青藏高原拉萨地体南部林芝岩群的物质来源与形成年代：岩石学与锆石U-Pb年代学

本文对位于青藏高原拉萨地体东南部林芝岩群中的变质岩进行了岩石学和年代学研究。研究表明,林芝岩群由角闪岩相的变质沉积岩和正片麻岩组成。变质沉积岩主要为含石榴石白云斜长角闪片岩、含石榴石云母石英片岩、含石榴石黑云钾长片麻岩、大理岩和石英岩等,代表性矿物组合包括石榴石+斜长石+角闪石+石英+黑云母+白云母,或石榴石+斜长石+钾长石+石英+夕线石+黑云母+白云母。花岗质片麻岩（含二云母片麻岩）的矿物组合是石英+斜长石+钾长石+黑云母+白云母。锆石U-Pb年代学分析表明,变质沉积岩中的碎屑锆石主要为岩浆成因,获得了2708~63Ma的²⁰⁶Pb/²³⁸U年龄范围,在~1100Ma和~550Ma出现两个年代峰值。碎屑锆石的变质增生边给出了35Ma的变质年龄。正片麻岩获得了496Ma的锆石结晶年龄和1158Ma的继承年龄。基于上述研究结果、区域对比和相邻变质岩石中获得的多期变质年龄,我们认为林芝岩群的原岩很可能形成在早古生代,其沉积物质主要来源于印度陆块,与特提斯喜马拉雅早古生代的岩石一起同为印度大陆北缘的沉积盖层,在环冈瓦纳大陆周缘造山过程中被寒武纪花岗岩侵入。在新特提斯洋向北的俯冲过程中,林芝岩群经历了晚中生代的安第斯型造山作用,在印度与欧亚大陆的俯冲-碰撞过程中,林芝岩群部分地经历了新生代的变质和岩浆作用再造。本研究证明,林芝岩群并不是传统上认为的拉萨地体的前寒武纪变质基底,其角闪岩相至麻粒岩相变质作用发生在中、新生代。     

大别山石马地区超高压变质岩角闪岩相变形的Rb-Sr同位素年龄及其构造意义

角闪岩相变形是大别山超高压变质岩的主期变形 ,露头和显微尺度的构造要素主要由这期变形产生 ,通过对超高压变质岩带内韧性剪切带中花岗片麻岩的Rb -Sr同位素年龄测定 ,获得一条变形花岗片麻岩的全岩 -白云母内部等时线年龄 ,表明超高压变质岩的角闪岩相变形产生于180Ma左右 ,超高压变质岩的主期变形确实为同角闪岩相变质期变形 ,该年龄与超高压变质岩的第二次快速冷却年龄一致 ,由此证实超高压变质岩在180Ma左右快速从下地壳折返至中地壳     

滇西南那邦变质基性岩两期变质作用的40Ar/39Ar年代学研究

中缅边界那邦变质基性岩出露于东缅著名的 Mogok带的东缘。那邦基性麻粒岩经历了早期麻粒岩相、晚期角闪岩相的两期变质作用的改造。早期变质作用的矿物石榴石和单斜辉石的 40 Ar/ 39Ar激光微区等时线年龄是 74.44± 1.44 Ma;石榴石和单斜辉石的 40 Ar/ 39Ar年龄谱图和等时线年龄均显示两组年龄 :74～ 76 Ma和 2 3～ 2 4Ma。晚期变质作用矿物角闪石的K- Ar法得出 2 3Ma,角闪石和斜长石的 40 Ar/ 39Ar年龄谱图和等时线年龄均显示 2 3～ 2 4Ma的变质年龄。综合这些结果 ,可以确定那邦基性麻粒岩的早期麻粒岩相变质作用的年龄是 74～ 77Ma,可能与新特提斯洋壳俯冲事件有关 ;晚期角闪岩相变质作用的年龄是 2 3～ 2 4Ma,与区内喜山期以来陆内块体响应两大陆会聚作用发生的大型走滑事件有关。那邦基性麻粒岩是世界上最年轻的麻粒岩相岩石之一 ,而且 ,两期变质作用年龄的确定对揭示区内与变质作用相关的地质事件具有重要意义。     

