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71.
Chemical Separation and Isotopic Variations of Cu and Zn From Five Geological Reference Materials 总被引:6,自引:0,他引:6
John B. Chapman Thomas F.D. Mason Dominik J. Weiss Barry J. Coles Jamie J. Wilkinson 《Geostandards and Geoanalytical Research》2006,30(1):5-16
This paper presents an adapted anion exchange column chemistry protocol which allowed separation of high-purity fractions of Cu and Zn from geological materials. Isobaric and non-spectral interferences were virtually eliminated for consequent multiple-collector ICP-MS analysis of the isotopic composition of these metals. The procedure achieved ∼ 100% recoveries, thus ensuring the absence of column-induced isotopic fractionation. By employing these techniques, we report isotopic analyses for Cu and Zn from five geological reference materials: BCR-027 blende ore (BCR), δ65 Cu = 0.52 ± 0.15‰ (n = 10) and δ66 Zn = 0.33 ± 0.07‰ (n = 8); BCR-030 calcined calamine ore (BCR), δ66 Zn = -0.06 ± 0.09‰ (n = 8); BCR-1 basalt (USGS), δ66 Zn = 0.29 ± 0.12‰ (n = 8); NOD-P-1 manganese nodule (USGS), δ65 Cu = 0.46 ± 0.08‰ (n = 10) and δ66 Zn = 0.78 ± 0.09‰ (n = 9); SU-1 Cu-Co ore (CCRMP), δ65 Cu = -0.018 ± 0.08‰ (n = 10) and δ66 Zn = 0.13 ± 0.17‰ (n = 6). All uncertainties are ± 2s; copper isotope ratios are reported relative to NIST SRM-976, and zinc isotope ratios relative to the Lyon-group Johnson Matthey metal (batch 3-0749 L) solution, JMC Zn. These values agree well with the limited data previously published, and with results reported for similar natural sample types. Samples were measured using a GVi IsoProbe MC-ICP-MS, based at the Natural History Museum, London. Long-term measurement reproducibility has been assessed by repeat analyses of both single element and complex matrix samples, and was commonly better than ± 0.07‰ for both δ66 Zn and δ65 Cu. 相似文献
72.
Traces of historical tropical cyclones and tsunamis in the Ashburton Delta (north‐west Australia) 下载免费PDF全文
Simon Matthias May Dominik Brill Max Engel Anja Scheffers Anna Pint Stephan Opitz Volker Wennrich Peter Squire Dieter Kelletat Helmut Brückner 《Sedimentology》2015,62(6):1546-1572
Although the north‐western coast of Western Australia is highly vulnerable to tropical cyclones and tsunamis, little is known about the geological imprint of historic and prehistoric extreme wave events in this particular area. Despite a number of site‐specific difficulties such as post‐depositional changes and the preservation potential of event deposits, both tropical cyclones and tsunamis may be inferred from the geomorphology and the stratigraphy of beach ridge sequences, washover fans and coastal lagoons or marshes. A further challenge is the differentiation between tsunami and storm deposits in the geological record, particularly where modern deposits and/or historical reports on the event are not available. This study presents a high‐resolution sedimentary record of washover events from the Ashburton River delta (Western Australia) spanning approximately the last 150 years. A detailed characterization of event deposits is provided, and a robust chronostratigraphy for the investigated washover sequence is established based on multi‐proxy sediment analyses and optically stimulated luminescence dating. Combining sedimentological, geochemical and high‐resolution optically stimulated luminescence data, event layers are assigned to known historical events and tropical cyclone deposits are separated from tsunami deposits. For the first time, the 1883 Krakatoa and 1977 Sumba tsunamis are inferred from sedimentary records of the north‐western part of Western Australia. It is demonstrated that optically stimulated luminescence applied in coastal sedimentary archives with favourable luminescence characteristics can provide accurate chronostratigraphies even on a decadal timescale. The results contribute to the data pool of tropical cyclone and tsunami deposits in Holocene stratigraphies; however, they also demonstrate how short‐lived sediment archives may be in dynamic sedimentary environments. 相似文献
73.
Human thermal perception is best described through thermal indices. The most popular thermal indices applied in human bioclimatology are the perceived temperature (PT), the Universal Thermal Climate Index (UTCI), and the physiologically equivalent temperature (PET). They are analysed focusing on their sensitivity to single meteorological input parameters under the hot and windy meteorological conditions observed in Doha, Qatar. It can be noted, that the results for the three indices are distributed quite differently. Furthermore, they respond quite differently to modifications in the input conditions. All of them show particular limitations and shortcomings that have to be considered and discussed. While the results for PT are unevenly distributed, UTCI shows limitations concerning the input data accepted. PET seems to respond insufficiently to changes in vapour pressure. The indices should therefore be improved to be valid for several kinds of climates. 相似文献
74.
75.
Evolution of the Upper Rhone River discharge and suspended sediment load during the last 80 years and some implications for Lake Geneva 总被引:1,自引:0,他引:1
76.
