OSL dating of the Middle Palaeolithic Hotel California site,Sierra de Atapuerca,north‐central Spain

In this study we present optically stimulated luminescence (OSL) dating results obtained at one of the most important open‐air Middle Palaeolithic sites in the Sierra de Atapuerca foothills – Hotel California. We also assess the possibility of obtaining extended‐range OSL chronologies for a nearby Middle Pleistocene fluvial deposit using several novel methods, namely OSL dating of individual quartz ‘supergrains’, multi‐grain aliquot thermally transferred OSL (TT‐OSL) dating and the first application of a single‐grain TT‐OSL dating procedure. Four single‐grain OSL ages constrain the Middle Palaeolithic occupation of Hotel California to between 71±6 and 48±3 ka. The Hotel California single‐grain equivalent dose (D_e) distributions are highly overdispersed and contain several dose populations, which are probably attributable to post‐depositional sediment mixing, partial bleaching and intrinsic scatter. The reliability of multi‐grain aliquot OSL dating is compromised by the complex underlying D_e dispersion affecting these samples, as well as by biasing multi‐grain averaging effects. Extended‐range OSL and TT‐OSL chronologies for the nearby Pico River terrace are consistent with each other and with broad independent age control. These experimental approaches yield a weighted average age of 348±16 ka for terrace T_A9 of the Arlanzón River sequence. Our results highlight the benefits of comparing ages obtained using several OSL methodologies to improve the robustness of luminescence chronologies. They also demonstrate the potential that single‐grain OSL techniques offer for establishing improved age constraints on the many other Middle Palaeolithic sites found at Atapuerca and elsewhere across north‐central Spain.     

Paper II – Dirt,dates and DNA: OSL and radiocarbon chronologies of perennially frozen sediments in Siberia,and their implications for sedimentary ancient DNA studies

Arnold, L. J., Roberts, R. G., MacPhee, R. D. E., Haile, J. S., Brock, F., Möller, P., Froese, D. G., Tikhonov, A. N., Chivas, A. R., Gilbert, M. T. P. & Willerslev, E. 2010: Paper II – Dirt, dates and DNA: OSL and radiocarbon chronologies of perennially frozen sediments in Siberia, and their implications for sedimentary ancient DNA studies. Boreas, Vol. 40, pp. 417–445. 10.1111/j.1502‐3885.2010.00181.x. ISSN 0300‐9483 The sedimentary ancient DNA (sedaDNA) technique offers a potentially invaluable means of investigating species evolution and extinction dynamics in high‐latitude environments. An implicit assumption of the sedaDNA approach is that the extracted DNA is autochthonous with the host deposit and that it has not been physically transported from older source deposits or reworked within the sedimentary profile by postdepositional mixing. In this paper we investigate whether these fundamental conditions are upheld at seven perennially frozen wetland sites across the Taimyr Peninsula and coastal lowlands of north‐central Siberia. Optically stimulated luminescence (OSL) and radiocarbon (¹⁴C) dating are used to constrain the ages of both the inorganic and organic fractions of perennially frozen deposits from which sedaDNA of extinct and extant species have been recovered. OSL and ¹⁴C age/depth profiles, as well as single‐grain equivalent dose (D_e) distribution characteristics, are used to assess the stratigraphic integrity of these sedaDNA sequences by (i) identifying the presence of primary or reworked organic and inorganic material, and (ii) examining the types of depositional and postdepositional processes that have affected specific sedimentary facies. The results of this study demonstrate that even though DNA preservation and stratigraphic integrity are commonly superior in perennially frozen settings, this does not, in itself, guarantee the suitability of the sedaDNA approach. The combined OSL and ¹⁴C chronologies reveal that certain perennially frozen sites may be poorly suited for sedaDNA analysis, and that careful site selection is paramount to ensuring the accuracy of any sedaDNA study – particularly for ‘latest appearance date’ estimates of extinct taxa.     

