Single and multigrain quartz‐luminescence dating of irrigation‐channel features in Santa Fe,New Mexico

Acequias (irrigation channels and ditches) were used by Spanish settlers, their descendants, and Native Americans in New Mexico. Several such features were recently excavated in Santa Fe, but material for numeric dating was difficult to find. Therefore, for this high‐energy‐deposition irrigation‐feature setting we applied optically stimulated luminescence (OSL) sediment dating methods to determine the timing of last filling of some of these acequias. We report multigrain single‐aliquot quartz (MGSAQ) OSL dating results and the first single‐grain quartz (SGQ) OSL dating results for irrigation features. One sample yielded an average age of 96 ± 13 yr, consistent with the maximum expected age of 127 yr (before 2007). An OSL age of 175 ± 15 yr for another sample delimits a sedimentation event since the first construction of that feature ca. 300 yr ago. A sample known to be younger than 400–450 yr but predating the mid‐19th century gave an SGQ age of 376 ±31 yr. These results indicate that: (1) Regional quartz in New Mexico is highly favorable to OSL dating; (2) in this setting, SGQ OSL dating is preferred to MGSAQ dating; and (3) for the last 500–600 yr, SGQ OSL dating in such settings is preferred to ¹⁴C dating because OSL dating lacks those ambiguities inherent in converting ¹⁴C ages to calendar years. © 2009 Wiley Periodicals, Inc.     

Luminescence chronology of non‐glacial sediments in Changeable Lake,Russian High Arctic,and implications for limited Eurasian ice‐sheet extent during the LGM

A 10.5 m core from Changeable Lake in the Severnaya Zemlya Archipelago just north of the Taymyr Peninsula intersects ca. 30 cm of diamicton at its base, interpreted as a basal till. Because the upper 10.13 m of this core consists of non‐glacial sediments, a maximum numeric age for these non‐glacial sediments would provide a clear lower limit to the timing of the last glaciation in the area of Changeable Lake. Radiocarbon (¹⁴C) dating of several materials from this core yielded widely scattered results. Consequently we applied photonic dating to sediments above the diamicton. The experimental single‐aliquot‐regenerative (SAR) dose fine‐grain method was applied to two samples, using the ‘double SAR’ approach. With one exception, these fine‐grain SAR results and the results of application of the SAR method to sand‐sized quartz grains from two samples, at ca. 9.95 m and ca. 10.05 m depth, are discrepant with age estimates from the multi‐aliquot infrared‐photon‐stimulated luminescence (IR‐PSL) method applied to fine grains. Multi‐aliquot IR‐PSL dating of 10 samples produces ages increasing monotonically from ca. 4 ka at 2 m to 53 ± 4 ka at 9.97 m. These self‐consistent multi‐aliquot IR‐PSL ages, along with limiting ¹⁴C ages of >47 ka at ca. 10 m, provide direct evidence that glacial ice did not advance over this lake basin during the Last Glacial Maximum, and thus delimit the northeastern margin of the Barents–Kara Sea ice‐sheet to somewhere west of this archipelago. The last regional glaciation probably occurred during marine isotope stage (MIS) 4 or earlier. Copyright © 2004 John Wiley & Sons, Ltd.     

Optically stimulated luminescence dating of late Holocene raised strandplain sequences adjacent to Lakes Michigan and Superior, Upper Peninsula, Michigan, USA

This study evaluates the accuracy of optically stimulated luminescence to date well-preserved strandline sequences at Manistique/Thompson bay (Lake Michigan), and Tahquamenon and Grand Traverse Bays (Lake Superior) that span the past ∼4500 yr. The single aliquot regeneration (SAR) method is applied to produce absolute ages for littoral and eolian sediments. SAR ages are compared against AMS and conventional ¹⁴C ages on swale organics. Modern littoral and eolian sediments yield SAR ages <100 yr indicating near, if not complete, solar resetting of luminescence prior to deposition. Beach ridges that yield SAR ages <2000 yr show general agreement with corresponding ¹⁴C ages on swale organics. Significant variability in ¹⁴C ages >2000 cal yr B.P. complicates comparison to SAR ages at all sites. However, a SAR age of 4280 ± 390 yr (UIC913) on ridge77 at Tahquamenon Bay is consistent with regional regression from the high lake level of the Nipissing II phase ca. 4500 cal yr B.P. SAR ages indicate a decrease in ridge formation rate after ∼1500 yr ago, likely reflecting separation of Lake Superior from lakes Huron and Michigan. This study shows that SAR is a credible alternative to ¹⁴C methods for dating littoral and eolian landforms in Great Lakes and other coastal strandplains where ¹⁴C methods prove problematic.     

