小秦岭303号石英脉流体包裹体Rb—Sr,^40Ar—^39Ar成矿年龄测定

用石英流体包裹体Ｒｂ－Ｓｒ、＾４０Ａｒ－＾３９Ａｒ法测定了小秦岭３０３号石英脉的形成时代为石元古代。其流体包裹体属Ｈ２Ｏ＋ＣＯ２＋ＣａＣｌ型,盐度为６．５％－１２．９８％,ＣＯ２含量高,Ｎａ＾＋〉Ｋ＋。３０３号石英脉Ｒｂ－Ｓｒ等时线年龄为（２３８２±３３６）Ｍａ－（２２３４±４７）Ｍａ,（＾８７ｓＲ／＾８６Ｓｒ）ｉ为（０．７３５１±０．００１９）－（０．７４１６±０．０００４）,＾４０Ａｒ＾＾３９     

早元古代滹沱群玄武岩Rb—Sr,Sm—Nd同位素体系初论

本文给出了的滹沱群下亚群青石村组玄武岩Ｒｂ－Ｓｒ、Ｓｍ－Ｎｄ全岩等时线年龄为２０４５．８±１７和２３６９±３０Ｍａ（２σ），角闪石＾４０Ａｒ＾－＾３９Ａｒ坪年龄和最高视年龄为１３６４±１９和１９３２±１９Ｍａ（１σ）；中亚群河边村组玄武岩Ｒｂ－Ｓｒ全岩等时线年龄图的投点呈完全离散状。     

广东东镇岩体微区^40Ar／^39Ar年龄及其意义

采用激光显微探针＾４０Ａｒ／＾３９Ａｒ测年技术（简称微区＾４０Ａｒ／＾３９Ａｒ法）对广东云开地区东镇岩体含眼球体的片麻状花岗质岩石中单矿物作了同位素年龄测定，获得眼球体内核中的巨晶状钾长石年龄（４１９．４０±４．３７）×１０＾６ａ。眼球体角缘中重结晶微粒状钾长石年龄（２７２．６３±３．１３）×１０＾６ａ，眼球体外壳中的强应变长条纹黑云母年龄（１７７．８４±２．２９）×１０＾ａ。暗色条带中的弱应变板     

燧石和脉石英中氩,氯的相关性对^40Ar—^39Ar定年意义

由于过剩Ａｒ的存在，长期以来燧石和脉石英的＾４０Ａｒ－＾３９Ａｒ定年被视为不可能。通过对这类矿物中Ａｒ，Ｃｌ丰度及其相关性研究，可以校正过剩Ａｒ，从而实现了这类矿物的年龄测定，这为沉积岩定年及成矿时代的研究提供了重要手段，应用这一技术测得长城系底砾岩中石英年龄为１７４４±９７Ｍａ，滹沱群郭家寨亚群热事件年龄为１７６６±４９Ｍａ，进而推断长城系与郭家寨亚群的层位呈上下系。     

柴北缘榴辉岩的峰期和退变质年龄：来自U—Pb及Ar—Ar同位素测定的 …

柴北缘大柴旦榴辉岩呈透镜状产于以角闪岩相变质条件为特征的片麻岩中。选择新鲜的保存较好的榴辉岩分别进行Ｕ－Ｐｈ和Ａｒ－Ａｒ同位素年代学测定,含石榴子石的白云母片麻岩（此榴辉岩的围岩）被选用于白云母的Ａｒ－Ａｒ测定。榴辉岩的 Ｕ－Ｐｈ测定显示~（２０６）Ｐｂ／~（２３８）Ｕ表面年龄统计权重平均值为（４９４． ６±６． ５）Ｍａ,代表榴辉岩的峰期变质作用年龄。同样榴辉岩样品的多硅白云母被分选出用于~（３９）Ａｒ－~（４０）Ａｒ年代学测定。测定结果获得的坪年龄为（４６６． ７±１． ２）Ｍａ,等时线年龄为（４６５． ９±５． ４）Ｍａ,代表榴辉岩在退变过程中的冷却年龄;围岩中白云母的~（３９）Ａｒ－~（４０）Ａｒ年代学测定,获得等时线年龄为（４７７． ６７±１７． ７２）Ｍａ。相似的 Ａｒ－Ａｒ年龄值表明,榴辉岩和围岩在抬升过程中经历了一致的冷却及退变质历史。     