Age of the Pomeranian ice‐marginal position in northeastern Germany determined by Optically Stimulated Luminescence (OSL) dating of glaciofluvial sediments

Lüthgens, C., Böse, M. & Preusser, F. 2011: Age of the Pomeranian ice‐marginal position in northeastern Germany determined by Optically Stimulated Luminescence (OSL) dating of glaciofluvial sediments. Boreas, 10.1111/j.1502‐3885.2011.00211.x. ISSN 0300‐9843 The Pomeranian ice margin is one of the most prominent ice‐marginal features of the Weichselian glaciation in northern Europe. Previous results of surface‐exposure dating (SED) of this ice margin disagree with established chronologies and ice retreat patterns, i.e. are much younger than previously expected. We crosscheck the age of the Pomeranian ice‐marginal position in northeastern Germany using single‐grain quartz Optically Stimulated Luminescence (OSL) dating of glaciofluvial sediments. OSL dating indicates an active ice margin between 20.1±1.6 ka and 19.4±2.4 ka forming outwash plains attributed to the Pomeranian ice‐marginal position. On the basis of these results, we suggest a critical reassessment of previous SED data available for the Pomeranian ice‐marginal position within their respective regional geomorphological contexts. From a process‐based point of view, SED ages derived from glacigenic boulders document the stabilization of the landscape after melting of dead ice and landscape transformation under periglacial conditions rather than the presence of an ice margin. SED indicates a first phase of boulder stabilization at around 16.4±0.7 ka, followed by landscape stabilization within the area attributed to the recessional Gerswalder subphase around 15.2±0.5 ka. A final phase of accumulation of glaciolacustrine and glaciofluvial sediments at around 14.7±1.0 ka documents the melting of buried dead ice at that time.     

Testing an approach to OSL dating of Late Devensian glaciofluvial sediments of the British Isles

In the British and Irish Isles, the understanding of expansion and retreat of the last ice sheet in Marine Isotope Stage (MIS) 2 has been hindered by a lack of chronological control for the timing of its maximum extent and subsequent retreat stages. In this research, a suite of lithofacies from a former distal ice marginal sandur at Orrisdale, Isle of Man, were identified and selected for optically stimulated luminescence dating. Different‐size fractions of quartz grains were extracted from selected lithofacies types with the aim of identifying which depositional environments and grain size fractions are best suited for optical dating. Tests have been undertaken to identify the luminescence properties of this quartz, including preheat dose recovery and constant‐wave optically stimulated luminescence (OSL) decay curve fitting. Equivalent dose distributions for all samples were wide and positively skewed, indicative of heterogeneous bleaching. A comprehensive statistically based decision‐making protocol has been defined in order to find the appropriate statistical model for burial dose estimation. Ages in the range of 17–14 ka have been obtained which agree with the expected geologically constrained chronology. The Orrisdale Formation is contemporaneous with Heinrich Event 1 and the Killard Point Stadial identified in eastern Ireland ca. 16.4 ka. The suggested approach for OSL dating of glaciofluvial sediments has the potential for much wider application to high latitude or temperate areas where there is an abundance of such sediments and where improved chronological control is much needed. Copyright © 2009 John Wiley & Sons, Ltd.     

OSL dating of a Holocene loess-paleosol sequence in the southern Loess Plateau,China

Optically stimulated luminescence (OSL) dating of polymineral fine-grained loess samples collected from the southern Loess Plateau of China was conducted using the single-aliquot regenerative-dose (SAR) protocol. A ‘Double-SAR’ procedure in which aliquots are subjected to both infrared (IR) and blue stimulations was used, and two sets of equivalent dose (D _e ) determinations were produced. These doses are assumed to be predominantly related to the feldspathic and quartz fine grain populations, respectively. The results revealed that the OSL ages estimated by infrared stimulated luminescence (IRSL) signals and those estimated by [post-IR] stimulated luminescence ([post-IR] OSL) signals disagreed. Specifically, the ages estimated using the IRSL signals were smaller than those estimated using [post-IR] OSL signals. The results of an anomalous fading test of the two types of OSL signals revealed that the [post-IR] OSL signals from the etched sub-sample (by H₂SiF₆ and HF) and the un-etched sub-sample did not fade significantly. However, the IRSL signals from the un-etched sub-sample showed obvious signs of fading. These findings indicate that the lower age estimated by IRSL is due to the anomalous fading of feldspar IR signals in the polymineral fine grains. For samples collected from greater than 100 cm, the estimates of their OSL ages using two types of luminescence signals generally agreed with their pre-estimated ages, especially those of the [post-IR] OSL signals. However, for the three samples that were collected from a depth of less than 100 cm, their OSL ages were remarkably underestimated, possibly due to the enhanced human activity (such as soil cultivation) that has occurred in the region since 3000 a B.P.     

