CHIME age dating of monazites from metamorphic rocks and granitic rocks of the Ryoke belt in the Iwakuni area, Southwest Japan

Abstract CHIME (chemical Th-U-total Pb isochron method) ages were determined for monazite from gneisses and granitoids of the Ryoke belt in the Iwakuni area. The CHIME monazite ages are 99.6 ± 2.4, 98.9 ± 2.1 and 98.2 ± 5.7 Ma for the Ryoke gneiss, 90.7 ± 2.2, 89.7 ± 2.0 and 89.3 ± 2.2 Ma for the Tajiri Granite, 91.0 ± 3.2, 90.6 ± 3.2 and 89.9 ± 3.2 Ma for the Namera Granite, 89.3 ±3.3 and 88.6 ± 5.6 Ma for a small stock at Shimizu, and 87.3 ± 1.6 and 86.6 ± 2.1 Ma for the post-tectonic Shimokuhara Granite. The CHIME monazite ages, interpreted as the time of the first attainment at the amphibolite facies conditions for the gneisses and as the time of emplacement for the granites, respectively, agree with the field intrusive sequence. The present dating documented that the Ryoke metamorphism in the Iwakuni area reached the amphibolite facies conditions at ∼98 Ma, was complete at -87 Ma, the time of emplacement of the post-tectonic Shimokuhara Granite.     

A high‐T metamorphic complex derived from the high‐P Suo metamorphic complex in the Omuta district,northern Kyushu,southwest Japan

New U–Pb ages of zircons from migmatitic pelitic gneisses in the Omuta district, northern Kyushu, southwest Japan are presented. Metamorphic zonation from the Suo metamorphic complex to the gneisses suggests that the protolith of the gneisses was the Suo metamorphic complex. The zircon ages reveal the following: (i) a transformation took place from the high‐P Suo metamorphic complex to a high‐T metamorphic complex that includes the migmatitic pelitic gneisses; (ii) the detrital zircon cores in the Suo pelitic rocks have two main age components (ca 1900–1800 Ma and 250 Ma), with some of the detrital zircon cores being supplied (being reworked) from a high‐grade metamorphic source; and (iii) one metamorphic zircon rim yields 105.1 ±5.3 Ma concordant age that represents the age of the high‐T metamorphism. The high‐P to high‐T transformation of metamorphic complexes implies the seaward shift of a volcanic arc or a landward shift of the metamorphic complex from a trench to the sides of a volcanic arc in an arc–trench system during the Early Cretaceous. The Omuta district is located on the same geographical trend as the Ryoke plutono‐metamorphic complex, and our estimated age of the high‐T metamorphism is similar to that of the Ryoke plutono‐metamorphism in the Yanai district of western Chugoku. Therefore, the high‐T metamorphic complex possibly represents the western extension of the Ryoke plutono‐metamorphic complex. The protolith of the metamorphic rocks of the Ryoke plutono‐metamorphic complex was the Jurassic accretionary complex of the inner zone of southwest Japan. The high‐P to high‐T transformation in the Omuta district also suggests that the geographic trend of the Jurassic accretionary complex was oblique to that of the mid‐Cretaceous high‐T metamorphic field.     

Metamorphic condition of a regional metamorphic complex in the Omuta district in northern Kyushu,southwest Japan

A high‐temperature (T) metamorphic complex occurs in the Omuta district, northern Kyushu, Japan. Three metamorphic zones are defined based on pelitic mineral assemblage, i.e. chlorite–biotite zone, muscovite–andalusite zone and sillimanite–K‐feldspar zone with ascending metamorphic grade from north to south. Two isograds trend approximately east–west, which is oblique to the boundary between the metamorphic complex and the Tamana Granodiorite located on the southeast. The metamorphic condition of two pelitic rocks that occur in the muscovite–andalusite zone and sillimanite–K‐feldspar zone are estimated as 510 ±30 °C, 300 ±60 MPa and 720 ±30 °C, 620 ±60 MPa, respectively. Thermodynamic consideration reveals that use of the same geothermobarometer enables precise determination of the difference in pressure between the samples as 320 ±10 MPa. This indicates that the pelitic samples were metamorphosed at different depth by 11–12 km that is significantly larger than the geographic distance of 6.8 km between the sample localities. This also suggests that crustal thinning took place after the high‐T metamorphism. The high‐T metamorphic complex is, therefore, not of static contact metamorphism but of dynamic regional metamorphism. The present result combined with petrological and chronological similarities implies that this complex suffered the regional Ryoke metamorphism.     