OSL dating of the Middle Palaeolithic Hotel California site,Sierra de Atapuerca,north‐central Spain

In this study we present optically stimulated luminescence (OSL) dating results obtained at one of the most important open‐air Middle Palaeolithic sites in the Sierra de Atapuerca foothills – Hotel California. We also assess the possibility of obtaining extended‐range OSL chronologies for a nearby Middle Pleistocene fluvial deposit using several novel methods, namely OSL dating of individual quartz ‘supergrains’, multi‐grain aliquot thermally transferred OSL (TT‐OSL) dating and the first application of a single‐grain TT‐OSL dating procedure. Four single‐grain OSL ages constrain the Middle Palaeolithic occupation of Hotel California to between 71±6 and 48±3 ka. The Hotel California single‐grain equivalent dose (D_e) distributions are highly overdispersed and contain several dose populations, which are probably attributable to post‐depositional sediment mixing, partial bleaching and intrinsic scatter. The reliability of multi‐grain aliquot OSL dating is compromised by the complex underlying D_e dispersion affecting these samples, as well as by biasing multi‐grain averaging effects. Extended‐range OSL and TT‐OSL chronologies for the nearby Pico River terrace are consistent with each other and with broad independent age control. These experimental approaches yield a weighted average age of 348±16 ka for terrace T_A9 of the Arlanzón River sequence. Our results highlight the benefits of comparing ages obtained using several OSL methodologies to improve the robustness of luminescence chronologies. They also demonstrate the potential that single‐grain OSL techniques offer for establishing improved age constraints on the many other Middle Palaeolithic sites found at Atapuerca and elsewhere across north‐central Spain.     

Direct luminescence chronology of the Epipaleolithic Kebaran site of Nahal Hadera V,Israel

We report direct luminescence ages for the culture‐bearing sediments of the Kebaran site of Nahal Hadera V (NHV) in the coastal plain of Israel. Although the site contains, in addition to rich lithic deposits, plentiful mammalian bone, it has proved to be undatable using radiocarbon dating, in spite of the fact that the cultural context places the time of occupation well within the range of radiocarbon dating. In contrast, luminescence dating of the site sediments proved successful. Luminescence ages were determined using the single aliquot additive‐dose (SAA) method, applied to sand‐sized quartz extracts to determine past equivalent doses (D_e). Dose rates (R) were calculated using thick source alpha counting for the uranium (U) and thorium (Th) concentrations and x‐ray fluorescence analysis for the potassium (K₂0) concentration. Of the five samples collected at the site, four represent cultural and subcultural deposits and the fifth represents the geological substrate for the archaeological deposit, a quartz‐rich, carbonate‐cemented dune sand known as aeolianite or kurkar. The luminescence age of the kurkar is 42.7 ± 6.3 ka. Human occupation of the site occurred between 21.3 ka and 14.0 ka ago, during the Last Glacial Maximum. © 2003 Wiley Periodicals, Inc.     

Re‐dating the Pilgrimstad Interstadial with OSL: a warmer climate and a smaller ice sheet during the Swedish Middle Weichselian (MIS 3)?

