超声测量方法、高温高压下电性的测量方法、高压差热分析法和高压下热学Gr櫣ｎｅｉｓｅｎ参数的测量方法诟呶赂哐瓜卵沂涂笪锏牡猿饬恐?,我们由超声脉冲透射方法改进为超声脉冲透射反射法 ,克服了样品室中压力和温度梯度对样品的影响。在高温高压下岩石和矿物的电学性质测量中 ,我们由直流法发展为阻抗谱法 ,不仅克服了样品极化对测量结果的影响 ,还可以获得离子在溶液中的多种物理化学参数 ,以及监测含水矿物在高温高压下的脱水动力学特征。在固体传压介质中建立的高压热学Gr櫣ｎｅｉｓｅｎ参数的测量方法 ,由于升压速率比较小且叶蜡石在高压下的热导系数增大 ,其测量结果需要进行校正 ,其测量方法有待进一步改进。     

添加剂对土体的加固作用及冻胀防治研究

将研制的高分子有机材料作为添加剂，加入到土体中，经过拌和夯实、干燥固结，能够起到稳定和提高土体的强度，并具有低渗透和低吸水等特性．冻胀试验表明：加入添加剂不仅能阻止土体冻胀的产生、外来水源的入侵及水分的迁移，还能隔断土体孔隙之间的联系，使水分在土体孔隙中不能运移，从而达到了防治冻胀的目的。