Peat soils are heterogeneous, anisotropic porous media. Compared to mineral soils, there is still limited understanding of physical and solute transport properties of fen peat soils. In this study, we aimed to explore the effect of soil anisotropy on solute transport in degraded fen peat. Undisturbed soil cores, taken in vertical and horizontal direction, were collected from one drained and one restored fen peatland both in a comparable state of soil degradation. Saturated hydraulic conductivity (K s) and chemical properties of peat were determined for all soil cores. Miscible displacement experiments were conducted under saturated steady state conditions using potassium bromide as a conservative tracer. The results showed that (1) the K s in vertical direction (K sv) was significantly higher than that in horizontal direction (Ksh), indicating that K s of degraded fen peat behaves anisotropically; (2) pronounced preferential flow occurred in vertical direction with a higher immobile water fraction and a higher pore water velocity; (3) the 5% arrival time (a proxy for the strength of preferential flow) was affected by soil anisotropy as well as study site. A strong correlation was found between 5% arrival time and dispersivity, K s and mobile water fraction; (4) phosphate release was observed from drained peat only. The impact of soil heterogeneity on phosphate leaching was more pronounced than soil anisotropy. The soil core with the strongest preferential flow released the highest amount of phosphate. We conclude that soil anisotropy is crucial in peatland hydrology but additional research is required to fully understand anisotropy effects on solute transport. 相似文献
77.
Sebastian Kowalczyk Kornelia Anna Żukowska Maciej Jan Mendecki Dominik Łukasiak 《Acta Geophysica》2017,65(1):223-235
Complex studies were carried out to recognize the fen structure and peat properties in the Ca?owanie Fen area, belonging to the Natura 2000 network. The studies were conducted in two study areas that differ significantly in terms of peat thickness. Electrical resistivity imaging (ERI) was used to identify the properties of the peat and its substrate, such as thickness and electrical resistivity. Comparison of the field studies with the laboratory tests has shown that the ash content rises electrical resistivity in peat. In addition, the study has shown that the application of non-invasive geophysical methods in protected areas is justified. The fen, as a medium containing mostly water, was a proper test area for the ERI measurements. 相似文献
78.
79.
Ingo Leya Jean‐Christophe David Thomas Faestermann Michaela Froehlich Niko Kivel Dominik Koll Gunther Korschinek Sarah McIntyre Silke Merchel Stefan Pavetich Georg Rugel Dorothea Schumann Thomas Smith Anton Wallner 《Meteoritics & planetary science》2020,55(4):818-831
We measured specific activities of the long‐lived cosmogenic radionuclides 60Fe in 28 iron meteorites and 53Mn in 41 iron meteorites. Accelerator mass spectrometry was applied at the 14 MV Heavy Ion Accelerator Facility at ANU Canberra for all samples except for two which were measured at the Maier‐Leibnitz Laboratory, Munich. For the large iron meteorite Twannberg (IIG), we measured six samples for 53Mn. This work doubles the number of existing individual 60Fe data and quadruples the number of iron meteorites studied for 60Fe. We also significantly extended the entire 53Mn database for iron meteorites. The 53Mn data for the iron meteorite Twannberg vary by more than a factor of 30, indicating a significant shielding dependency. In addition, we performed new model calculations for the production of 60Fe and 53Mn in iron meteorites. While the new model is based on the same particle spectra as the earlier model, we no longer use experimental cross sections but instead use cross sections that were calculated using the latest version of the nuclear model code INCL. The new model predictions differ substantially from results obtained with the previous model. Predictions for the 60Fe activity concentrations are about a factor of 2 higher, for 53Mn, they are ~30% lower, compared to the earlier model, which gives now a better agreement with the experimental data. 相似文献
80.
Andrei A. Andreev Lyudmila S. Shumilovskikh Larisa A. Savelieva Raphael Gromig Grigory B. Fedorov Anna Ludikova Bernd Wagner Volker Wennrich Dominik Brill Martin Melles 《Boreas: An International Journal of Quaternary Research》2019,48(2):377-386
Lake Ladoga hosts preglacial sediments, although the Eurasian ice sheet overrode the area during the LGM. These sediments were first discovered by a seismic survey and are investigated using a 22.75‐m‐long core. Its upper 13.30 m comprise Holocene and Lateglacial sediments separated from the lower 11.45 m of preglacial sediments by a hiatus. They consist of highly terrigenous lacustrine sediments, which according to OSL dating, were deposited during an early stage of the last ice age (MIS 5). The palynological data allow a first reconstruction of the Early Weichselian environmental history for northwestern Russia. Birch and alder forests with broad‐leaved taxa dominated during MIS 5d (c. 118–113 ka), suggesting a climate more favourable than in the Holocene. A high content of well‐sorted sands and poorly preserved palynomorphs indicates a shallow‐water environment at least temporarily. More fine‐grained sediments and better preserved organic remains suggest deeper water environments at the core location during MIS 5c (c. 113–88 ka). Pine and spruce became dominant, while broad‐leaved taxa started to disappear, especially after c. 90 ka, pointing to a gradual climate cooling. An increase in open herb‐dominated habitats at the beginning of MIS 5b (c. 88–86 ka) reflects a colder and dryer climate. However, later (c. 86–82 ka) pine and spruce again became more common. Birch and alder forests dominated in the area c. 82–80 ka (beginning of MIS 5a). Although open treeless habitats also became more common at this time, a slight increase in hazel may point to somewhat warmer climate conditions coinciding with the beginning of MIS 5a. The studied sediments also contain numerous remains of freshwater algae and cysts of marine and brackish‐water dinoflagellates and acritarchs documenting that the present lake basin was part of a brackish‐water basin during the Early Weichselian, probably as a gulf of the Pre‐Baltic Sea. 相似文献