激光质谱测定南极乔治王岛北海岸A635玄武岩微区^40Ar—^39Ar的等…

采用连续激光直接对岩石光片样品微区熔样，以高灵敏度、高精确度的质谱计测试，对南极乔治王岛玄武岩样品进行＾４０Ａｒ－＾３９－Ａｒ汪守年，取得了成功。样品置反应堆中心Ｅ－５孔道，以１．８×１０＾１８ｎ／ｃｍ＾２的快中子总通量照射，时间为５０ｈ，放射性冷却后进行测定。     

TritonX—100—5—Br—PADAP光度法测定铜和镍

研究了非离子型表面活性剂ＴｒｉｔｏｎＸ－１００存在下,用５－Ｂｒ－ＰＡＤＡＰ光度法测定铜镍的方法。结果表明：在ＰＨ９．０的硼砂缓冲介质中,５－Ｂｒ－ＰＡＤＡＰ与铜和镍生成紫红色络合物,λｍａｘ＾Ｃｕ＝５７５ｎｍ,εＣｕ＝１．０４×１０＾５Ｌ·ｍｏｌ＾－１·ｃｍ＾－１,λｍａｘ＾Ｎｉ＝５７５ｎｍ,εＮｉ＝１．１４×１０＾５Ｌ·ｍｏｌ＾－１·ｎｍ＾－１。铜和镍的质量浓度分别在０￣５６０μｇ／Ｌ和０￣５     

郯庐断裂带北段形成的年代学及其意义

对郯庐断裂带北段内的依兰－伊通断裂带测定断民支岩的黑云母单矿物＾４０Ａｒ／＾３９Ａｒ坪年龄为１００±２．３－９５．７±２．７４Ｍａ，同时测定了带内的辉绿岩全岩Ｒｂ－Ｓｒ等时线年龄为１００±５．９Ｍａ，而辉绿岩中辉石单矿物的＾４０Ａｒ／＾３９Ａｒ坪年龄为１０５Ｍａ。结合断裂切过下白垩统泉头组，表明左行走滑断裂形成于１００Ｍａ左右，即早白垩世末期。     

河北张－宣金矿区含金石英脉~（40）Ar／~（39）Ar年龄

为解决张－宣地区含金石英脉形成的时代，对区内５个典型金矿脉测定了４０Ａｒ／３９Ａｒ年龄，分别为：１３６２．０±２４．８Ｍａ，９６３．７±２２．３Ｍａ，５７９．６±８．５Ｍａ，５７０．８±２４．２Ｍａ，１６７．９±１．２Ｍａ。谱线特征均为马鞍形，最低视年龄为石英的结晶年龄。依次相当于晋宁运动中期，晋宁运动晚期，蓟县运动晚期和燕山运动中期。     

激光显微探针^40Ar／^39Ar定年进入了人类历史领域：评美国伯克莱地质年代学

美国伯克莱地质年代学中心Ｐ．Ｒ．Ｒｅｎｎｅ等（１９９７）对采自意大利维苏威火山公元７９年爆发喷出物中的透长石,进行了激光显微探针＾４０Ａｒ／＾３９Ａｒ定年,从４６个分析数据中得到了＾４０Ａｒ／＾３９Ａｒ等时线年龄为１９２５±９４ａ,接近于与现今使用的格里历１９８１年前一致。这证明激光显微探针＾４０Ａｒ／＾３９Ａｒ定年法的可信度已扩展到记录人类历史的时间范畴。Ｒｅｎｎｅ等的最新研究成果把３０多年来Ｋ     

Linking deformation, migmatite formation and zircon U–Pb geochronology in polymetamorphic orthogneisses, Sveconorwegian Province, Sweden

