Characterisation of brown coal humic acids and modified humic acids using pyrolysis gcms and other techniques

It has been proposed that Victorian brown coal can be considered as a two-component structure — a lignocellulosic “host”, containing various amounts of weakly bound or entrapped “guest” material together with very small amounts of inorganic and/or mineral matter. The latter predominantly consists of wax esters and/or terpenoid material. In this paper we describe attempts to gain structural information regarding the more complex, “host” component of the coal. Our initial model compound has been humic acid that can be readily obtained from the coal by alkaline extraction. It has been found that “pure” humic acid, free from material associated with the “guest” components of the coal, can be obtained by a highly selective, low-yielding alkaline extraction. This humic acid has been studied by nmr spectroscopy and pyrolysis gas chromatography-mass spectroscopy (py-gc/ms). The products arising from py-gc/ms have been compared with those obtained from similar pyrolysis of whole coals. Alkylation of humic acids using alkyl halides in the presence of base has been successfully carried out and reactivity of the resulting materials compared with those of the parent coal and humic acid.     

MD－50型钻机液压系统的设计

介绍了ＭＤ－５０型钻机液压系统的设计原理和主要液压元件的选择依据，并通过对设计和实践的总结，谈了作者在全液压钻机液压系统设计中的一些体会。     

南天山蛇绿混杂岩和中天山南缘糜棱岩的40Ar/39Ar年龄及其大地构造意义

⁴⁰Ar/³⁹Ar同位素年龄测定,获得南天山蛇绿混杂岩基质黑云母石英片岩单矿物黑云母的两个坪年龄分别为(370.0±4.8)Ma和(259.0±3.3)Ma;中天山南缘长英质糜棱岩单矿物黑云母的坪年龄为(250.5±7.9)Ma,二云母花岗岩单矿物白云母的坪年龄为(348.9±0.3)Ma。结合南天山古生代沉积特征和塔里木及伊犁-哈萨克斯坦板块古地磁数据的综合分析,提出南天山晚泥盆世至石炭纪早期完成向伊犁-哈萨克斯坦板块的B型俯冲,中-晚二叠世进行陆内A型俯冲造山的板块碰撞演化模式。     

三种锰硅酸盐矿物的鉴别及其研究意义

蜡硅锰矿，粒硅锰矿，鉴别，研究意义     

泡沫泥浆钻进工艺及护壁堵漏机理研究

介绍了所研制的ＤＦ－１型泡沫剂组分及性能；对泡沫泥浆钻进的配方进行了研究，得出的最优配方应用于现场，取得了较好的效果，并对泡沫泥浆的护壁机理进行了研究。     

桩长及水泥掺入量对柔性桩承载力等的影响

采用弹性无限半空间体内的Mindlin应力解和分层总和法，计算分析了柔性桩的荷载传递规律，较详细地讨论了桩长、固化剂（水泥）掺入量对柔性桩复合地基承载力、变形的影响。计算值与实测值比较吻合。     

中强震与江苏新沂地震台地电阻率异常的关系研究

运用速率法、滑动富氏法对江苏省新沂地震台1990年至1999年地电阻率观测资料进行了分析，研究了电阻率异常与江苏省及其邻近地区的中强震的关系。结果表明．从1994年到1997年之间发生的中强震，新沂地震台地电阻率3个测向有不同程度的异常与之对应。研究结果表明．资料异常呈现出的各向异性和其对应性与地球自转加速年份、孕震期的应力状态、震区构造、介质结栖有关。     

多尺度分解在地震信号处理中的应用

利用小波分析中的多尺度分解及信号消噪技术，对记录不清、信噪比小、震相无法辨认的地震信号进行处理。结果表明：多尺度分解在弱震信号提取和弱震相的识别等方面有很好的效果。     

多相地貌单元场地勘察中基岩与卵砾石、孤石的鉴别

在多相地貌单元场地勘察中，基岩与卵砾石的鉴别难度较大。应利用初步感性认识、钻进状态、岩样特征等多手段对基岩与卵砾石进行判别，以提高判别率。     

Age of Yingfeng rapakivi granite pluton on the north flank of Qaidam and its geological significance

Rapakivi granite is a very rare and special type of rocks in the crust. Nearly all the typical Proterozoic rapakivi occurred in stable craton, and was regarded as representing special anorogenic settings and rifting events of the supercontinents. Therefore, rapakivi has constantly been attracting the attention of researchers from various countries[15]. For example, the Protero- zoic rapakivi granites occurring in Miyun, Beijing, has been studied in detail by the researchers both at home and …