Regional-Scale Excess Ar wave in a Barrovian type metamorphic belt, eastern Tibetan Plateau

Laser step heating ⁴⁰Ar/³⁹Ar analysis of biotite and muscovite single crystals from a Barrovian type metamorphic belt in the eastern Tibetan plateau yielded consistent cooling ages of ca. 40 Ma in the sillimanite zone with peak metamorphic temperatures higher than 600°C and discordant ages from 46 to 197 Ma in the zones with lower peak temperatures. Chemical Th‐U‐Total Pb Isochron Method (CHIME) monazite (65 Ma) and sensitive high mass‐resolution ion microprobe (SHRIMP) apatite (67 Ma) dating give the age of peak metamorphism in the sillimanite zone. Moderate amounts of excess Ar shown by biotite grains with ages of 46 to 94 Ma at metamorphic grades up to the high‐grade part of the kyanite zone probably represent incomplete degassing during metamorphism. In contrast, the high‐grade part of the kyanite zone yields biotite ages of 130 to 197 Ma. The spatial distribution of these older ages in the kyanite zone along the sillimanite zone boundary suggests they reflect trapped excess argon that migrated from higher‐grade regions. The most likely source is muscovite that decomposed to form sillimanite. The zone with extreme amounts of excess argon preserves trapped remnants of an ‘excess argon wave’. We suggest this corresponds to the area where biotite cooled below its closure temperature in the presence of an elevated Ar wave. Extreme excess Ar is not recognized in muscovite suggesting that the entrapment of the argon wave by biotite took place when the rocks had cooled down to temperatures lower than the closure temperature of muscovite. The breakdown of phengite during ultrahigh‐pressure (UHP) metamorphism may be a key factor in accounting for the very old apparent ages seen in many UHP metamorphic regions. This is the first documentation of a regional Ar‐wave spatially associated with regional metamorphism. This study also implies that resetting of the Ar isotopic systems in micas can require temperatures up to 600°C; much higher than generally thought.     

Zircon U–Pb sensitive high mass-resolution ion microprobe dating of granitoids in the Ryoke metamorphic belt, Kinki District, Southwest Japan

Abstract Zircon U–Pb sensitive high mass-resolution ion microprobe dating was carried out on three types of granitic rock (gneissose biotite granodiorite, biotite granite and two-mica granite) from the Cretaceous Ryoke belt of the Kinki district, Southwest Japan. The results give the ages of granitic magmatism in the Shigi-san area of between 87 and 78 Ma and suggest extensive melting of the Cretaceous Ryoke granitic crust to form the two-mica granite, probably at ca 80 Ma. Discrimination into older and younger granites based on development of gneissosity does not appear to represent the sequence of magma generation, although there is some scope in the interpretation of the zircon U–Pb data that would allow all three granites to form at 83 Ma. Compilation of chemical Th-U-total Pb isochron dating method ages, whole rock Rb–Sr isotope ages and U–Pb isotope ages indicates that most Ryoke plutonism occurred from ca 70 Ma to ca 100 Ma. Younger (85 Ma–70 Ma) plutonism with the formation of two-mica granite occurred only in the eastern sector of the Ryoke belt, including the Kinki District.     

The chemical Th-U-total Pb isochron ages of Jiaodong and Jiaonan metamorphic rocks in the Shandong Peninsula, eastern China

Abstract The chemical Th-U-total Pb isochron method (CHIME) was applied to determine the age of monazite and thorite in five gneisses and zircon in an ultra high-pressure (UHP) phengite schist from the Su-Lu region, eastern China. The CHIME ages and isotopic ages reported in the literature show that gneisses in the Su-Lu region are divided into middle Proterozoic (1500–1720 Ma) and Mesozoic (100–250 Ma) groups. The Proterozoic group includes paragneiss and orthogneiss of the amphibolite-granulite facies, and their protolith age is late Archean-early Proterozoic. The Mesozoic group is mainly composed of orthogneiss of the greenschist-epidote amphibolite facies, and the protolith age is Middle Paleozoic-Early Proterozoic. The Proterozoic and Mesozoic gneisses occupy northern and southern areas of the Su-Lu region, respectively, which are divided by a major Wulian-Qingdao-Yantai fault. Ultra high-pressure metamorphic rocks occur as blocks in the Mesozoic gneisses, and form a UHP complex.
The UHP phengite schist in the Mesozoic orthogneiss contains detrital zircons with late Proterozoic CHIME age ( ca 860 Ma). Age of the UHP metamorphism is late Proterozoic or younger, and protolith age of the UHP metamorphic rocks is probably different from that of the surrounding Mesozoic gneisses.     