Absolute ages of migmatization in the polymetamorphic, parautochthonous basement of the Sveconorwegian Province, Sweden, have been determined using U–Pb ion probe analysis of zircon domains that formed in leucosome of migmatitic orthogneisses. Migmatite zircon was formed by recrystallization whereas dissolution–reprecipitation and neocrystallization were subordinate. The recrystallized migmatite zircon was identified by comparison of zircon in mesosomes and leucosomes. It is backscatter electron‐bright, U‐rich (800–4400 ppm) with low Th/U‐ratios (generally 0.01–0.1), unzoned or ‘oscillatory ghost zoned’, and occurs as up to 100 μm‐thick rims with transitional contacts to cores of protolith zircon. Protolith ages of 1686 ± 12 and 1668 ± 11 Ma were obtained from moderately resorbed, igneous zircon crystals (generally Th/U = 0.5–1.5, U < 300 ppm) in mesosomes; protolith zircon is also present as resorbed cores in the leucosomes. Linkage of folding, synchronous migmatization and formation of recrystallized zircon rims allowed direct dating of south‐vergent folding at 976 ± 7 Ma. At a second locality, similar recrystallized zircon rims in leucosome date pre‐Sveconorwegian migmatization at 1425 ± 7 Ma; an upper age bracket of 1394 ± 12 Ma for two overprinting phases of deformation (upright folding along gently SSW‐plunging axes and stretching in ESE) was set by zircon in a folded metagranitic dyke. Lower age brackets for these events were set at 952 ± 7 and 946 ± 8 Ma by zircon in two crosscutting and undeformed granite–pegmatite dykes. Together with previously published data the present results demonstrate: (i) Tectonometamorphic reworking during the Hallandian orogenesis at 1.44–1.42 Ga, resulting in migmatization and formation of a coarse gneissic layering. (ii) Sveconorwegian continent–continent collision at 0.98–0.96 Ga, involving (a) emplacement of an eclogite unit, (b) regional high‐pressure granulite facies metamorphism, (c) southvergent folding, subhorizontal, east–west stretching and migmatization, all of which caused overprint or transposition of older Mesoproterozoic and Sveconorwegian structures. The Sveconorwegian migmatization and folding took place during or shortly after the emplacement of Sveconorwegian eclogite and is interpreted as a result of north–south shortening, synchronous with east–west extension and unroofing during late stages of the continent–continent collision.     

Radiometric dating of the Middle Palaeolithic tool industry and associated fauna of Pin Hole Cave,Creswell Crags,England

Uranium-series dating of derived speleothem suggests that the sediments enclosing a Middle Palaeolithic stone artefact assemblage in Pin Hole Cave probably accumulated after about 64 ka, and ¹⁴C dates indicate a likely age of > 40 ka for the large mammal fauna associated with it. Electron spin resonance data from the fauna conform with these age constraints and are consistent with accumulation between 38 and 50 ka. This evidence supports the view that Britain was recolonised by hominids during Oxygen Isotope Stage 3. Stratigraphically higher stone tool industries demonstrate the local presence of both early Upper and late Upper Palaeolithic cultures. © 1998 John Wiley & Sons, Ltd.     

甘肃巴谢剖面黄土-古土壤的光释光测年研究

光释光（OSL）测年是测定第四纪沉积物年龄的一种新技术。它通过单色光束激发使晶体中储存的电离辐射能释放出来。与热释光（TL）测年相比，OSL测年可以不考虑残留的OSL信号，而且测量具有简便、迅速且准确等优点。本文用细颗粒光释光技术对甘肃巴谢剖面的黄土-古土壤进行了测定，其测年结果与14C测年结果相吻合。这表明，光释光是一项极潜力的年代学技术。     

川西北平武地区南一里花岗闪长岩锆石U-Pb定年及其地质意义

川西北平武地区的碧口地块中出露较多的印支期岩浆侵入岩类,但缺乏精确的年代学资料.笔者运用阴极发光技术,对碧口地块西南缘的南一里化岗闪长岩中的锆石进行了细致的内部结构分析,并在此基础上利用LA-ICP-MS锆石U-Pb原位定年技术进行了同位素年龄测定.结果表明,花岗闪长岩中锆石Th/U比值较高,阴极发光图像显示锆石内部发育振荡环带,具岩浆成因特点;南一里花岗闪长岩的结晶年龄为223.1±2.6 Ma(MSWD=1.4),表明其形成时代为晚三叠世早期、南一里花岗闪长岩侵入时代晚于勉略构造带的主碰撞期,侵位于后碰撞环境,或者至少是由同碰撞到后碰撞的转折阶段.     