大别山含柯石英榴辉岩区—一个晚太古代的超高压变质带

安徽碧溪岭岩体的锆石U-Pb年龄为2774±24Ma。它显示大别山的含柯石英榴辉岩可能形成于晚太古代。榴辉岩多硅白云母的Ar-Ar等时线年龄(662±13Ma)也同样限定其退变质作用的上界年龄在寒武纪。同位素年代学结果与该类榴辉岩严格产出在由大别群组成的太古宙地块中的地质特征一致。我们相信,大别山含柯石英榴辉岩变质地区可能是一个晚太古代的超高压变质带。大别山地区在中生代三叠纪时期处于南秦岭构造带的东延部分。大别群以及赋存其中的含柯石英榴辉岩共同遭受晚期的区域动力变质事件。作者分别测得斜长片麻岩白云母Ar-Ar等时线年龄为192.6±3.8Ma,榴辉岩中低角闪岩相普通角闪石Ar-Ar坪年龄230.7±4.6Ma。它们代表大别群片麻岩和榴辉岩两种原始变质岩的印支期改造年龄。     

大别山双河超高压变质矿物Ｏ同位素平衡及其对Sm-Nd和Rb-Sr等时线年龄有效性的制约

对大别造山带双河超高压榴辉岩和片麻岩Sm-Nd和Rb-Sr等时线矿物进行了O同位素地质测温。尽管Sm-Nd等时线给出一致的三叠纪年龄(213~238 Ma)，同一样品Rb-Sr等时线却给出侏罗纪年龄(171~174 Ma)。片麻岩、榴辉岩和榴闪岩矿物对O同位素测温得到600~720℃和420~550℃两组温度，分别对应于约225±5 Ma榴辉岩相变质和约175±5 Ma角闪岩相退变质条件下停止同位素扩散交换的温度。同一样品三叠纪Sm-Nd等时线年龄的保存、侏罗纪Rb-Sr等时线年龄的出现以及有规律的O同位素温度，表明在角闪岩相退变质过程中，Sr和O在含水矿物（如黑云母和角闪石）中的扩散速率在手标本尺度上比石榴石Nd和多硅白云母Sr的扩散速率快。     

吉林四平银(金)矿床Rb-Sr定年及热液活动的时间跨度

四平银（金）矿床石英包裹体 Rb－Sr等时线年龄 187± 4 Ma，表明首期成矿作用发生在燕山早期，矿床 Rb－Sr等时线年龄与蚀变绢云母 K－Ar年龄差异及不同矿段矿化特征差异表明，蚀变绢云母 K－Ar年龄反映后期热液成矿事件时代，四平银（金）矿床至少经历了两期热液成矿事件，首期成矿事件发生在燕山早期，晚期成矿事件发生在燕山中期，成矿热液活动时间跨度约 33 Ma。     

大别山北部黄土岭片麻岩的锆石U-Pb年龄和氧同位素组成：古老的原岩和多阶段历史

利用阴极发光和离子探针技术，对大别山北部黄土岭片麻岩的锆石进行了内部结构、U-Pb年龄和氧同位素组成的系统分析。黄土岭片麻岩的锆石具有核-幔-边三层结构，核部是原岩的岩浆锆石，形成时代为-2800Ma；幔部是变质重结晶的产物，变质作用的时代为-2000Ma；边部则是在-110Ma从部分熔融体里结晶出来的增生锆石，是受大别山燕山期构造-岩浆事件影响的反映。黄土岭片麻岩和麻粒岩中-2800Ma和-2000Ma的年龄，以及麻粒岩中约3400Ma的残留锆石年龄均可以与扬子崆岭群变质岩对比。由此可以推断，北大别在构造属性上属于扬子板决，扬子与华北板决的缝合线应在北大别以北。锆石的核-幔-边具有不同的氧同位素组成，氧同位素数据表明黄土岭片麻岩的原岩是S型花岗岩，在-2000Ma和-110Ma的事件中都有外来物质(流体或熔体)的加入。     

