Enzymatic synthesis of methyl-galactoaldehyde

Methyl-galactosides were oxidized at room temperature by galactose oxidase in a one-step reaction and afforded methyl-galactoaldehyde in excellent yield and high purity. The resulting galactoaldehyde as a useful intermediate can be directly used in glycopeptide synthesis.     

长江上游洪涝暴雨环流形势中期演变趋势分析

本文通过对1980年以来长江上游10次洪涝过程的500hpa环流形势分析,并用车比雪夫多项式对500hpa高度场进行展开,研究了各类洪涝过程的中期演变特征,发现代表不同洪涝过程环流形势变化的不同的车氏系数值都有明显的特征变化,结合欧洲中心中期数值预告96小时500hpa高度场的车氏系数分析,可为洪涝暴雨的中期预报提供一种新的思路。     

基于SAR干涉点目标分析技术的城市地表形变监测

通过深入研究干涉点目标的相位模型,提出基于空间搜索的邻近点目标干涉相位差解缠方法,用以计算点目标的地形残差和线性形变,以及分离点目标大气延迟相位和非线性形变相位的时空域滤波方法,解决干涉点目标分析中的关键问题.最后,以苏州地区地表沉降监测为应用试验,利用形成的SAR干涉点目标形变信息提取技术,获取苏州市区1992-2002年间的地表沉降信息.研究结果与已有文献记录保持比较好的一致性,证明SAR干涉点目标技术完全可以发展成为应用于城市地表形变监测的实用化技术.

Abstract：

Interferometric point target analysis (IPTA) is one of the latest developments in radar interferometric processing. It is achieved by analysis of the interferometric phases of some individual point targets, which are discrete and present temporarily stable backscattering characteristics, in long temporal series of interferometric SAR images. This paper analyzes the interferometric phase model of point targets, and then addresses two key issues within IPTA process. Firstly, a spatial searching method is proposed to unwrap the interferometric phase difference between two neighboring point targets. The height residual error and linear deformation rate of each point target can then be calculated, when a global reference point with known height correction and deformation history is chosen. Secondly, a spatial-temporal filtering scheme is proposed to further separate the atmosphere phase and nonlinear deformation phase from the residual interferometric phase. Finally, an experiment of the developed IPTA methodology is conducted over Suzhou urban area. Totally 38 ERS-1/2 SAR scenes are analyzed, and the deformation information over 3 546 point targets in the time span of 1992-2002 are generated. The IPTA-derivecl deformation shows very good agreement with the published result, which demonstrates that the IPTA technique can be developed into an operational tool to map the ground subsidence over urban area.     

空间信息网络服务中的数据安全策愀

以地理信息网络服务的安全策略为研究对象，根据我国空间数据生产到应用整个流程保密管理规定，研究地理空间数据在存储、分发、传输、表现以及与其他系统集成应用阶段上的安全策略，解决地理空间数据共享与空间数据安全之间的矛盾。     

基于直线感知增强的边缘提取算法

根据视觉识别边缘的感知特性,提出了一种基于直线感知增强的弱边缘的边缘提取算法。借鉴视觉的直线感知方式,针对弱边缘整体上呈直线分布的特点将其筛选出来,进行编组、连接和扩展。与Edison边缘提取算子的比较实验证明,本算法在对弱边缘的提取和虚假边缘的抑制上有显著增强。     

Evolution of Electric Currents Associated with Two M-Class Flares

Using one-minute cadence vector magnetograms from Big Bear Solar Observatory (BBSO), we analyze the temporal behavior of derived longitudinal electric currents associated with two flares on July 26, 2002. One of the events is an M1.0 flare which occurred in active region NOAA 10044, while the other is an M8.7 flare in the adjacent region 10039. Rapid changes of magnetic fields in the form of flux emergence are found to be associated with both of these events. However, the temporal behavior of electric currents are very different. For the M1.0 flare, the longitudinal electric current density drops rapidly near the flaring neutral line; while for the M8.7 flare, the current density rapidly increases, confirming the picture of the current-carrying flux emergence. We offer a possible explanation for such a difference: magnetic reconnection at different heights for the two events, near the photosphere for the M1.0 flare, and higher up for the M8.7 flare.     

邻菲啰啉在测定亚铁中的保护效果

样品在分解过程中 ,亚铁易被空气部分氧化 ,致使测试结果偏低 ,采用在HF H2 SO4溶矿过程中加入邻菲卟罗啉 ,与亚铁形成络合物 ,对保护亚铁具有较好的效果。拟定了在塑料坩埚中加邻菲卟罗啉、H2 SO4及HF ,中高温电热板溶矿 ,容量法测定样品中的亚铁 ,方法精密度为 0 .2 3% ,样品加标准回收率 98.8%～ 10 1.9%。此方法具有较好的应用效果     

有关边界层问题中一类奇异积分方程新的存在性结果

对边界层理论新结果中出现的一类奇异积分方程w（t）=∫1 t（1-s）（λ＋λs＋s）/w（s）ds＋（1-t）∫t 0s/w（s）ds,t∈（0,1）进行讨论，并得出了上述方程在λ∈（-1/2,0）上正解存在性的新结果。     

三维旋转扫描测量平台设计与实现

本设计主要用于360°旋转的三维扫描,实现角度数据的实时获取。设计中采用单片机控制交流伺服电机进行自定的角度、速度与方向的旋转并实时上传时间、角度数据至上位机进行处理,实现了对平台旋转精度的控制与检测,着重研究了该传感器误差源的产生,对实际应用中的误差进行了定量分析,利用偏心改正、4分频等方法减少了误差,提高了参数精度。角度范围为360°,角度分辨率为0.01°。