Age gap between the intrusion of gneissose granitoids and regional high‐temperature metamorphism in the Ryoke belt (Mikawa area), central Japan

The relationships between the intrusion of gneissose granitoids and the attainment of regional high‐T conditions recorded in metamorphic rocks from the Ryoke belt of the Mikawa area, central Japan, are explored. Seven gneissose granitoid samples (tonalite, granodiorite, granite) were collected from three distinct plutonic bodies that are mapped as the so‐called “Older Ryoke granitoids.” Based on bulk‐rock compositions and U–Pb zircon ages obtained by laser ablation inductively coupled plasma mass spectrometry, the analyzed granitoids can be separated into two groups. Gneissose granitoids from the northern part of the area give weighted mean ²⁰⁶Pb/²³⁸U ages of 99 ±1 Ma (two samples) and 95 ±1 Ma (one sample), whereas those from the southern part yield 81 ±1 Ma (two samples) and 78–77 ±1 Ma (two samples). Regional comparisons allow correlation of the northern granitoids (99–95 Ma) with the Kiyosaki granodiorite, and mostly with the Kamihara tonalite found to the east. The southern granitoids are tentatively renamed as “78–75 Ma (Hbl)?Bt granite” and “81–75 Ma Hbl?Bt tonalite” (Hbl, hornblende; Bt, biotite). and seem to be broadly coeval members of the same magmatic suite. With respect to available age data, no gneissose granitoid from the Mikawa area shows a U–Pb zircon age which matches that of high‐T metamorphism (ca 87 Ma). The southern gneissose granitoids (81–75 Ma), although they occur in the highest‐grade metamorphic zone, do not seem to represent the heat source which produced the metamorphic field gradient with a low dP/dT slope.     

Microstructurally controlled monazite chronology of ultrahigh-temperature granulites from southern India: Implications for the timing of Gondwana assembly

Ultrahigh‐temperature (UHT) granulite facies rocks from the Achankovil Shear Zone area and the southern domain of the Madurai Granulite Block in South India contain monazite useful for in situ microprobe U–Pb dating. The UHT rocks examined consist of garnet + cordierite (retrograde) + quartz + mesoperthite + biotite + plagioclase + Fe‐Ti oxides ± orthopyroxene ± sillimanite and accessory zircon and monazite. Sillimanite occurs only as inclusions in garnet. Microstructural observations suggest garnet, orthopyroxene, spinel and mesoperthite are products of peak metamorphism. Post‐peak formation of cordierite ± orthopyroxene ± quartz and cordierite + spinel + Fe‐Ti oxides assemblages is also observed. Geothermobarometry on orthopyroxene and garnet‐orthopyroxene bearing assemblages suggest peak UHT conditions of T = 940–1040°C and P = 8.5–9.5 kbar. This was followed by a retrograde stage of 3.5–4.5 kbar and 720 ± 60°C, estimated from garnet‐cordierite assemblages. A small population of rounded, probably detrital, monazites in these rocks yield ages from Meso‐ to Neoproterozoic indicating a heterogeneous source. The youngest associated spot ages are 660–600 Ma suggesting protolith deposition up to ca 600 Ma. In contrast, the vast majority of monazites that crystallized during the latest metamorphic event show late Neoproterozoic to Cambrian ages. Probability‐density plots of monazite age data show a ‘peak’ between 533 and 565 Ma, but this peak need not reflect a particular thermal event. Collating ages from homogenous metamorphic monazites associated with minerals stable at peak P‐T conditions suggests peak metamorphism in these rocks occurred at 580–600 Ma. Together with a re‐evaluation of available data from adjacent granulite blocks in southern India, these data suggest the main metamorphic event coinciding with the suturing of India with the Gondwana amalgam probably occurred 580–600 Ma. The 500–550 Ma ages commonly reported in previous studies might represent post‐peak thermal events.     

