Problems associated with luminescence dating of Late Quaternary glacial sediments in the NW Scottish Highlands

Linking the timing of glacial episodes and behaviour to climatic shifts that are documented in ice and marine sedimentary archives is key to understanding ocean-land interactions. In the NW Scottish Highlands a large number of closely spaced (‘hummocky’) moraines formed at retreating glacier margins. Independent age control on one palaeo-glacier limit is consistent with the timing of Younger Dryas (YD) glaciation in the area, but adjacent glacier lobes have remained undated due to the lack of sites and material for ¹⁴C dating. Direct dating of ice-marginal moraines using optically stimulated luminescence (OSL) techniques has never been attempted before in Scotland, but if successful, they may be the most appropriate methods for constraining the age of sediment deposition in the absence of organic material. Coarse-grained quartz and K-feldspar minerals from supraglacial sheet flow deposits and glacilacustrine sediments within ice-marginal moraines were analysed using the single-aliquot regenerative-dose (SAR) protocol. Independent age control and clear geomorphological relationships indicate that all samples should yield YD or post-Last Glacial Maximum (LGM) ages. Quartz OSL shine down curves showed low luminescence sensitivity, significant medium-to-slow components, a weak fast component, and scattered SAR data; Linearly Modulated-OSL (LM-OSL) measurements confirmed that the fast component was weak or absent. In contrast, feldspar infrared stimulated luminescence (IRSL) was highly sensitive with excellent SAR data. However, SAR data from 3 mm diameter aliquots of feldspar (200 grains) give higher than expected equivalent doses (D_e) by an order of magnitude. SAR measurements of small clusters of feldspar grains (ranging from 1–8) considerably broaden the apparent D_e distribution, but even the lowest value is about 2–3 times the expected D_e. Two possibilities arise to explain the quartz and feldspar data: (1) that glacial sequences in the NW Highlands re-work inherited (older) glacial deposits and that some of the pre-Devensian existing glacial landforms have only been modified during Devensian glaciation; or (2) that the sedimentary processes operating in these ice-marginal environments are not conducive to adequate bleaching of quartz and feldspar grains. Our study implies that ice-proximal supraglacial sediments from this region in NW Scotland reflect older ages of deposition, but dating YD sediments has not been possible.     

Comparison of paired quartz OSL and feldspar post-IR IRSL dose distributions in poorly bleached fluvial sediments from South Africa

A comparative study using quartz optically stimulated luminescence (OSL) and feldspar post-infrared infrared stimulated luminescence (post-IR IRSL) was undertaken on Quaternary fluvial sediments from an unnamed tributary of the Moopetsi River in South Africa. The aim is to assess whether the post-IR IRSL signal can be used to date incompletely bleached sediments. Several post-IR IRSL signals using varying stimulation and preheat temperatures were investigated; of these the post-IR IRSL₂₂₅ signal was deemed most appropriate for dating because it bleached most rapidly. The feldspar post-IR IRSL₂₂₅ equivalent dose (D_e) values from this site are consistently larger than those from quartz OSL, probably due to differences in the bleaching characteristics of the two signals. Additionally, the post-IR IRSL₂₂₅ D_e values within a sample showed less variation in precision than the quartz D_e data, possibly due to greater averaging between grains in the feldspar small aliquots. The agreement between ages based on the OSL and post-IR IRSL₂₂₅ signals was better for younger samples (<20 ka) than for older ones (>50 ka); the cause of this variation is unclear.     