Alexanderson, H., Johnsen, T. & Murray, A. S. 2009: Re‐dating the Pilgrimstad Interstadial with OSL: a warmer climate and a smaller ice sheet during the Swedish Middle Weichselian (MIS 3)? Boreas, 10.1111/j.1502‐3885.2009.00130.x. ISSN 0300‐9483. Pilgrimstad in central Sweden is an important locality for reconstructing environmental changes during the last glacial period (the Weichselian). Its central location has implications for the Scandinavian Ice Sheet as a whole. The site has been assigned an Early Weichselian age (marine isotope stage (MIS) 5 a/c; >74 ka), based on pollen stratigraphic correlations with type sections in continental Europe, but the few absolute dating attempts so far have given uncertain results. We re‐excavated the site and collected 10 samples for optically stimulated luminescence (OSL) dating from mineral‐ and organic‐rich sediments within the new Pilgrimstad section. Single aliquots of quartz were analysed using a post‐IR blue single aliquot regenerative‐dose (SAR) protocol. Dose recovery tests were satisfactory and OSL ages are internally consistent. All, except one from an underlying unit that is older, lie in the range 52–36 ka, which places the interstadial sediments in the Middle Weichselian (MIS 3); this is compatible with existing radiocarbon ages, including two measured with accelerator mass spectrometry (AMS). The mean of the OSL ages is 44±6 ka (n=9). The OSL ages cannot be assigned to the Early Weichselian for all reasonable adjustments to water content estimates and other parameters. The new ages suggest that climate was relatively mild and that the Scandinavian Ice Sheet was absent or restricted to the mountains for at least parts of MIS 3. These results are supported by other recent studies completed in Fennoscandia.     

Exploring the method of optical dating and comparison of optical and 14C ages of Late Weichselian coversands in the southern Netherlands

A study was made of the applicability of three different techniques for equivalent dose (D_e) determination in the optical dating of quartz: the single‐aliquot regenerative‐dose technique (SAR), the single‐aliquot additive‐dose technique (SAAD) and the multiple‐aliquot additive‐dose technique (MAAD). For this purpose, quartz grains were extracted from a sequence of Upper Pleniglacial to Late‐glacial coversands exposed at the locality of Ossendrecht in the southwestern Netherlands, a site for which both radiocarbon and earlier luminescence dates are available, providing independent age control. Upon testing the different assumptions underlying each of the three OSL techniques investigated, the SAR protocol was found to be the technique of choice. The optical ages obtained with this protocol were in good agreement with the chronostratigraphical position of the sediments investigated and with the available chronostratigraphical information on the same and equivalent deposits. This confirms the suitability of the SAR technique for dating coversands. Furthermore, a small laboratory intercomparison of SAR‐based D_e determinations yielded results that were in fair overall agreement. Copyright © 2004 John Wiley & Sons, Ltd.     

Infrared stimulated luminescence dating of an Eemian (MIS 5e) site in Denmark using K‐feldspar

Buylaert, J.‐P., Huot, S., Murray, A.S. & Van den haute, P.: Infrared stimulated luminescence dating of an Eemian (MIS 5e) site in Denmark using K‐feldspar. Boreas, 10.1111/j.1502‐3885.2010.00156.x. ISSN 0300‐9483. Infrared stimulated luminescence (IRSL) dating of K‐feldspars may be an alternative to quartz optically stimulated luminescence (OSL) dating when the quartz OSL signal is too close to saturation or when the quartz luminescence characteristics are unsuitable. In this paper, Eemian (MIS 5e) coastal marine sands exposed in a cliff section on the coast of southern Jutland (Denmark) are used to test the accuracy and precision of IRSL dating using K‐feldspars. This material has been used previously to test quartz OSL dating ( Murray & Funder 2003 ): a small systematic underestimation of <10% compared to the expected age of ～130 ka was reported. In our study, a single‐aliquot regenerative‐dose (SAR) IRSL protocol is used to determine values of equivalent dose (D_e) and the corresponding fading rates (g values). A significant age underestimation (of up to ～35%) is observed; this is attributed to anomalous fading. Using a single site‐average fading rate of 3.66 ± 0.09%/decade to correct the IRSL ages for all samples provides good agreement between the average fading‐corrected K‐feldspar age (119 ± 6 ka) and the independent age control (132–125 ka). This is despite the reservations of Huntley & Lamothe (2001) that their fading correction method is not expected to work on samples older than ～20–50 ka. This fading‐corrected feldspar result is not significantly different from the overall revised quartz age (114 ± 7 ka) also presented here. We conclude that fading‐corrected IRSL ages measured using K‐feldspar may be both precise and accurate over a greater age range than might be otherwise expected.     