光释光测年法——综述及进展

光释光(OSL)测年是对沉积物最后一次曝光(或热)事件年代的测定,其测试对象主要为石英和长石。自20世纪80年代该方法提出以来,在国内外得到了广泛的应用。但国内不少地学工作者对该技术的原理与测年方式了解十分有限,为了使应用者能更好、更全面地了解和使用这一方法,对OSL测年法及其近年来的国内外主要研究进展进行了回顾,重点对OSL测年法的基本原理、样品采集及实验室前处理过程、等效剂量(De)值的测定方式、环境剂量率的计算,以及影响测年结果可靠性的重要因素等进行了全面介绍、分析和探讨。同时,对近年来国内外关于De值测定方法与技术上的进展及已经获得较可信年龄的相关方法等进行了总结分析,并对OSL可能测年的范围和影响结果可靠性的一些潜在因素,以及对获得100ka~1Ma间的年龄新的释光信号研究方法等进行了介绍和探讨。     

Optically Stimulated Luminescence (OSL) dating of glacial sediments from Arctic Russia - depositional bleaching and methodological aspects

Optical dating has been extensively used for stratigraphical correlation in the reconstruction of Eurasian ice-sheet dynamics and palaeoenvironmental changes during the last glaciation. In recent terrestrial studies in Arctic Russia, Optically Stimulated Luminescence (OSL) is the main chronological tool, and has been used across the whole of the Eurasian north. We report new OSL ages obtained on glaciofluvial and glaciolacustrine sediments from the Arkhangelsk and Taymyr regions of Arctic Russia and discuss the characteristics of the quartz OSL signal in terms of its saturation limit, variability among samples from the same location, and initial signal resetting in different depositional environments. It is shown that effect of partial bleaching in our mainly Weichselian samples is trivial because: modern analogues are well zeroed; there is good agreement between OSL and ¹⁴C ages in young samples; and skewness in the dose distribution of relatively older samples is mainly due to varying shapes of the growth curves. The overall reliability of the OSL ages from Arctic Russia, when compared with the limited independent age controls available, appears to be good.     

Chronologies of sedimentary changes in the south Bohai Sea,China: constraints from luminescence and radiocarbon dating

The alternation of terrestrial and marine deposits is an indicator of past environmental and sea‐level changes. The age of deposition is usually dated by means of radiocarbon. However, radiocarbon dates of molluscan shells from coastal areas may be complicated by various sources of carbon, and problematic for deposits of 40–50 ka or older. Herein, we apply the Optically Stimulated Luminescence (OSL) dating method to date samples from terrestrial and marine/coastal sediments extracted from three cores in the south Bohai Sea, China. Multiple‐ and single‐aliquot regenerative‐dose procedures using OSL signals from fine‐silt (4–11 μm), coarse‐silt (38–63 μm) and fine‐sand (63–90 or 90–125 μm) quartz were employed to determine the equivalent dose (D _e). The results showed that: (i) OSL ages from quartz of different grain sizes and different protocols are consistent with each other; (ii) for Holocene samples, most of the radiocarbon dates agree well with OSL ages; (iii) for pre‐Holocene samples, radiocarbon dates cluster at 40–50 ¹⁴ C ka BP, whereas OSL ages are in stratigraphic order from 11 ka to 176 ka. Because of the self‐consistency of the quartz OSL ages, the stratigraphic agreement in the three cores, and the clustering of the radiocarbon dates, we suggest that the quartz OSL ages are more reliable with respect to dating the samples from the south Bohai Sea. Finally, the four marine strata identified in the south Bohai Sea are likely to have formed during the Holocene, Marine Isotopic Stage (MIS) 3–5, MIS 6 and probably MIS 7, respectively.     