Luminescence dating of the late Quaternary sediments in Hangzhou Bay,China

Coastal plain of Hangzhou Bay, to the south of the present Yangtze Estuary, is closely linked to the evolution of the Yangtze River delta. However, absolute age of Pre-Holocene sediments is limited, which hinders the understanding of this area's environmental evolution. In this study, using optically stimulated luminescence (OSL), single aliquots and single grains of quartz and K-feldspar were used to date the late Quaternary sediments in coastal plain on the southern Hangzhou Bay. The vertical difference in particle size composition render either silt- or sand-sized quartz for dating. Cross-checking of multiple OSL dating methods indicated that the upper ∼65 m recorded the Holocene part of the succession; sediment from a depth of 136.6 m was dated to ∼180 ka. It was found that the single-grain method was more reliable in comparison to single-aliquot age, the former minimized the effect of signal components. Single-grain quartz and K-feldspar luminescence yielded consistent ages at sample depth of 136.6 m (∼160–180 ka), while the latter gave robust age at depth of 115.5 m (∼150 ka). This chronology is in general in accordance with neighbouring cores and can constrain paleomagnetic dating results in those cores. Taking together, the study site has thickest Holocene deposits in comparison to the highland centered around Taihu Lake on the southern Yangtze delta. Moreover, the luminescence characteristics of quartz from different sample depths, behaved differently with respect to luminescence sensitivity, signal components and saturation level, perhaps reflecting varied provenance and weathering characteristics caused by climate change.     

Bayesian analysis of individual and systematic multiplicative errors for estimating ages with stratigraphic constraints in optically stimulated luminescence dating

Many dating techniques include significant error terms which are not independent between samples to date. This is typically the case in Optically Stimulated Luminescence (OSL) dating where the conversion from characteristic equivalent doses to the corresponding ages using the annual dosimetry data includes error terms that are common to all produced datings. Dealing with these errors is essential to estimate ages from a set of datings whose chronological ordering is known. In this work, we propose and we study a Bayesian model to address this problem. For this purpose, we first consider a multivariate model with multiplicative Gaussian errors in a Bayesian framework. This model relates a set of characteristic equivalent doses to the corresponding ages while taking into account for the systematic and non-systematic errors associated to the dosimetry. It thus offers the opportunity to deal properly with stratigraphic constraints within OSL datings, but also with other datings possessing errors which are independent from systematic errors of OSL (e.g. radiocarbon). Then, we use this model to extend an existing Bayesian model for the assessment of characteristic equivalent doses from Single Aliquot and Regenerative (SAR) dose measurements. The overall Bayesian model leads to the joint estimation of all the variables (which include all the dose–response functions and characteristic equivalent doses) of a sequence of, possibly heterogeneous, datings. We also consider a more generic solution consisting in using directly the age model from a set of characteristic equivalent dose estimates and their associated standard errors. We finally give an example of application on a set of five OSL datings with stratigraphic constraints and observe a good adequacy between the two approaches.     

Detecting post-depositional sediment disturbance in sandy deposits using optical luminescence

Post-depositional mixing or exhumation is common in surficial sediments, yet may be unobservable from field evidence. However, any disturbance may have significant consquences in terms of establishing a reliable luminescence age determination. Optically stimulated luminescence (OSL) measurements, particularly measurements at the single grain level, can be used to gain an insight into both contemporary and past post-depositional processes.

This paper examines sites from Texas and Florida (USA) with independent chronological control to demonstrate the potential effects of varying degrees of bioturbation on OSL. Results show that contemporary soil forming processes clearly impact on the palaeodose (D_e) replicate distributions which are measured in order to derive an OSL age. Significant levels of scatter and apparently zero dose grains are observed in the upper-most sediments; declining with depth from the surface. D_e replicates from undisturbed and fully bleached sediments are unskewed, show low overdispersion (OD) and comparable single grain and single aliquot OSL ages. Bioturbated sediments, however, may show highly skewed multi-model D_e distributions with higher OD values, zero dose grains at depth, and significant diffences between single grain and single aliquot results. True burial ages may be derived from minimally bioturbated sediments through the application of statistical analysis such as finite mixture modelling to isolate D_e components. However, for significantly bioturbated sediments, the latter approach, even at the single grain level, produces inaccurate ages. In such cases we argue that additional evidence (both dating and contexual) may be required to identify with confidence the burial D_e population.     