The deglaciation of Clyde Inlet,northeastern Baffin Island,Arctic Canada

The behaviour of ice sheets as they retreated from their Last Glacial Maximum (LGM) positions provides insights into Lateglacial and early Holocene ice‐sheet dynamics and climate change. The pattern of deglaciation of the Laurentide Ice Sheet (LIS) in arctic fiord landscapes can now be well dated using cosmogenic exposure dating. We use cosmogenic exposure and radiocarbon ages to constrain the deglaciation history of Clyde Inlet, a 120 km long fiord on northeastern Baffin Island. The LIS reached the continental shelf during the LGM, retreated from the coastal lowlands by 12.5 ± 0.7 ka (n = 3), and from the fiord mouth by 11.7 ± 2.2 ka (n = 4). Rapid retreat from the outer fiord occurred 10.3 ± 1.3 ka (n = 6), with the terminus reaching the inner fiord shortly after 9.4 ka (n = 2), where several moraine systems were deposited between ca. 9.4 and ca. 8.4 ka. These moraines represent fluctuations of the LIS during the warmest summers since the last interglaciation, and this suggests that the ice sheet was responding to increased snowfall. Before retreating from the head of Clyde Inlet, the LIS margin fluctuated at least twice between ca. 7.9 and ca. 8.5 ka, possibly in response to the 8.2 ka cold event. Copyright © 2006 John Wiley & Sons, Ltd.     

江西岿美山钨矿矿床的成矿年龄及地质特征

江西省定南县岿美山钨矿区位于南岭东西向构造带东段与武夷山北东-北北东向构造带南段的复合部位,是赣南地区以石英脉型黑钨矿和矽卡岩型白钨矿共生为特征的钨矿床,其是否为南岭地区燕山期的成矿作用,一直没有精确的年代学研究成果。本文采用锆石SHRIMP U-Pb定年和辉钼矿Re-Os同位素定年技术,对岩体年龄和成矿年龄进行了精细的测定,获得成矿黑云母花岗岩体的锆石SHRIMP U-Pb年龄为（157.7±2.7） Ma（n=11,MSWD=1.9）,黑钨矿石英脉的辉钼矿Re-Os等时线年龄为（153.7±1.5） Ma（n=5,MSWD=0.16）,显示岿美山区是华南地区中生代钨矿大规模成岩成矿作用的产物之一。根据“五层楼+地下室”的找矿模型,并结合矿区的最新找矿线索,研究认为在矿区深部岩体的内外接触带具有存在新矿体的可能性,该区深部具有较大的找矿潜力,同时探索性地提出赣南地区石英脉型钨矿深边部存在矽卡岩型钨矿化的可能,对区域钨矿的深边部找矿工作具有指导意义。     

皖南东源含W、Mo花岗闪长斑岩及成矿年代学研究

在详细野外观察、剖面测量和研究分析的基础上,对"江南古陆"东段北缘的皖南祁门东源含W、Mo斑岩体进行了锆石U-Pb测年,重点讨论了成岩成矿关系和成矿物质来源。东源中细粒似斑状花岗闪长斑岩呈小岩株产出,SHR IMP锆石U-Pb测年结果为(146±1)M a,其内辉钼矿Re-Os同位素测年结果为(146.4±2.3)M a,成矿与岩体形成同期,均形成于晚侏罗世。辉钼矿的Re含量(22.02×10-6~98.09×10-6)指示成矿物质来源为壳幔混源。     