苏鲁造山带古元古代超高温麻粒岩及其构造意义

本文报道了在苏鲁超高压变质带北端威海地区识别出的古元古代超高温泥质麻粒岩。泥质麻粒岩与大理岩、钙硅酸盐岩和片麻岩等变质表壳岩伴生。这些表壳岩以透镜体的形式产于经历了三叠纪超高压变质的新元古代正片麻岩中。泥质麻粒岩由石榴石、夕线石、斜长石、钾长石、反条纹长石、石英、黑云母、白云母和金红石组成。黑云母和白云母呈石榴石和夕线石的冠状体产出,为退变质矿物。相平衡模拟结果表明,麻粒岩峰期变质的温度和压力条件为~940℃和~1.2GPa。泥质麻粒岩中的锆石近等粒状或椭圆形,具有扇状或冷杉状分带,大多数具有平坦甚至亏损的重稀土配分模式,并有Eu负异常,为典型的麻粒岩相变质锆石。锆石的LA-ICP-MS U-Pb定年结果给出了1845±9Ma的207Pb/206Pb加权平均年龄,表明超高温麻粒岩形成于古元古代。结合现有的其他研究结果,我们推测扬子板块北缘经历了古元古代的增生造山作用。     

皖东侵入岩矿物Rb-Sr和Ar-Ar年代学及其与氧同位素平衡之间的关系

为探讨花岗质岩石中矿物O同位素平衡与Rb Sr矿物等时线年龄有效性之间的关系 ,测定了皖东屯仓与横山两个石英二长岩体中单矿物的Rb Sr和O同位素组成以及角闪石和黑云母的Ar Ar年龄。屯仓岩体的石英 -角闪石对温度为 5 4 5± 2 5℃ ,石英 -黑云母对温度为 4 6 0± 2 0℃ ,石英 -斜长石对温度 385± 4 0℃。横山岩体的石英 -角闪石对温度为 5 30± 2 5℃ ,石英 -黑云母对温度为 390± 15℃和石英 -斜长石对温度 2 85± 35℃。反映封闭体系中矿物在冷却过程中的退化交换再平衡。矿物间的氧同位素平衡对应于有地质意义的Rb Sr矿物等时线年龄。屯仓岩体的全岩 -角闪石 -斜长石Rb Sr等时线年龄 (12 8.4± 4 .7Ma)与角闪石的Ar Ar年龄 (12 5 .5 1± 0 .5 5Ma)在误差范围内一致 ,全岩 -角闪石 -斜长石 -黑云母Rb Sr等时线年龄 (12 0 .3± 2 .6Ma)与黑云母的Ar Ar年龄 (118.0± 0 .1Ma)一致。横山岩体的全岩 -角闪石 -斜长石Rb Sr矿物等时线年龄 (10 8± 15Ma)比角闪石的Ar Ar年龄 (12 5 .7± 1.8Ma)低 ,全岩 -角闪石 -斜长石 -黑云母Rb Sr等时线年龄 (118.6± 1.2Ma)小于黑云母的Ar Ar年龄 (12 0 .0± 0 .2Ma)。Rb Sr等时线年龄小于Ar Ar年龄是由于长石的蚀变引起的。大的等时线误差是由于Rb/Sr比值变化范围太小     