Luminescence dating of quartz from ironstones of the Xingu River,Eastern Amazonia

This study reports on the first investigation into the potential of quartz luminescence dating to establish formation ages of ferruginous duricrust deposits (ironstones) of the Xingu River in Eastern Amazonia, Brazil. The studied ironstones comprise sand and gravel cemented by goethite (FeO(OH)), occurring as sandstones and conglomerates in the riverbed of the Xingu River, a major tributary of the Amazon River. The Xingu ironstones have a cavernous morphology and give origin to particular habitat for benthic biota in an area that hosts the largest rapids in Amazonia. So far, the Xingu ironstones have uncertain formation ages and their sedimentary origin is still poorly understood. In this way, seven samples of ironstones distributed along the lower Xingu River were collected for optically stimulated luminescence (OSL) dating of their detrital quartz sand grains. Additionally, the organic content of some samples was dated by radiocarbon (¹⁴C) for comparison with quartz OSL ages. The luminescence ages of the sand-sized quartz grains extracted from the ironstones were obtained from medium (100–300 grains) and small (10–20 grains) aliquots using the single aliquot regenerative-dose (SAR) protocol. Equivalent doses (D_e) distributions have varied overdispersion (OD) both for medium size aliquots (OD = 19–58 %) and small size aliquots (OD = 29–76 %). No significant trend was observed between D_e and aliquot size. The studied ironstones grow over the riverbed, but stay below or above water throughout the year due to the seasonal water level variation of the Xingu River. However, the effect of water saturation in dose rates is reduced due to relatively low porosity of ironstones. Water saturated dose rates (dry sample dose rates) range from 2.70 ± 0.21 (2.79 ± 0.22) Gy/ka to 12.34 ± 0.97 (13.26 ± 1.12) Gy/ka, which are relatively high when compared to values reported for Brazilian sandy sediments elsewhere (∼1 Gy/ka). Samples with high overdispersion (>40 %) are mainly attributed to mixing of grains trapped in different time periods by goethite cementation. The obtained OSL ages for water saturated (dry) samples range from 3.4 ± 0.3 (3.3 ± 0.4) ka to 59.6 ± 6.0 (58.1 ± 6.4) ka, using D_e determined from medium size aliquots and dose response curves fitted by an exponential plus linear function. Radiocarbon ages of the bulk organic matter extracted from selected ironstone varied from ca. 4 cal ka BP to ca. 23 cal ka BP. Significant differences were observed between OSL and radiocarbon ages, suggesting asynchronous trapping of organic matter and detrital quartz within the ironstone matrix. These late Pleistocene to Holocene ages indicate that ironstones of the Xingu River result from an active surface geochemical system able to precipitate goethite and cement detrital sediments under transport. The obtained ages and differences between OSL and radiocarbon ages point out that the ironstones have multiphase and spatially heterogeneous growth across the Xingu riverbed. Our results also expand the application of luminescence dating to different sedimentary deposits.     

A revised burial dose estimation procedure for optical dating of youngand modern-age sediments