Rb–Sr isochron ages of the Cretaceous granitoids in the Ryoke belt, Kinki district, Southwest Japan

Abstract Granitoids are widely distributed in the Ryoke belt and have been divided into four main igneous stages based on their field setting. In this paper, we present Rb–Sr isochron ages for the younger Ryoke granitoids (second stage to fourth stage) in the Kinki district. The Yagyu granite (second stage) gave a Rb–Sr whole‐rock isochron age of 74.6 ± 10.9 Ma with an initial ⁸⁷Sr/⁸⁶Sr ratio of 0.70938 ± 0.00016, and a Rb–Sr mineral isochron age of 71.8 ± 0.1 Ma. The Narukawa granite (second stage) yielded a Rb–Sr mineral isochron age of 79.5 ± 0.4 Ma. A Rb–Sr whole‐rock isochron age of 78.3 ± 3.0 Ma with an initial ⁸⁷Sr/⁸⁶Sr ratio of 0.70764 ± 0.00014 was obtained for the Takijiri adamellite (third stage). The Katsuragi quartzdiorite (fourth stage) gave a Rb–Sr whole‐rock isochron age of 85.1 ± 18.3 Ma (initial ⁸⁷Sr/⁸⁶Sr ratio of 0.70728 ± 0.00006), and mineral isochron ages of 76.9 ± 0.5 Ma and 74.8 ± 0.5 Ma. The Minamikawachi granite (fourth stage) gave a Rb–Sr whole‐rock isochron age of 72.8 ± 2.0 Ma with an initial ⁸⁷Sr/⁸⁶Sr ratio of 0.70891 ± 0.00021. These age data indicate that the igneous activity in younger Ryoke granitoids of Kinki district occurred between 80 and 70 Ma, except for the Katsuragi quartz diorite. The isotopic data on the various igneous stages in Kinki district correspond with the relative timing from field observations. Based on the initial ⁸⁷Sr/⁸⁶Sr ratios, the granitoids of the Ryoke belt in Kinki district are spatially divided into two groups. One is granitoids with initial ⁸⁷Sr/⁸⁶Sr ratio of 0.707–0.708, distributed in the southern part of the Ryoke belt. The other is granitoids with initial ⁸⁷Sr/⁸⁶Sr ratio of 0.708–0.710 distributed in the northern part of the Ryoke belt. The initial ⁸⁷Sr/⁸⁶Sr ratios of granitoids increase with decreasing (becoming younger) Rb–Sr whole‐rock isochron ages.     

Cretaceous granitoids and their zircon U–Pb ages across the south‐central part of the Abukuma Highland,Japan

Zircons separated from Cretaceous granitoids are dated from a south‐central transect of the Abukuma metamorphic and granitic terrane. The zircon ages do not follow ‘older’ and ‘younger’ granitoid ages that are used conventionally. In the western part of the study area (Zones I, II and III) where the Takanuki and Gosaisho metamorphic rocks are exposed, the Iritono quartz dioritic stock intruding the greenschist facies rocks in Zone III exhibits the oldest age of 121 Ma in the studied region. Quartz diorite located northward shows 112 Ma, but the other four granitoids intruding into the Takanuki and Gosaisho metamorphic rocks are younger and 103–99 Ma. Two‐mica and biotite granites belong to the youngest age group of 99 Ma. The granitic activities of both the Abukuma and Ryoke belts were initiated by intrusion of quartz dioritic magmas and were ended by two‐mica granite activity. The ages of the eastern two batholiths vary from 110 to 106 Ma (four samples), and show no age common to the Kitakami granitoids farther to the north. Throughout the Japanese Islands arc, Cretaceous granitic activities became younger toward the marginal sea side from the Kitakami Mountains, to the Abukuma Highland, and the Ryoke Belt, then to the Sanin belt of the Inner Zone of Southwest Japan.     