稀有金属花岗伟晶岩锆石、锡石与铌钽铁矿U-Pb和白云母~(40)Ar/~(39)Ar测年对比研究——以阿尔金中段吐格曼北锂铍矿床为例

稀有金属花岗伟晶岩年代学是花岗伟晶岩型稀有金属矿床研究的重要内容。目前测年方法较多,但不同方法测试结果的对比研究亟待开展。我们选择吐格曼北花岗伟晶岩型锂铍矿床3条含矿伟晶岩开展锆石、锡石、铌钽铁矿及白云母四种矿物不同方法的测年对比研究。结果显示:1)ρ31白云母-锡石伟晶岩中锡石238U/206Pb-207Pb/206Pb谐和年龄为468±8.7Ma (MSWD=1.1,N=39)、白云母-钠长石-锂辉石伟晶岩中锆石206Pb/238U谐和年龄为458.7±2.3Ma (MSWD=7.2,N=16); 2)ρ38白云母-钠长石-锂辉石伟晶岩中锆石206Pb/238U谐和年龄为454.7±4.0Ma (MSWD=8.0,N=10)、白云母40Ar/39Ar坪年龄为350.2±1.6Ma (MSWD=4.7); 3)ρ87含铌钽铁矿-白云母-石英伟晶岩中铌钽铁矿206Pb/238U谐和年龄为464.1±2.7Ma (MSWD=5.2,N=39)。可以看出,铌钽铁矿与锡石的U-Pb年龄在误差范围内一致,可能代表花岗伟晶岩岩浆结晶的年龄; 2件样品的蜕晶化锆石U-Pb年龄也可以对比,可能代表岩浆锆石蜕晶化后经流体交代作用及重结晶作用导致U-Pb同位素系统重置的时间。白云母Ar-Ar年龄明显晚于铌钽铁矿、锡石和锆石的U-Pb年龄,鉴于ρ38白云母-钠长石-锂辉石伟晶岩脉中白云母与锂辉石发生了强烈变形与蚀变,认为变形的白云母记录的是叠加变形与热液蚀变的时间。由此推断吐格曼北锂铍花岗伟晶岩形成于468～454Ma,这意味着阿尔金山地区中-晚奥陶世可能存在持续时间较长的稀有金属成矿事件。基于花岗伟晶岩矿物成因与吐格曼北锂铍花岗伟晶岩不同方法测年对比结果,可以得出以下结论:铌钽铁矿与锡石的U-Pb年龄可代表伟晶岩岩浆结晶的年龄,蜕晶化的锆石U-Pb年龄记录的是岩浆锆石蜕晶化后经流体交代作用及重结晶作用导致U-Pb同位素系统重置的时间,含钾矿物的40Ar/39Ar年龄能够约束伟晶岩的变形与蚀变年龄;多种定年方法的联合约束可以更好地限定稀有金属花岗伟晶岩的各个阶段成矿事件时间。     

Geochronology of magmatism and mineralization of the Daheishan giant porphyry molybdenum deposit,Jilin Province,Northeast China: constraints on ore genesis and implications for geodynamic setting

Daheishan giant porphyry Mo deposit is located in the Lesser Xing’an–Zhangguangcai Ranges, Jilin Province, NE China. Mineralization is closely related to the Daheishan intrusive complex, which can be divided into Changganglin biotite granodiorite, Qiancuoluo biotite granodiorite, and Qiancuoluo granodioritic porphyry. Four stages of mineralization are distinguished, based on the cross-cutting relationships of mineralized veins. LA-ICPMS zircon U-Pb analysis yields ²⁰⁶Pb/²³⁸U ages of 177.9 ± 2.3 Ma for the Changganglin biotite granodiorite, 169.9 ± 2.3 Ma for the Qiancuoluo biotite granodiorite, and 166.6 ± 4.0 Ma for the Qiancuoluo granodioritic porphyry. Hydrothermal fluids responsible for mineralization evolved from different magmas. Six molybdenite samples yield Re-Os model ages of ~167 Ma. Muscovite from the last mineralization stage gives a ⁴⁰Ar/³⁹Ar plateau age of 163.6 ± 0.9 Ma. Geochronology data indicate that the entire magmatic system lasted for about 10 million years, and the total duration of hydrothermal activity was less than 4 million years. The ε_Hf(t) values of zircons obtained from the Changganglin biotite granodiorite, Qiancuoluo biotite granodiorite, and Qiancuoluo granodioritic porphyry range from 4.5 to 9.1, 5.7 to 10.9, and 4.4 to 7.1, respectively, indicating that they were mainly derived from the depleted mantle, although contaminated by crustal materials to a greater or lesser extent. The formation of the Daheishan porphyry Mo deposit was temporally and spatially related to the amalgamation of Jiamusi Massif and Songliao terrane in the Palaeo-Pacific Ocean regime. Regional Hf isotopic compositions of zircon suggest an episode of crustal growth in the Phanerozoic in the Lesser Xing’an–Zhangguangcai Ranges. Regional Mo mineralization ages suggest a peak of porphyry Mo mineralization in the Jurassic in the Lesser Xing’an-Zhangguangcai Ranges.