The presence of genuinely zero-age or near-zero-age grains in modern-age and very young samples poses a problem for many existing burial dose estimation procedures used in optical (optically stimulated luminescence, OSL) dating. This difficulty currently necessitates consideration of relatively simplistic and statistically inferior age models. In this study, we investigate the potential for using modified versions of the statistical age models of Galbraith et al. [Galbraith, R.F., Roberts, R.G., Laslett, G.M., Yoshida, H., Olley, J.M., 1999. Optical dating of single and multiple grains of quartz from Jinmium rock shelter, northern Australia: Part I, experimental design and statistical models. Archaeometry 41, 339–364.] to provide reliable equivalent dose (D_e) estimates for young and modern-age samples that display negative, zero or near-zero D_e estimates. For this purpose, we have revised the original versions of the central and minimum age models, which are based on log-transformed D_e values, so that they can be applied to un-logged D_e estimates and their associated absolute standard errors. The suitability of these ‘un-logged’ age models is tested using a series of known-age fluvial samples deposited within two arroyo systems from the American Southwest. The un-logged age models provide accurate burial doses and final OSL ages for roughly three-quarters of the total number of samples considered in this study. Sensitivity tests reveal that the un-logged versions of the central and minimum age models are capable of producing accurate burial dose estimates for modern-age and very young (<350 yr) fluvial samples that contain (i) more than 20% of well-bleached grains in their D_e distributions, or (ii) smaller sub-populations of well-bleached grains for which the D_e values are known with high precision. Our results indicate that the original (log-transformed) versions of the central and minimum age models are still preferable for most routine dating applications, since these age models are better suited to the statistical properties of typical single-grain and multi-grain single-aliquot D_e datasets. However, the unique error properties of modern-age samples, combined with the problems of calculating natural logarithms of negative or zero-Gy D_e values, mean that the un-logged versions of the central and minimum age models currently offer the most suitable means of deriving accurate burial dose estimates for very young and modern-age samples.     

Luminescence dating of Weichselian interstadial sediments from the German Baltic Sea coast

A cliff outcrop called Kluckow, in the Baltic Sea area, with a (glacio-) fluvial to (glacio-) lacustrine succession, provides a unique opportunity to resolve uncertainties in the timing and extent of several poorly constrained Weichselian ice advances. Based on a detailed lithofacies analysis, we selected four sampling horizons for luminescence dating to determine a depositional chronology. We measured both coarse-grain quartz and potassium-rich feldspar for age determination using optically stimulated luminescence (OSL) and post-IR infrared stimulated luminescence (pIRIR). Furthermore we addressed potential problems such as incomplete bleaching and quartz saturation effects. The resulting luminescence-chronology, supported by one radiocarbon age, illustrates a depositional time interval of the investigated sequence between ∼62 and ∼22 ka. Within this sequence a mussel-bearing fluvial sand indicate interstadial climate conditions at approximately 46 ka. The upper part of the section is composed of a 4 m thick glaciolacustrine silty clay and an overlying glaciofluvial sand; the latter yielded an OSL age of ∼22 ka. Shortly after these sequences formed, the subsequent ice advance (indicated by the overlying till sheet) reached the study area. Based on our new chronology and lithofacies analysis, we conclude that the Scandinavian Ice Sheet did not reach the study area between ∼62 and ∼22 ka.     

Optical dating of a Paleolithic site near the eastern coastal region of Shandong,northern China

Many archaeological sites were excavated in China, but rarely in the adjacent coastal areas. An archaeological site at Huangniliang in the coastal area of Shandong Province, northern China was excavated in 2013. Abundant stone artifacts including hammers, cores, flakes, chunks, and retouched tools are found in the silty aeolian sediments. In this study, optically stimulated luminescence (OSL) technique was employed to establish the chronological framework of the site. Medium-grained (45–63 μm) quartz was extracted from six sediment samples for dating. The equivalent doses obtained with the single-aliquot regenerative-dose (SAR) protocol are shown to increase with depth. Three samples from the stone-tool containing layer yield OSL ages ranging from 54 ka to 59 ka, providing the earliest geochronological evidence for the presence of humans in the eastern coast of Shandong peninsula during the early period of Marine Isotope Stage (MIS) 3.     

Luminescence dating of canal sediments from Angkor Borei, Mekong Delta, Southern Cambodia