OSL signal resetting in young deposits determined with a pulsed photon‐stimulated luminescence (PPSL) unit

Optical Stimulated Luminescence (OSL) is a technique that can be used for dating geological materials deposited within the last half‐million years, including sediments transported by air, water or gravity, as well as rocks heated at high temperatures. Recently, several studies have shown that OSL can also provide information on sediment transport. The pulsed photon‐stimulated luminescence (PPSL) unit (also known as a portable OSL reader) developed by the Scottish Universities Environmental Research Centre is an instrument designed to read luminescence signals from bulk (untreated) sediment samples comprising poly‐mineral and poly‐grain fractions. In this contribution, we evaluate the potential of the PPSL unit to assess the degree of OSL signal resetting in 27 young deposits (<2 ka) transported by different geomorphic agents in volcanic, coastal and fluvial depositional settings located in Mexico. Our results are in agreement with previous findings that used the Risø TL/OSL reader, confirming that sediments transported by debrisflows contain the highest inherited luminesce signals. Infrared stimulation (IRSL) values in volcanic ash, lavas, and sand beach and dune deposits exhibit low scatter. However, with blue stimulation (BLSL) these samples reveal a large degree of scattering, attributed to charge transfer in the case of the coastal deposits and to the low sensitivity of quartz in the case of volcanic material. The luminescence signals of fluvial sediments exhibit a highly scattered distribution in both IRSL and BLSL. We conclude that the use of a PPSL unit is a simple approach to assess the degree of OSL signal resetting in deposits sourced from different geological environments. This research contributes to previous studies that have investigated new applications of the PPSL unit to assist in OSL dating of geological materials.     

A robust feldspar luminescence dating method for Middle and Late Pleistocene sediments

Luminescence dating is used extensively to provide absolute chronologies for Late Pleistocene sediments. Nowadays, most optical dates are based on quartz optically stimulated luminescence (OSL). However, the application of this signal is usually limited to the last ～100 ka because of saturation of the quartz luminescence signal with dose. In contrast, the feldspar infrared stimulated luminescence (IRSL) dose–response curve grows to much higher doses; this has the potential to extend the datable age range by a factor of 4–5 compared with quartz OSL. However, it has been known for several decades that this IRSL signal is unstable, and this instability often gives rise to significant age underestimation. Here we test against independent age control the recently developed feldspar post‐IR IRSL approach to the dating of sediments, which appears to avoid signal instability. A physical model explaining our observations is discussed, and the method is shown to be accurate back to 600 ka. The post‐IR IRSL signal is reduced by exposure to daylight more slowly than that from quartz and low‐temperature IRSL, preventing its general application to young (e.g. Holocene) sediments. Nevertheless, this new approach is widely applicable (feldspar of appropriate luminescence behaviour is even more ubiquitous than quartz). These characteristics make this a method of great importance for the dating of Middle and Late Pleistocene deposits.     

Is X‐ray core scanning non‐destructive? Assessing the implications for optically stimulated luminescence (OSL) dating of sediments

Optically stimulated luminescence (OSL) dating is widely used to date clastic deposits, including those collected by coring. X‐ray scanning of cores has become popular because of the rapidly acquired, high‐resolution information it gives about optical, radiographic and elemental variations. Additionally, X‐ray scanning is widely viewed as a non‐destructive method. However, such instruments use an intense X‐ray beam that irradiates the split core to enable both X‐radiographic and X‐ray fluorescence (XRF) analysis. This irradiation will influence the optically stimulated luminescence signal in the sediments. This study determines the radiation dose delivered to sediments in a core during an X‐ray scan, and assesses the implications for studies wishing to combine X‐ray scanning and OSL dating. Copyright © 2009 John Wiley & Sons, Ltd.     