Sm–Nd, Rb–Sr and K–Ar geochronology of the Higo metamorphic terrane, west-central Kyushu, Japan

The Higo metamorphic terrane situated in west-central Kyushu island, southwest Japan, is composed of greenschist- to granulite-facies metamorphic rocks. The southern part of the metamorphic terrane consists mainly of garnet–biotite gneiss and garnet–cordierite–biotite gneiss, and orthopyroxene or cordierite-bearing S-type tonalite with subordinate amounts of hornblende gabbro. Rb–Sr, Sm–Nd and K–Ar isotopic ages for these rocks have been determined here. The garnet–biotite gneiss gives an Sm–Nd age of 227.1 ± 4.9 Ma and a Rb–Sr age of 101.0 ± 1.0 Ma. The hornblende gabbro has an Sm–Nd age of 257.9 ± 2.5 Ma and a K–Ar age of 103.4 ± 1.1 Ma. These age differences of the same samples are due to the difference in the closure temperature for each system and minerals. The garnet-cordierite–biotite gneiss contains coarse-grained garnet with a zonal structure conspicuously distinguished in color difference (core: dark red; rim: pink). Sm–Nd internal isochrons of the garnet core and the rim give ages of 278.8 ± 4.9 Ma (initial ¹⁴³Nd/¹⁴⁴Nd ratio = 0.512311 ± 0.000005) and 226.1 ± 28.4 Ma (0.512277 ± 0.000038), respectively. These ages are close to formation of the garnet core and the rim. It has been previously suggested that the Higo metamorphic terrane belongs to the Ryoke metamorphic belt. But Sr and Nd isotopic features of the rocks from the former are different from those of the Ryoke metamorphic rocks, and are similar to those of the granulite xenoliths contained in the Ryoke younger granite.     

New SHRIMP U–Pb zircon ages of granitic rocks in the Hida Belt,Japan: Implications for tectonic correlation with Jiamushi massif

Granitoids in the Hida region of Japan encompass two main rock types: younger type‐1 granites and older type‐2 granites. Sensitive high mass‐resolution ion microprobe (SHRIMP) U–Pb zircon dating of older type‐2 granites collected from the Tateyama area show similar ages of 245 ± 2 Ma and 248 ± 5 Ma for two gneissose granites, while a significantly younger intrusion age of 197 ± 3 Ma was determined for the younger type‐1 granites collected from the Hayatsukigawa River which belongs to the Okumayama pluton. A felsic gneiss sample (07HI‐3) collected from the right bank of the Hayatsukigawa River yielded multiple complex ages at 330 ± 6 Ma, indicating the timing of the Hida regional tectono‐thermal events that formed the Hida gneisses; 243 ± 8 Ma, representing the timing of intrusion of the augen granite; and 220 Ma, indicating the timing of regional dextral ductile shearing that caused a repeated recrystallization of metamorphic rocks in the study area. Considering the geochronological data, the rock types and assemblages, basement, and Sr–Nd isotopic constraints, we propose that the Hida Belt separated from the Jiamushi massif, which is located in the eastern margin of the Central Asian Orogenic Belt.     

Thermal evolution of the Ryoke metamorphic belt, southwestern Japan: Tectonic and numerical modeling

Abstract The Ryoke metamorphic belt of southwestern Japan is composed of Cretaceous Ryoke granitoids and associated metamorphic rocks of low-pressure facies series. The Ryoke granitoids are divided into sheet-like bodies (e.g. Gamano granodiorite) and stock-like bodies. The Gamano granodiorite intruded concordantly into the high-grade metamorphic rocks without development of a contact metamorphic aureole, and the intrusion ages of the granodiorite are similar to the ages of thermal peak of the low pressure (low-P) metamorphism. It is suggested that the low-P Ryoke metamorphism resulted from the intrusion of the Gamano granodiorite. In this study, a simple 1-D numerical model of conductive heat transfer was used to evaluate the thermal effects of emplacement of the Gamano granodiorite. Calculated temperature-time ( T-t ) paths are characterized by a rapid increase of metamorphic temperature and a relatively short-lived period of high temperature. For example, the T-t path at the 15-km depth is characterized by a rapid average increase in temperature of 1.4 × 10-³°C/year and high temperatures for < ca 0.5 Ma. The calculated peak temperature for each depth is nearly equal to the petrologically estimated value for each correlated metamorphic zone. The results suggest that the magma-intrusion model is one possible thermal model for low-pressure facies series metamorphism.     