四川冕宁沙坝麻粒岩的岩石地球化学性质及形成时代

沙坝麻粒岩是扬子陆块西缘前寒武系变质杂岩的重要代表。麻粒岩具有Ba、Ce、LREE和Al的富集以及Nb、Ta、Zr、Hf、Ti和HREE亏损的岩石化学性质,结合对麻粒岩的Rb—Sr、Sm—Nd4、0Ar/39Ar和锆石U—Pb测年结果的分析和比较,表明沙坝麻粒岩的原岩形成于新元古代(780Ma)扬子陆块西缘活动大陆边缘的岛弧环境。根据对麻粒岩的变质演化历史和岩石地球化学特征分析,角闪岩相退变质的流体作用对麻粒岩的Rb—Sr、Sm—Nd和40Ar/39Ar同位素计时体系产生了严重干扰,这也是沙坝麻粒岩峰期变质和角闪岩相退变质时代难以确定的重要原因。     

Rb-Sr and Sm-Nd Geochronology of the Eppawala Metamorphic Rocks and Carbonatite,Wanni Complex,Sri Lanka

Petrological studies on the surrounding metamorphic rocks of the Eppawala carbonatite body, Wanni complex, Sri Lanka, revealed that these rocks had been metamorphosed under amphibolite to granulite facies conditions. Garnet-sillimanite-biotite gneiss shows lower range of metamorphic temperature (730–770°C) than the migmatite gneiss (750–780°C) and the pressure varies from 6.6–7.8 kbar to 5.6–6.4 kbar respectively. The metamorphic age of the garnet-sillimanite-biotite gneiss and migmatite gneiss dated 607±23 Ma and 626±16 Ma, respectively for mineral — whole rock isochron in Sm-Nd system. These ages are compatible with the ages of regional high-grade metamorphism occurred 610–550 Ma in the three crustal units in Sri Lanka.Rb-Sr system for biotite, apatite and whole-rock fractions suggests 493±5 Ma for the Eppawala carbonatite body. This age indicates the cooling age of the biotite. The presence of non-crystalline carbonatite matrix and large hexagonal apatite crystals suggests a slow cooling history. Further, low closure temperature of biotite in Rb-Sr system suggests that the intrusion age of carbonatite body should be more than 493 Ma, but non-metamorphosed nature provides evidence that the intrusion age of the carbonatite body should be less than the period of regional metamorphism 610–550 Ma. Therefore, Eppawala carbonatite body has a strong possibility to be a late to post magmatic intrusion. The other late to post magmatic intrusions in the Wanni complex and Highland complex are dated between 580–550 Ma. Therefore, the most probable intrusion age of the Eppawala carbonatite body is suggested to be around 550 Ma.     

大别山北部榴辉岩和英云闪长质片麻岩锆石U-Pb年龄及多期变质增生

大别山北部榴辉岩及英云闪长质片麻岩的锆石U-Pb年龄分析表明：北部榴辉岩相峰期变质时代为226～230Ma左右;北部塔儿河一带英云闪长质片麻岩经历过印支期变质事件;大别山北部与南部超高压岩石中一致的（226～230Ma）高压或超高压变质年龄表明,北部镁铁-超镁铁质岩带中部分岩石也曾作为扬子俯冲陆壳的一部分,在印支期发生过高压或超高压变质作用;本区锆石发生过两期变质增生事件,一是印支期高压或超高压变质,另一期是燕山期热变质事件;榴辉岩及英云闪长质片麻岩的原岩形成时代为晚元古代;锆石U-Pb年龄可用多期变质增生模型来解释。     

Geochronology of Yanshanian Magmatism and Metamorphism in the Hinterland of the Dabie Mountains and Their Geologic Implications1

Abstract A strong tectono-magmatic thermal event has been revealed by field observations of granitic, migmatitic and metamorphic rocks in the hinterland of the Dabie Mountains. K-Ar, Ar-Ar and Rb-Sr determinations show that the event took place 133–117 Ma ago (Yanshanian). Contemporaneously, a southwestward thrust-type ductile shearing at multiple levels occurred in the lower crust or at even deeper levels, suggesting that the Dabie Mountains region was still under the influence ot strong continent-continent overlapping tectonism of the Yangtze block under the Sino-Korean block at depth. Metamorphic rocks of amphibolite facies, migmatites and deep structural deformations resulting from this tectonothermal event are now exposed to the surface. The present features of the Dabie Mountains thus have appeared only since ca. 100 Ma B.P. The block composed of the Dabie Group is not an uplift or shield which would have undergone a long-continued erosion.     