Establishing the Late Pleistocene-Holocene sedimentation boundary in the southern North Sea using OSL dating of shallow continental shelf sediments

This paper provides insight into the fate of Late Weichselian and Early Holocene sediments accumulated in the German sector of the southern North Sea. A combination of optically stimulated luminescence (OSL) dating and radiocarbon dating was applied to set up the chronology. Seven cores were studied to obtain ten quartz OSL samples and ten radiocarbon samples. The core locations were chosen along a southeast to northwest transect along the western side of the Elbe palaeovalley, giving a good coverage of the entire German North Sea area. All samples for OSL dating showed a significant scatter in the equivalent dose (D_e) distribution of quartz due to heterogeneous bleaching. The Minimum Age Model (MAM-3) was found to be the most suitable to extract true burial ages. It was inferred from the study that sedimentation did still occur during the late deglaciation period in many areas. These are mainly Late Weichselian glaciofluvial or glaciolacustrine sediments directly overlain by early Holocene fluvial and/or transgressive deposits and followed by modern marine sands. However, considerable late Weichselian erosion or a possible period of non-deposition was observed in the highland area to the northeast of the Dogger Bank and a small discontinuity in the near-shore region was noticed, probably due to early Holocene fluvial erosion. Relicts of a palaeo-river bank or terrace were identified in core 14VC to the east of the Dogger Bank. A possible interpretation of the Pleistocene-Holocene interface along the core transect is provided based on lithology and measured OSL and radiocarbon ages.     

OSL Age Determination of Archaeological Stone Structures Using Trapped Aeolian Sediments: A Case Study from the Negev Highlands,Israel

Optically stimulated luminescence (OSL) dating is widely applied to sediments in paleoenvironmental sciences. However, there are only limited examples determining the age of archaeological stone structures by OSL using dust deposits. The age of dust deposits associated with ancient buildings may be used to date the onset of settlement (sediment below structures), settlement activity (occupation layer), or the time after a settlement had been abandoned or destroyed (sediment between collapsed roofs and walls). In this study, OSL dating is applied to establish numerical dates for settlement structures situated in the Negev Highlands, Israel. Two archaeological sites are investigated to identify their occupation history, by dating nine samples of aeolian dust trapped within the remains of ancient buildings. The OSL dating technique is applied using coarse grain quartz and a standard single‐aliquot regenerative‐dose (SAR) protocol. It was possible to date the onset of sedimentation in a later phase of the human occupation or shortly after the sites were abandoned, to 3.7 ± 0.3 ka (Intermediate Bronze Age) at the central site and to 2.7 ± 0.2 ka (Iron Age) at the ephemeral site. These results are supported by archaeological evidence gained from pottery finds and the architecture of the ancient buildings.     

Testing optically stimulated luminescence dating on sand-sized quartz of deltaic deposits from the Sperchios delta plain,central Greece

This study reports on the first investigation into the potential of luminescence dating to establish a chronological framework for the depositional sequences of the Sperchios delta plain, central Greece. A series of three borehole cores(20 m deep) and two shallow cores(4 m deep), from across the delta plain, were extracted, and samples were collected for luminescence dating. The luminescence ages of sand-sized quartz grains were obtained from small aliquots of quartz, using the Single-Aliquot Regenerative-dose(SAR) protocol.The equivalent dose determination included a series of tests and the selection of the Minimum Age Model(MAM) as the most appropriate statistical model. This made it possible to confirm the applicability of quartz Optically Stimulated Luminescence(OSL) dating to establish absolute chronology for deltaic sediments from the Sperchios delta plain.Testing age results of the five cores showed that the deltaic sediments were deposited during the Holocene.A relatively rapid deposition is implied for the top ~14 m possibly as a result of the deceleration in the rate of the sea-level rise and the transition to terrestrial conditions, while on the deeper parts, the reduced sedimentation rate may indicate a lagoonal or coastal environment.     