CHIME monazite ages of metasediments from the Altai orogen in northwestern China: Devonian and Permian ages of metamorphism and their significance

Abstract   The chemical Th-U-total Pb isochron method (CHIME) has been applied to determine the ages of monazite grains from metasediments of greenscshist-amphibolite facies in the Altai orogen, northwest China. The area of distribution of these metamorphic rocks is divided into the Permian (261–268 Ma) central-western and Devonian (377–382 Ma) eastern units on the basis of their metamorphic ages. The Devonian CHIME ages are consistent with the Pb–Pb ages of granitoid in the eastern unit, and support the idea that emplacement of the granitoids was synchronous with regional metamorphism at deep levels. The Permian metamorphic ages (the present study) and igneous ages previously reported from the central-western unit can be interpreted in terms of subduction of crustal material and oceanic plate, and rapid exhumation.     

The petrogenesis and implications of deformed late Caledonian–early Hercynian granites in the Wuyi area,South China

Precambrian basement rocks have been affected by Caledonian thermal metamorphism. Caledonian‐aged zircon grains from Precambrian basement rocks may have resulted from thermal metamorphism. However, Hercynian ages are rarely recorded. Zircon U–Pb Sensitive High Resolution Ion Microprobe (SHRIMP) dating reveals that zircon ages from the Huyan, Lingdou, and Pengkou granitic plutons can be divided into two groups: one group with ages of 398.9 ±5.3 Ma, 399 ±5 Ma, and 410.2 ±5.4 Ma; and a second group with ages of 354 ±11 Ma, 364.6 ±6.7 Ma, and 368 ±14 Ma. The group of zircon U–Pb ages dated at 410–400 Ma represent Caledonian magmatism, whereas the 368–354 Ma ages represent the age of deformation, which produced gneissosity. The three plutons share geochemical characteristics with S‐type granites and belong to the high‐K calc‐alkaline series of peraluminous rocks. They have (⁸⁷Sr/⁸⁶Sr)_i ratios of 0.710 45–0.724 68 and εNd(t) values of ?7.33 to ?10.74, with two‐stage Nd model ages (T_DM2) ranging from 1.84 Ga to 2.10 Ga. Magmatic zircon εHf(t) values range from ?3.79 to ?8.44, and have T_DMC ages of 1.65–1.93 Ga. The data suggest that these granites formed by partial melting of Paleoproterozoic to Mesoproterozoic continental crust. A collision occurred between the Wuyi and Minyue microcontinents within the Cathaysia Block and formed S‐type granite in the southwest Fujian province. The ca 360 Ma zircon U–Pb ages can represent a newly recognized period of deformation which coincided with the formation of the unified Cathaysia Block.     

In situ LA-ICP-MS zircon U-Pb age of ultrahigh-pressure eclogites in the Yukahe area,northern Qaidam Basin

Zircon grains were selected from two types of ultrahigh-pressure (UHP) eclogites, coarse-grained phengite eclogite and fine-grained massive eclogite, in the Yukahe area, the western part of the North Qaidam UHP metamorphic belt. Most zircon grains show typical metamorphic origin with residual cores in some irregular grains and sector, planar or misty internal textures on the cathodoluminescence (CL) images. The contents of REE and HREE of the core parts of grains range from 173 to 1680 μg/g and 170 to 1634 μg/g, respectively, in phengite eclogite, and from 37 to 2640 μg/g and 25.7 to 1824 μg/g, respectively, in massive eclogite. The core parts exhibit HREE-enriched patterns, representing the residual zircons of protolith of the Yukahe eclogite. The contents of REE and HREE of the rim parts and the grains free of residual cores are much lower than those for the core parts. They vary from 13.1 to 89.5 μg/g and 12.5 to 85.7 μg/g, respectively, in phengite eclogite, and from 9.92 to 45.8 μg/g and 9.18 to 43.8 μg/g, respectively, in massive eclogite. Negative Eu anomalies and Th/U ratios decrease from core to rim. Positive Eu anomalies are shown in some grains. These indicate that the presence of garnet and the absence of plagioclase in the peak metamorphic mineral assemblage, and the zircons formed under eclogite facies conditions. LA-ICP-MS zircon U-Pb age data indicate that phengite eclogite and massive eclogite have similar metamorphic age of 436±3Ma and 431±4Ma in the early Paleozoic and magmatic protolith age of 783–793 Ma and 748–759 Ma in the Neo-proterozoic. The weighted mean age of the metamorphic ages (434±2 Ma) may represent the UHP metamorphic age of the Yukahe eclogites. The metamorphic age is well consistent with their direct country rocks of gneisses (431±3 Ma and 432±19 Ma) and coesite-bearing pelitic schist in the Yematan UHP eclogite section (423–440 Ma). These age data together with field observation and lithology, allow us to conclude that the Yukahe eclogites were Neo-proterozoic igneous rocks and may have experienced subduction and UHP metamorphism with continental crust at deep mantle during the early Paleozoic, therefore the metamorphic age of 434±2 Ma of the Yukahe eclogites probably represents the continental deep subduction time in this area.