北大别片麻岩的锆石U—Pb年龄离子探针测定及其地质意义

本文对北大别西部的湖北英山万家老屋、罗田七道河尹家店和安徽金寨丁埠乡李集3个片麻岩样品中锆石进行了BSE显微结构分析，并在此基础上对锆石进行了离子探针U－Pb年龄测定。结果表明北大别存在两种类型的片麻岩，它们的原岩分别形成于晋宁期和燕山期，其中英山万家老屋片麻岩的形成年龄为794Ma，后期地质事件对其锆石U－Pb年龄造成的影响较小；七道河尹家店片麻岩的形成年龄为730Ma，并可能受到燕山期岩浆事件的影响，得到了140Ma左右的变质年龄；丁埠乡李集片麻岩的形成年龄为140Ma。结合已有的年代学结果，北大别地体广泛存在晋宁期的岩浆事件，表明其可能为扬子板块的北缘。     

变质锆石成因的岩相学研究——高级变质岩U-Pb年龄解释的基本依据

岩相学在研究高级变质岩 (含深熔片麻岩 )的锆石中起着重要的作用 ,其内容主要包括锆石的形貌和表面特征 ,锆石在岩石中的赋存状态 ,与主晶的关系和内部结构等方面。基于大别山地区的一些榴辉岩相岩石、麻粒岩相岩石和片麻状花岗质岩石中锆石的研究 ,阐述了继承锆石、变质锆石、深熔锆石、变质增生、深熔增生和后期流体改造的基本岩相学特征。结合大别山地区的 4个实例 ,说明了高级变质岩中锆石的岩相学研究方法和步骤 ,并初步提出了高级变质岩锆石U -Pb年龄解释的岩相学标志。     

Single zircon evaporation ages: Evidence for the Mesoproterozoic crust in the southeastern Nigerian basement complex

The Ukwortung area of the Obudu Plateau exposes high-grade metamorphic rocks of upper amphibolite to granulite facies. Zircon grains from three locations of Southwest Obudu Plateau were dated by the Pb-Pb dating method. This single zircon radiometric dating method confirms the occurrence of Mesoproterozoic crust in the southeastern Nigeria basement complex. The pyroxene gneiss (granulite facies) sample from Biereberi near Ukpe yielded a mean age of 2061.4±0.4 Ma, suggesting the presence of Paleoproterozoic crust. The combined 207Pb/206Pb ratios from the garnet-biotite gneiss in the area gave a mean age of 1794.4±0.4 Ma. This further confirms the pres-ence of Paleoproterozoic crustal components within the Obudu Plateau. The Mesoproterozoic (1548.8±0.5 Ma) and Neoproterozoic (619.8±0.9 Ma) ages were obtained from two populations of zircon grains from the leucogranite in Okordem, Southwest Obudu. These "signatures" collaborate the occurrence of Mesoproterozoic ages in the Afar region and Cameroon basements along with the southeastern Nigerian basement complex, constituting the major portion of the West Central African mobile belt. The zircon age of 1794.4±0.4 Ma may probably be the maximum depositional age of the meta-sediment (garnet-biotite gneiss) and the age of 1548.8±0.5 Ma may be interpreted as the time of emplacement of the granitoid. The Neoproterozoic age (619.8±0.9 Ma) probably records the metamorphic event that was prevalent during the Pan-African period and thus affected the area.     