Optically Stimulated Luminescence (OSL) dating of sand‐filled wedge structures and their fine‐grained host sediment from Jonzac,SW France

Two sand wedge structures and their host sediments, from Jonzac in SW France, were successfully dated using Optically Stimulated Luminescence (OSL) measurements on both small aliquots and single grains of quartz from the 180–212 μm size fraction. One of the sand wedges clearly contains primary infilling. However, grain‐size analysis and field observations do not clearly indicate whether the other feature represents a primary sand wedge or a composite sand wedge with primary and secondary infilling. OSL results and the geological setting justify using the Central Age Model (CAM) for the calculation of age estimates. Grain‐size analysis and detailed investigations of OSL results revealed the contamination of one sand wedge sample with host sediment. However, age calculation using the Finite Mixture Model (FMM) provided what is considered to be a reliable age estimate for the contaminated sample. The age estimates for all samples correspond to Marine Isotope Stage (MIS) 3. While fine‐grained sediments were deposited in the middle of MIS 3 (c. 43–55 ka), the sand wedges unexpectedly correspond to the end of this period (c. 33 ka) or the onset of MIS 2 (c. 27 ka). The sand wedges were probably formed during intense but short cold periods, possibly correlated with a Heinrich event (H2 and/or H3). The results help us to assess how effective luminescence dating is on sand wedges and the limitations involved in correlating sand wedge ages with Heinrich events, and contribute to the debate on the timing of cryogenic formation processes and the permafrost distribution in SW France.     

Luminescence dating of Middle Pleistocene proglacial deposits from northern Switzerland: methodological aspects and stratigraphical conclusions

Optically stimulated luminescence (OSL) dating was applied to proglacial deposits from the Klettgau Valley in northern Switzerland, which is understood to record several phases of glaciation prior to the Last Interglacial. The aim was to provide an independent chronology for the different sedimentary units to understand better the complex depositional history of the region. This time range requires care when assessing the reliability of the luminescence protocols applied. Equivalent doses for fine‐ and coarse‐grain quartz remained below 300 Gy, while dose response curves for both fractions continued to display growth above 500 Gy. Dose recovery tests confirmed the ability of the single aliquot regenerative (SAR) protocol to recover laboratory doses of a similar size to burial doses, and isothermal decay measurements confirmed the stability of the quartz signal. Having passed rigorous testing criteria, quartz OSL ages of up to ～200 ka were considered reliable but significantly underestimated expected ages and prompt a reconsideration of earlier interpretations of the stratigraphy for this site. Rather than representing three separate glaciations, quartz luminescence ages instead suggest that these deposits record up to four independent ice advances during Marine Isotope Stage 6. For both single grain and single aliquot feldspar dating, it was not possible to separate the conflicting influences of anomalous fading and partial bleaching. However, uncorrected feldspar central age model ages were found to be in reasonable agreement with quartz age estimates, and suggest that feldspar ages may still offer useful additional information in this region.     

Exploring the method of optical dating and comparison of optical and 14C ages of Late Weichselian coversands in the southern Netherlands

A study was made of the applicability of three different techniques for equivalent dose (D_e) determination in the optical dating of quartz: the single‐aliquot regenerative‐dose technique (SAR), the single‐aliquot additive‐dose technique (SAAD) and the multiple‐aliquot additive‐dose technique (MAAD). For this purpose, quartz grains were extracted from a sequence of Upper Pleniglacial to Late‐glacial coversands exposed at the locality of Ossendrecht in the southwestern Netherlands, a site for which both radiocarbon and earlier luminescence dates are available, providing independent age control. Upon testing the different assumptions underlying each of the three OSL techniques investigated, the SAR protocol was found to be the technique of choice. The optical ages obtained with this protocol were in good agreement with the chronostratigraphical position of the sediments investigated and with the available chronostratigraphical information on the same and equivalent deposits. This confirms the suitability of the SAR technique for dating coversands. Furthermore, a small laboratory intercomparison of SAR‐based D_e determinations yielded results that were in fair overall agreement. Copyright © 2004 John Wiley & Sons, Ltd.     