Work to apply luminescence dating to archaeological sites in the Lower Mekong Delta has continued with a programme aimed at dating ancient canal sediments and brick monuments in the vicinity of ancient city of Angkor Borei. Following the successful application of OSL dating to the Paris 2 canal near Angkor Borei further fieldwork and analysis has been undertaken. The infill and substrate of the larger Paris 4 canal connecting Angkor Borei to Oc Eo, some 80 km to the south in Vietnam has been sampled and subjected to luminescence analysis. Field spectroscopy and underwater bleaching experiments were also conducted in the Baray and Angkor Borei in 2004. The results show that both illumination intensities and spectral distributions are severely altered by as little as 1.5 m of turbid water, and that OSL bleaching rates for both quartz and feldspars are reduced. Since quartz resetting is heavily dependant on the UV components in daylight, which have preferentially attenuated the effects of turbid water on OSL zeroing rates are especially marked. The new data from the Paris 4 canal, which has been dated by OSL to be between the first millenium BC and the late first millenium AD are significant to understanding the archaeological development of the Fu Nan state in the Lower Mekong Delta, and the sequence of development of the canal network linking inland agrarian sites and coastal trading centres.     

Reliability of equivalent-dose determination and age-models in the OSL dating of historical and modern palaeoflood sediments

The challenge of accurately estimating the deposition age of incompletely-bleached samples in luminescence dating has motivated developments in the analysis of single grain dose distributions, and a number of statistical approaches have been proposed over the last few years. In this study, we compare the behaviour of the arithmetic average, so-called ‘robust statistics’, the Central Age Model (CAM), the Minimum Age Model (MAM) and the Internal–External Consistency Criterion (IEU) and lowest 5% method, when applied to single-grain dose distributions from a sequence of eight recent (40–1000 years) flash-flood deposits. These sediments are expected to be incompletely bleached, but all have age control from historical records. Modifications were made to allow the use of the standard CAM and MAM models with dose distributions containing near zero and negative dose values. An assessment of minimum over-dispersion (OD) is based on dose recovery tests based on gamma-irradiated samples. We then present a detailed analysis of the effect of an additional uncertainty added to the individual dose estimates on the burial dose estimates from the MAM and the IEU approach. The results of the various models are discussed in terms of the accuracy of the resulting age, and we conclude that, overall, the IEU approach generates the most accurate ages. We also demonstrate that accurate doses can be obtained for those older samples for which uncertainties of ∼40 years are unimportant by applying the IEU model to small aliquot (∼30 grains) dose distributions. From our study we conclude that these and similar young slack-water flood deposits can be accurately dated using quartz OSL, opening up the possibility of establishing time series of flood discharge in catchments for which no instrumental or historical record exists.     

The minimum extraction technique: A new sampling methodology for optically stimulated luminescence dating of museum ceramics

This paper introduces a novel optically stimulated luminescence (OSL) sampling protocol, referred to as the minimum extraction technique (MET), which assists in the OSL dating of museum ceramics. Here we outline how to extract a sample using this technique, as well as offering a discussion on the preparation protocols used for the method, and the calculation of the internal and external dose rates. A major benefit of MET is the minute sample size required, resulting in minimal damage to the museum object.MET permits OSL dating of material which would otherwise be usually off-limits for conventional OSL dating, for example, those housed in museum collections. In particular, MET can be used on objects which originate from regions where scientific analysis is currently not permitted on archaeological material, often owing to heritage laws.     

Investigating the potential of HCl-only treated samples using range-finder OSL dating

Rapid sample preparation and measurement protocols for optically stimulated luminescence (OSL) dating have been investigated as a method of increasing the throughput of samples (e.g. Roberts et al. 2009). Here, we investigate the potential of dating samples treated using only hydrochloric acid (HCl) for providing accurate range-finder ages for quartz. The equivalent dose (D_e) is underestimated for older samples using a standard single-aliquot regenerative-dose (SAR) protocol, but measurement of the post-IR OSL signal (e.g. Roberts and Wintle, 2003) provides D_e estimates within 15% of the ‘target fully prepared D_e’ for two-thirds of samples. The application of a standardised growth curve (SGC) is also investigated. For these dune samples, the most efficient preparation and measurement procedure from which accurate D_e estimates can be obtained is treatment with HCl-only, measurement of the natural and regenerative post-IR OSL signal, and calculation using a region-independent SGC. A slightly longer protocol incorporating an additional preparation stage of heavy liquid density separation can be used to improve D_e estimates in samples where feldspar-contamination is thought to be particularly problematic. In practice, these time savings of days to weeks in the preparation and measurement protocols mean that a large number of samples can first be rapidly treated with HCl, the post-IR blue OSL signal measured using a shortened double-SAR protocol, and D_e calculated by applying an independent SGC before then deciding which samples require full preparation and measurement, rather than the inefficiency of committing time and resources to all samples if this is unnecessary for the context of a particular suite of samples. The potential of this rapid preparation and measurement protocol is discussed in relation to sand dune dating studies.     

