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电感耦合等离子体质谱法同时测定地下水中硼溴碘 总被引:6,自引:4,他引:2
建立了电感耦合等离子体质谱法同时测定地下水中B、Br、I的方法。选定φ=2%(体积分数)的稀NH3.H2O介质消除碘的记忆效应。采用干扰较少的10B和79Br同位素。B、Br、I在0~10 000 ng/mL呈良好的线性关系。方法的检出限为10B 0.176 ng/mL,79Br 0.876ng/mL,127I 0.132 ng/mL;精密度(RSD,n=12)为10B 2.86%,79Br 3.36%,127I 2.69%;10B的阶梯加标回收率为94.6%~101.5%,79Br为98.3%~104.9%,127I为96.5%~102.0%。 相似文献
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赣南崇义县淘锡坑钨矿位于南岭东西向构造带东段,属于以黑钨矿石英脉型为主的钨多金属矿床。矿床形成与燕山期中酸性岩浆作用有密切关系,石英矿脉受一组北西向断裂控制,穿切新元古界。本文在淘锡坑钨矿区3个揭露到花岗岩体顶部的中段(206、106、56中段)采集到岩体顶部云英岩样品,利用40Ar/39Ar同位素定年测得云英岩中的白云母的坪年龄分别为152.7 ± 1.5 Ma(206中段),153.4 ± 1.3 Ma(106中段),155.0 ± 1.4 Ma(56中段)。与前人用其他方法测定的花岗岩成岩和成矿年龄几乎一致。花岗岩和云英岩全岩稀土元素均具有M型四分组效应和强烈的Eu亏损特征,反映出花岗质岩浆经历了高度分异演化及其岩体结晶晚期流体/熔体相互作用。综合前人在南岭地区同类矿床的研究资料,可知南岭地区160~150Ma成岩成矿作用主要分布于南岭中-东段,可能为大陆边缘弧后岩石圈伸展的构造动力学背景的产物。 相似文献
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西天山达巴特矿区火山岩的形成时代、构造背景及对斑岩型矿化的制约 总被引:9,自引:0,他引:9
本文通过对西天山地区比较典型的达巴特斑岩铜钼矿床矿区范围内出露的英安岩和花岗斑岩进行了系统的岩石地球化学分析,对流纹斑岩和花岗斑岩中的锆石进行了SHRIMPU—Pb定年研究,分别获得了315.9±5.9Ma和278.7±5.7Ma。岩石化学、微量以及稀土元素特征表明从英安岩到花岗斑岩,岩体具有明显的分异演化特征和很好的继承性。火山岩和次火山岩的精确定年为准确厘定火山岩形成的时限和地球动力学背景提供了依据。结合已有的Re-Os法获得的矿化年龄,表明晚石炭世末-早二叠世初(278.7±5.7Ma),西天山地区进入板块碰撞-板内伸展阶段,由于深源岩浆侵位,在达巴特矿区形成了由花岗斑岩、流纹斑岩和流纹质角砾熔结凝灰岩组成的椭圆形火山机构,并导致相关矿床的形成。 相似文献
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Min Sun Chao Yuan Wenjiao Xiao Xiaoping Long Xiaoping Xia Guochun Zhao Shoufa Lin Fuyuan Wu A. Kröner 《Chemical Geology》2008,247(3-4):352-383
Gneissic rocks in the Chinese Altai Mountains have been interpreted as either Paleozoic metasedimentary rocks or Precambrian basement. This study reports geochemical and geochronological data for banded paragneisses and associated gneissic granitoids collected along a NE–SW traverse in the northwestern Chinese Altai. Petrological and geochemical data suggest that the protoliths of the banded gneisses were possibly immature sediments with significant volcanic input and that the gneissic granitoids were derived from I-type granites formed in a subduction environment. Three types of morphological features can be recognized in zircons from the banded gneisses and are interpreted to correlate with different sources. Zircons from five samples of banded paragneiss cluster predominantly between 466 and 528 Ma, some give Neoproterozoic ages, and a few yield discordant Paleoproterozoic to Archean ages. Zircon Hf isotopic compositions indicate that both juvenile/mantle and crust materials were involved in the generation of the source rocks from which these zircons were derived. In contrast, zircons occur ubiquitously as elongated euhedral prismatic crystals in the four samples of the gneissic granitoids, and define single populations for each sample with mean ages between 380 and 453 Ma. The general absence of Precambrian inheritance and positive zircon ?Hf values for these granitoids suggest insignificant crustal contribution to the generation of the precursor magmas. Our data can be interpreted in terms of a progressive accretionary history in early to middle Palaeozoic times, and the Chinese Altai may possibly represent a magmatic arc built on a continental margin dominated by Neoproterozoic rocks. 相似文献
50.
Hong-Fu Zhang Steven L. Goldstein Xin-Hua Zhou Min Sun Jian-Ping Zheng Yue Cai 《Contributions to Mineralogy and Petrology》2008,155(3):271-293
The ages of subcontinental lithospheric mantle beneath the North China and South China cratons are less well-constrained than
the overlying crust. We report Re–Os isotope systematics of mantle xenoliths entrained in Paleozoic kimberlites and Mesozoic
basalts from eastern China. Peridotite xenoliths from the Fuxian and Mengyin Paleozoic diamondiferous kimberlites in the North
China Craton give Archean Re depletion ages of 2.6–3.2 Ga and melt depletion ages of 2.9–3.4 Ga. No obvious differences in
Re and Os abundances, Os isotopic ratios and model ages are observed between spinel-facies and garnet-facies peridotites from
both kimberlite localities. The Re–Os isotopic data, together with the PGE concentrations, demonstrate that beneath the Archean
continental crust of the eastern North China Craton, Archean lithospheric mantle of spinel- to diamond-facies existed without
apparent compositional stratification during the Paleozoic. The Mesozoic and Cenozoic basalt-borne peridotite and pyroxenite
xenoliths, on the other hand, show geochemical features indicating metasomatic enrichment, along with a large range of the
Re–Os isotopic model ages from Proterozoic to Phanerozoic. These features indicate that lithospheric transformation or refertilization
through melt-peridotite interaction could be the primary mechanism for compositional changes during the Phanerozoic, rather
than delamination or thermal-mechanical erosion, despite the potential of these latter processes to play an important role
for the loss of garnet-facies mantle. A fresh garnet lherzolite xenolith from the Yangtze Block has a Re depletion age of
∼1.04 Ga, much younger than overlying Archean crustal rocks but the same Re depletion ages as spinel lherzolite xenoliths
from adjacent Mesozoic basalts, indicating Neoproterozoic resetting of the Re–Os system in the South China Craton. 相似文献