     

Permian felsic magmatism in the Neoproterozoic Nagar Parkar Igneous Complex of the Malani Igneous Suite: Evidence from zircon U–Pb age

We report Permian (ca. 272 Ma ±5.4 Ma) felsic dykes that intrude into the Neoproterozoic (ca. 750 Ma) magmatic suite of the Nagar Parkar Igneous Complex (NPIC), the western extension of the Malani Igneous Suite (MIS). The NPIC consists of Neoproterozoic basement amphibolites and granites (riebeckite–aegirine gray granites and the biotite–hornblende pink granites), all of which are intruded by several generations of mafic and felsic dykes. Granitic magmatism occurred in the Late Neoproterozoic (ca. 750 Ma) due to the subduction‐, followed by the rift‐related tectonic regime during the breakup of the Rodinia supercontinent. U–Th–Pb zircon and monazite CHIME age data of 700–800 Ma from the earlier generation porphyritic felsic dykes suggest the dyke intrusion was coeval or soon after the emplacement of the host granites. Our findings of Permian age orthophyric felsic dykes provide new insights for the prevalence of active tectonics in the MIS during late Paleozoic. Textural features and geochemistry also make the orthophyric dykes distinct from the early‐formed porphyritic dykes and the host granites. Our newly obtained age data combined with geochemistry, suggest the existence of magmatism along the western margin of India (peri‐Gondwana margin) during Permian. Like elsewhere in the region, the Permian magmatism in the NPIC could be associated with the rifting of the Cimmerian micro‐continents from the Gondwana.     

Radiometric ages of Alpine metamorphic rocks in the western and central Alps

Abstract The chronological characteristics of Alpine metamorphic rocks are described and Alpine metamorphic events are reinterpreted on the basis of chronological data for the western and central Alps from 1960 to 1992. Metamorphic rocks of the Lepontine, Gran San Bernardo, Piemonte, Internal Crystalline Massifs and Sesia-Lanzo mostly date Alpine metamorphic events, but some (along with granitoids and gneisses from the Helvetic and Southern Alps) result from the Variscan, Caledonian or older events and thus predate the Alpine events. Radiometric age data from the Lepontine area show systematic age relations: U-Pb monazite (23-29 Ma), Rb-Sr muscovite (15–40 Ma) and biotite (15–30 Ma), K-Ar biotite (10-30 Ma), muscovite (15–25 Ma) and hornblende (25-35 Ma), and FT zircon (10-20 Ma) and apatite (5-15 Ma), which can be explained by the different closure temperatures of the isotopic systems. A 121 Ma U-Pb zircon age for a coesite-bearing whiteschist (metaquartzite) from the Dora-Maira represents the peak of ultra-high pressure metamorphism. Coesite-free eclogites and blueschists related to ultra-high pressure rocks in the Penninic crystalline massifs yield an ⁴⁰Ar-³⁹Ar plateau age of about 100 Ma for phengites, interpreted as the cooling age. From about 50 Ma, eclogites and glaucophane schists have also been reported from the Piemonte ophiolites and calcschists, suggesting the existence of a second high P/T metamorphic event. Alpine rocks therefore record three major metamorphic events: (i) ultra-high and related high P/T metamorphism in the early Cretaceous, which is well preserved in continental material such as the Sesia-Lanzo and the Penninic Internal Crystalline Massifs; (ii) a second high P/T metamorphic event in the Eocene, which is recognized in the ophiolites and calcschists of the Mesozoic Tethys; and (iii) medium P/T metamorphism, in which both types of high P/T metamorphic rocks were variably reset by Oligocene thermal events. Due to the mixture of minerals formed in the three metamorphic events, there is a possibility that almost all geochronological data reported from the Alpine metamorphic belt show mixed ages. Early Cretaceous subduction of a Tethyan mid-ocean ridge and Eocene continental collision triggered off the exhumation of the high pressure rocks.     