巢湖杭埠河流域湖相沉积物多指标揭示的全新世以来环境演变

在巢湖杭埠河流域中的古湖盆中心——三河圩区获取28.6 m长的湖相岩芯（SZK1507孔）,利用AMS¹⁴C测年技术建立可靠的地层年代序列,通过对SZK1507孔738 cm以上段湖相沉积物平均粒径、磁化率、总氮（TN）、总有机碳（TOC）及C/N的综合分析,高分辨率重建了巢湖杭埠河流域全新世以来的古环境演变过程.结果表明,本区域的环境变化过程可以分为4个阶段,阶段Ⅰ（约10050—9700 cal.a B.P.）与阶段Ⅲ（约9250—5300 cal.a B.P.）气候较为湿润,巢湖水位较高,平均粒径、磁化率值较低,TN、TOC、C/N也偏低;阶段Ⅱ（约9700—9250 cal.a B.P.）与阶段Ⅳ（约5300 cal.a B.P.以来）气候干燥,巢湖水量减少,水位降低,平均粒径、磁化率值、TN、TOC、C/N均较高.一些全球范围内显著发生的气候突变事件在SZK1507孔沉积记录中也有体现,如9.3、8.2和4.2 ka B.P.事件等.将巢湖杭埠河流域10000 cal.a B.P.以来的平均粒径、磁化率、TN、TOC、C/N沉积记录与全新世以来的北纬30°夏季太阳辐射量、太阳黑子数、火山喷发对大气中硫酸盐含量贡献率等进行对比,发现巢湖杭埠河流域全新世气候突变事件主要受控于北半球夏季太阳辐射量变化、太阳活动以及火山活动等因素,并与它们之间复杂的响应机制有关.     

Investigation of the applicability of standardised growth curves for OSL dating of quartz from Haua Fteah cave,Libya

The establishment of standardised growth curve (SGC) for equivalent dose (D_e) determination can substantially reduce the amount of instrument time required for OSL measurements. In this study, we investigated the applicability of SGC for the optically stimulated luminescence (OSL) signal from single grains and small aliquots of sedimentary quartz from Haua Fteah cave, in Libya. The samples exhibit large inter-grain and inter-aliquot variation in the shape of their single grain and small aliquot dose response curves (DRCs) constructed from a range of sensitivity-corrected regenerative dose signals (L_x/T_x), which prevents the establishment of a single common SGC among different grains or small aliquots. Instead, the DRCs for the small aliquots can be divided into a minimum of three groups using the Finite Mixture Model, with the DRC saturating at a different dose level for each group. In order to establish a common DRC, or SGC, for each group, we propose a new normalisation method, the so-called least-squares normalisation procedure (‘LS-normalisation’), which largely reduces the variation between aliquots within the same group and allows the establishment of a common DRC, or SGC, for each group. In order to apply the SGC method for these samples, two regenerative dose points are needed for each aliquot to attribute it to one of the groups based on the ratio of the L_x/T_x signals for two sensitivity-corrected regenerative dose points. Equivalent dose (D_e) values for each aliquot can be estimated using the fitting parameters calculated for the SGC of the relevant group to which it belongs, together with measurements of the natural signal (L_n), one regenerative dose signal (L_x1) and their corresponding test dose signals (T_n, T_x1). For the samples investigated from Haua Fteah, we found that D_e estimates obtained from the SGCs are consistent with those obtained using a full SAR procedure. Our results suggest that small single-aliquot and single-grain D_e values obtained from application of the SGC may be underestimated if there is a significant proportion of early-saturating grains present in the sample; such grains or aliquots are mostly rejected due to saturation when analysed using the full SAR procedure. In this case, it is necessary to calculate the D_e values based only on those grains or aliquots that have relatively high saturation levels.     