The Dabieshan Coesite-bearing Eclogite Terrain-A Late Archaean Ultra - high- Pressure Metamorphic Belt

A U -Pb zircon age of 2774±24 Ma for eclogite from the Bixiling rock body of Anhui Province, central China, indicates that the Dabieshan coesite-bearing eclogite was probably formed in the Late Archaean. A phengite Ar-Ar isochron age of 662±13 Ma for the eclogite confines also an upper limit age of its subsequent retrograde metamorphism in the Precambrian. The results of isotopic dating for such type of eclogite coincide with the geological features of its restricted occurrence within the Archaean metamaorphic terrain composed of the Dabie Group. It is believed that the Dabieshan coesite-bearing eclogite terrain might be a Late Archaean ultra-high-pressure metamorphic belt. The Dabie Mountains area was the eastward extension of the southern Qinling structural belt during the Triassic. Both the Dabie Group and the coesite-bearing eclogite hosted therein underwent a late-stage dynamic metamorphic event. The present authors have obtained a muscovite Ar-Ar isochron age of 192.6±2.8 Ma from plagioclase gn     

大别山东部花岗片麻岩的锆石U-Pb年龄

花岗片麻岩是大别山区除超高压变质杂岩外的另一种重要岩石类型,本文测得南大别二长花岗片麻岩中单颗粒锆石U-Pb不一致线的上交点年龄为789±43 Ma.位于五河一水吼韧性剪切带南缘的糜棱岩化二长花岗片麻岩中锆石的²⁰⁷Pb/²⁰⁶Pb表面年龄接近一致年龄,为715～777 Ma,平均757 Ma,U-Pb不一致线的上交点年龄为815±70 Ma,下交点年龄为482±167 Ma.北大别石英二长片麻岩中锆石²⁰⁷Pb/206表面年龄的变化范围较广,介于594～700 Ma,平均为649 Ma,U-Pb不一致线的上、下交点年龄分别为814±97 Ma和477±77 Ma.这说明这些正片麻岩的侵位时间范围大致为750～850 Ma的晚元古代;南、北大别正片麻岩中的锆石年代学显示它们可能具有相似的形成与演化历史;约480 Ma前后的加里东运动对大别山地区可能也有影响.     

Carboniferous and Triassic eclogites in the western Dabie Mountains,east‐central China: evidence for protracted convergence of the North and South China Blocks

SHRIMP U–Pb dating and laser ablation ICP‐MS trace element analyses of zircon from four eclogite samples from the north‐western Dabie Mountains, central China, provide evidence for two eclogite facies metamorphic events. Three samples from the Huwan shear zone yield indistinguishable late Carboniferous metamorphic ages of 312 ± 5, 307 ± 4 and 311 ± 17 Ma, with a mean age of 309 ± 3 Ma. One sample from the Hong'an Group, 1 km south of the shear zone yields a late Triassic age of 232 ± 10 Ma, similar to the age of ultra‐high pressure (UHP) metamorphism in the east Qinling–Dabie orogenic belt. REE and other trace element compositions of the zircon from two of the Huwan samples indicate metamorphic zircon growth in the presence of garnet but not plagioclase, namely in the eclogite facies, an interpretation supported by the presence of garnet, omphacite and phengite inclusions. Zircon also grew during later retrogression. Zircon cores from the Huwan shear zone have Ordovician to Devonian (440–350 Ma) ages, flat to steep heavy‐REE patterns, negative Eu anomalies, and in some cases plagioclase inclusions, indicative of derivation from North China Block igneous and low pressure metamorphic source rocks. Cores from Hong'an Group zircon are Neoproterozoic (780–610 Ma), consistent with derivation from the South China Block. In the western Dabie Mountains, the first stage of the collision between the North and South China Blocks took place in the Carboniferous along a suture north of the Huwan shear zone. The major Triassic continent–continent collision occurred along a suture at the southern boundary of the shear zone. The first collision produced local eclogite facies metamorphism in the Huwan shear zone. The second produced widespread eclogite facies metamorphism throughout the Dabie Mountains–Sulu terrane and a lower grade overprint in the shear zone.