Fission track and U–Pb zircon ages of psammitic rocks from the Harushinai unit,Kamuikotan metamorphic rocks,central Hokkaido,Japan: constraints on metamorphic histories

Accurate pressure–temperature–time (P–T–t) paths of rocks from sedimentation through maximum burial to exhumation are needed to determine the processes and mechanisms that form high‐pressure and low‐temperature type metamorphic rocks. Here, we present a new method combining laser ablation–inductively coupled plasma–mass spectrometry (LA–ICP–MS) U–Pb with fission track (FT) dates for detrital zircons from two psammitic rock samples collected from the Harushinai unit of the Kamuikotan metamorphic rocks. The concordant zircon U–Pb ages for these samples vary markedly, from 1980 to 95 Ma, with the youngest age clusters in both samples yielding Albian‐Cenomanian weighted mean ages of 100.8 ± 1.1 and 99.3 ± 1.0 Ma (2σ uncertainties). The zircon U–Pb ages were not reset by high‐P/T type metamorphism, because there is no indication of overgrowth within the zircons with igneous oscillatory zoning. Therefore, these weighted mean ages are indicative of the maximum age of deposition of protolithic material. By comparison, the zircon FT data yield a pooled age of ca. 90 Ma, which is almost the same as the weighted mean age of the youngest U–Pb age cluster. This indicates that the zircon FT ages were reset at ca. 90 Ma while still at their source, but have not been reset since. This conclusion is supported by recorded temperature conditions of less than about 300 °C (the closure temperature of zircon FTs), as estimated from microstructures in the deformed detrital quartz grains in psammitic rocks, and no shortening of fission track lengths in the zircon. Combining these new data with previously reported white mica K–Ar ages indicates that the Harushinai unit was deposited after ca. 100 Ma, and underwent burial to its maximum depth before being subjected to a localized thermal overprint during exhumation at ca. 58 Ma.     

A metamorphic history from micron-scale Pb/Pb chronometry of Archean monazite

Ion microprobe measurements of Pb isotope ratios in monazites have been obtained, in situ, from thin sections using the Cambridge ISOLAB 120. Molecular interferences are sufficiently resolved at an RP of 6500 to allow ²⁰⁷Pb/²⁰⁶Pb dating of monazite with precisions as low as 4–5 Ma (2σ). The results presented here provide important information on the chronological history of the Late Archean metamorphism of the Wind River Range, Wyoming (USA).

Matrix monazites and monazite inclusions in garnets from a metapelite from the northern Wind River Range have been analysed by SIMS. In a previous study peak metamorphic conditions (T = 800°C; P = 8 ± 1 kb^*) were estimated using inclusion assemblages in garnets from this same sample. Isolated monazite inclusions in garnet yield ²⁰⁷Pb/²⁰⁶Pb age estimates of 2781 ± 6 to 2809 ± 10 Ma. Those along fractures yield lower ages (2603–2687 Ma) which are similar to TIMS and SIMS ages of matrix monazites. A single large (500 μm) monazite grain locally preserves growth zoning, but has a recrystallised core and a resorbed (recrystallised?) rim. Age estimates for these three regions are 2788 ± 9 Ma, 2663 ± 4 and 2523 ± 6 Ma, respectively. Thus the inclusion assemblages of Sharp and Essene^* may record peak metamorphic conditions at ca. 2.8 Ga, and indicate a phase of metamorphism that predates by over 100 Ma the emplacement of the Bridger Batholith, the major lithologic component of the northern Wind River Range.

The analysed monazite grains appear to preserve ca. 300 Ma history, even within a single grain. Monazite inclusions in garnet that are fully armoured may provide estimates for the time of garnet growth, even in high grade terranes where most chronometers are reset. The age pattern preserved by the large monazite grain cannot be simply related to diffusion controlled closure. Instead, a chronology is preserved which can be related to the petrographic setting of indicidual grains through in situ analysis.