Testing the applicability of standardised growth curves (SGCs) for OSL signals of quartz grains from the Yangtze Delta,China

The standardised growth curve (SGC) technique has the potential to save instrument time for equivalent dose (D_e) determination when applying single-aliquot regenerative-dose (SAR) protocol during optically stimulated luminescence (OSL) measurements. In this study, we test the applicability of two commonly used SGC procedures for OSL signals of quartz grains from aqueous deposits of the Yangtze Delta in China, which have been reported for weak luminescence signals and suffering from partial bleaching. Multiple silt-sized and sand-sized fractions of quartz samples from eight cores are used to construct SGCs by test dose standardisation (TD-SGC) and least-squares normalisation (LS-SGC), respectively. Three strategies, i.e. region-specific (SGC_R), region with core-specific (SGC_R + C) and core-specific (SGC_C), are adopted to categorise these normalised data into different SGC datasets. The large variability of dose response signals is substantially reduced by the SGC procedures for most of these datasets. Hence, common SGCs for a variety of samples from the Yangtze Delta can be established, irrespective of their distinctive particle sizes and luminescence characteristics. The D_e values are then estimated using both TD-SGC and LS-SGC procedures for samples from a specific core. Comparing to the full SAR protocol, the TD-SGC procedure roughly gives reproducible D_e estimates lower than ∼100 Gy while the LS-SGC procedure derives generally consistent D_e estimates of up to ∼230 Gy. Although LS-SGC_C and LS-SGC_R + C procedures replicate the most consistent D_e values, the LS-SGC_R procedure performs better in efficiency with a slightly less accuracy. In addition to careful comparison of LS-SGC and full SAR procedures, we suggest that a synchronous ratio derived by the chosen regenerative dose and its response signal for re-normalisation can be used to predict the LS-SGC D_e reliability on samples from similar sedimentary environments.     

Optically stimulated luminescence age of the Old Cedar midden, St. Joseph Peninsula State Park, Florida

We report optically stimulated luminescence (OSL) dating results from the Old Cedar midden in St. Joseph Peninsula State Park, located between the Gulf of Mexico and St. Joseph Bay near Port St. Joe, FL, USA. The Old Cedar site (8GU85) is located on top of a relict beach ridge which is actively eroding into St. Joseph Bay. Old Cedar is noted for its conch shell tool assemblage, otherwise rare at northwest Florida archaeological sites, and is believed to have been utilized during the Late Woodland Weeden Island and possibly the Fort Walton periods [Benchley, E.D., Bense, J.A., 2001. Archaeology and history of St. Joseph Peninsula State Park: Phase I investigations. Report of Investigations, No. 89, University of West Florida Archaeology Institute]. After removing surficial erosion deposits, we extracted OSL core samples from both the midden layer and the underlying beach ridge. The resulting OSL age is compared with the age of another beach ridge on St. Joseph Peninsula. We hope that this study will aid in the investigation and conservation of Old Cedar specifically and other Weeden Island sites in the St. Joseph Bay area.     