Apparent OSL ages of modern deposits from Fåbergstølsdalen,Norway: implications for sampling glacial sediments

The application of optically stimulated luminescence (OSL) dating within glacial settings can be limited where sediments have not had their OSL signal fully reset by sunlight exposure. Heterogeneous bleaching can result in age overestimations, and although it is recognized that certain depositional settings are more likely to have experienced sufficient sunlight exposure to bleach the OSL signal, no comprehensive study has empirically investigated the processes of sediment bleaching, or the variability in bleaching between deposits of the same type and within the same glacial catchment. A suite of modern glacial and glaciofluvial sediments from Fåbergstølsdalen, southern Norway, have been analysed to explore the controls that sedimentary processes and depositional setting have on bleaching of the OSL signal of quartz. There is considerable variability in the residual OSL ages of similar modern deposits, which reflects high sensitivity of the OSL signal to sediment source, sedimentary process, transport distance and depositional setting. Overdispersion values are greatest for the sediments which have been most heterogeneously bleached and these sediments have the lowest residual ages. Sampling strategies that incorporate sufficient consideration of the depositional framework of sample settings can minimize the effects of unbleached residuals on OSL age determinations.     

Infrared stimulated luminescence dating of an Eemian (MIS 5e) site in Denmark using K‐feldspar

Buylaert, J.‐P., Huot, S., Murray, A.S. & Van den haute, P.: Infrared stimulated luminescence dating of an Eemian (MIS 5e) site in Denmark using K‐feldspar. Boreas, 10.1111/j.1502‐3885.2010.00156.x. ISSN 0300‐9483. Infrared stimulated luminescence (IRSL) dating of K‐feldspars may be an alternative to quartz optically stimulated luminescence (OSL) dating when the quartz OSL signal is too close to saturation or when the quartz luminescence characteristics are unsuitable. In this paper, Eemian (MIS 5e) coastal marine sands exposed in a cliff section on the coast of southern Jutland (Denmark) are used to test the accuracy and precision of IRSL dating using K‐feldspars. This material has been used previously to test quartz OSL dating ( Murray & Funder 2003 ): a small systematic underestimation of <10% compared to the expected age of ～130 ka was reported. In our study, a single‐aliquot regenerative‐dose (SAR) IRSL protocol is used to determine values of equivalent dose (D_e) and the corresponding fading rates (g values). A significant age underestimation (of up to ～35%) is observed; this is attributed to anomalous fading. Using a single site‐average fading rate of 3.66 ± 0.09%/decade to correct the IRSL ages for all samples provides good agreement between the average fading‐corrected K‐feldspar age (119 ± 6 ka) and the independent age control (132–125 ka). This is despite the reservations of Huntley & Lamothe (2001) that their fading correction method is not expected to work on samples older than ～20–50 ka. This fading‐corrected feldspar result is not significantly different from the overall revised quartz age (114 ± 7 ka) also presented here. We conclude that fading‐corrected IRSL ages measured using K‐feldspar may be both precise and accurate over a greater age range than might be otherwise expected.     

博斯腾湖湖泊沉积物光释光年代测量*

使用光释光年代学的单片再生法测量了博斯腾湖沉积剖面中碳酸盐泥及粉砂质泥底部的浅湖相灰色粉细砂和风成沙的年龄,对剖面上部碳酸盐层中陆生植物残体进行了AMS ¹⁴ C测年。通过不同测片的等效剂量(D_e)值的分布状况评价了样品的晒褪程度,选择不随灵敏度校正后的自然释光信号变化的相对集中的等效剂量(D_e)值计算了样品的埋藏年龄。通过这些年龄结果的对比,发现石英矿物的OSL年龄和AMS ¹⁴ C年龄在地层上是一致的,表明尽管在浅湖相细砂中存在不完全晒褪,但根据相对较小而集中的D_e值计算得到的年龄结果是可靠的。这些年龄结果和地层资料揭示末次冰消期以来至早全新世,博斯腾湖处于无水干盆地向深水湖泊转化的浅水湖泊状态,现代深水博斯腾湖大约形成于距今8ka前后。