Chronology of the Paleolithic site of Xibaimaying in the Nihewan Basin,North China,inferred from optical dating of fine-grained quartz

The Paleolithic site of Xibaimaying (XBMY), once considered the youngest flake tool site within the Nihewan Basin, North China, is an ideal archive to study the chronological relationship between flake tool and microblade industries in the Nihewan Basin during the Upper Palaeolithic, but the previous ages obtained for the site remain controversial. From 2015 to 2019, three areas at two archaeological localities (XBMY-I and XBMY-II) of the site were excavated, and well-preserved fossils and flake tools were unearthed. In this study, a total of 26 samples were collected from the three areas for optically stimulated luminescence (OSL) dating using a single-aliquot regenerative-dose (SAR) protocol on fine-grained quartz. A shared ‘Standardized growth curve’ (SGC) for a section was constructed to reduce the time required for D_e estimation. The long-term weighted average water contents of the samples during their burial period were estimated based on the in-situ water contents of continuous samples from a nearby borehole. All the OSL ages were modelled via Bayesian statistics using the OxCal software, modifying the OSL ages with stratigraphic constraints in each section. The results show that the cultural layer bearing flake tool assemblages falls within the period of 122–36 ka, indicating that the flake tool industry of the Xibaimaying site is comparable to that of the Youfangbei (108–86 ka), Banjingzi (∼86 ka) and Xinmiaozhuang (75–63 ka) sites, rather than the youngest one in the Nihewan basin, which explains why the Xibaimaying site is characterized as pure flake tool culture without any ‘advanced’ trait. The OSL dating results also shed new light on the study of sedimentary processes in the Xibaimaying site area. The different deposition rates (0.01–1.61 mm/a) for the sediments at the three newly excavated areas imply complex geomorphologic processes in the site area.     

The potential of cryptotephra and OSL dating for refining the chronology of open-air archaeological windblown sand sites: A case study from Mirkowice 33, northwest Poland

The discovery of a cryptotephra (nonvisible volcanic horizon) in a windblown sand archaeological site in Poland highlights how luminescence and tephrostratigraphy may combine to better refine the chronology of such sites. In this study we identify a cryptotephra horizon which on the basis of major and minor element geochemistry and an OSL age of 2.3 ± 0.1 ka is correlated to the Glen Garry tephra. The different methodological strengths of OSL and tephrostratigraphy may be harnessed to counter the limitations of a single approach to produce a more secure chronology. Although in this study the tephra deposition event is shown to post-date the archaeological activity, the methodological approach is clearly demonstrated. Further investigations will reveal if cryptotephra layers are commonly preserved in such environmental settings. If this is so then future applications of this approach may prove to be more widely applicable.     

Variations in the sensitivity of the optically stimulated luminescence from quartz in the Xifeng section: A spatiotemporal comparison across the Chinese Loess Plateau since the last interglaciation

The sensitivity of the optically stimulated luminescence (OSL) from quartz is thought to be mainly influenced by source rock (crystallization temperature and quartz defect types) and depositional history (irradiation/bleaching cycles). In this study, the OSL sensitivity of quartz of different grain sizes from loess (L1) and paleosol (S1) layers at the Xifeng section of the Chinese Loess Plateau was analyzed. The OSL sensitivity of the samples from the Xifeng section shows a distinct difference between glacial and interglacial cycles, which is consistent with the patterns observed from magnetic susceptibility (MS) and grain sizes. The highest OSL sensitivity is observed in S1, which is twelve times the lowest sensitivity observed in L1. Moreover, the contribution of the fast component of quartz OSL from the paleosol accounts for more than 90% of the total OSL signal. In contrast, the middle and slow components contribute more in loess, and a significant variation among different aliquots was observed.Comparison of the data obtained from loess sections from different regions, including Xifeng, Luochuan, Jingyuan and Shimao, show significant differences in the magnitudes of OSL sensitivity but a similar pattern between glacial and interglacial periods. The results of this study suggest that, except for the wildfire model proposed to interpret the high OSL sensitivity in paleosol (Zhang, 2018), the shift of wind pattern of westerly wind (i.e., transporting “dim” source from North Tibetan Plateau and northwesterly wind (i.e., transporting “bright” source from Alxa Arid Lands and the subsequent mixture from the different sources may partially contribute to the different OSL sensitivities observed for Xifeng and Luochuan. In contrast, the OSL sensitivity of Shimao samples from L1 was affected by the input from the Mu Us Desert, and those of Jingyuan may affected by the contribution from the Yellow River.