Holocene eolian activation as a proxy for broad-scale landscape change on the Gila River Indian Community, Arizona

Eolian sediments are common within the middle Gila River Valley, southern Arizona, and reflect variability in eolian and fluvial processes during the late Holocene. This study focuses on deciphering the stratigraphic record of eolian deposition and associated luminescence dating of quartz extracts by single aliquot regeneration (SAR) protocols. Stratigraphic assessment coupled with luminescence ages indicates that there are four broad eolian depositional events at ca. 3145 ± 220 yr, 1950-1360 yr, 800 ± 100 yr, and 690-315 yr. This nascent chronology, correlated with regional archeological evidence and paleoclimate proxy datasets, leads to two general conclusions: (1) loess deposits, transverse-dune formation and sand-sheet deposition in the late Holocene are probably linked to flow variability of the Gila River, though the last two events are concordant with regional megadroughts; and (2) the stability of eolian landforms since the 19th century reflects the lack of eolian sediment supply during a period of fluvial incision, resulting in Entisol formation on dunes. The prime catalyst of eolian activity during the late Holocene is inferred to be sediment supply, driven by climate periodicity and variable flow within the Gila River catchment.     

A detailed post‐IR IRSL dating study of the Niuyangzigou loess site in northeastern China

In this study, we report standard quartz SAR OSL and post‐IR infrared (IR) stimulated luminescence (post‐IR IRSL; pIRIR₂₉₀) measurements made on sand‐sized quartz and K‐feldspar extracts from the loess‐palaeosol sequence at Niuyangzigou in northeastern China. The quartz OSL characteristics are satisfactory. Extensive pIRIR_50,290 dose recovery tests were performed by adding doses on top of the natural dose. We found that dose recovery ratios improve significantly when the test dose ranges between ~15 and ~80% of the total dose, and good dose recovery (within ±5% of unity) can be obtained up to ～800 Gy. Otherwise, the dose recovery ratio deviates from unity. The D_e values also depend on the test dose size and so we conclude that the effect of test dose size should be routinely considered in pIRIR dating. First IR stimulation plateau pIRIR₂₉₀ results are compared with multiple elevated temperature ‐pIRIR (MET‐pIRIR) data. It appears that the low temperature MET‐pIRIR data are strongly affected by poor dose recovery, but this is not the case for the pIRIR₂₉₀ results. Natural signal measurements at the highest (first IR) stimulation temperature on a sample expected to be in field saturation suggest that ~10% signal loss occurs in pIRIR signals. Long‐term laboratory bleaching experiments (>80 days) show that a constant (or very difficult to bleach) residual pIRIR₂₉₀ signal is reached after ~300 h, corresponding to a dose of 6.2±0.7 Gy. Quartz OSL and feldspar pIRIR_50,290 ages are in good agreement at least back to c. 70 ka. Beyond this the quartz ages begin to underestimate but the feldspar ages are in agreement with the expected Last Interglacial age palaeosol.     

OSL Age Determination of Archaeological Stone Structures Using Trapped Aeolian Sediments: A Case Study from the Negev Highlands,Israel

Optically stimulated luminescence (OSL) dating is widely applied to sediments in paleoenvironmental sciences. However, there are only limited examples determining the age of archaeological stone structures by OSL using dust deposits. The age of dust deposits associated with ancient buildings may be used to date the onset of settlement (sediment below structures), settlement activity (occupation layer), or the time after a settlement had been abandoned or destroyed (sediment between collapsed roofs and walls). In this study, OSL dating is applied to establish numerical dates for settlement structures situated in the Negev Highlands, Israel. Two archaeological sites are investigated to identify their occupation history, by dating nine samples of aeolian dust trapped within the remains of ancient buildings. The OSL dating technique is applied using coarse grain quartz and a standard single‐aliquot regenerative‐dose (SAR) protocol. It was possible to date the onset of sedimentation in a later phase of the human occupation or shortly after the sites were abandoned, to 3.7 ± 0.3 ka (Intermediate Bronze Age) at the central site and to 2.7 ± 0.2 ka (Iron Age) at the ephemeral site. These results are supported by archaeological evidence gained from pottery finds and the architecture of the ancient buildings.     

Timing of fluvial sedimentation in the Upper Rhine Graben since the Middle Pleistocene: constraints from quartz and feldspar luminescence dating

The Heidelberg Basin (HDB) hosts one of the thickest Quaternary sediment successions in central Europe. To establish a reliable Middle and Upper Pleistocene chronology for a recently drilled core from the depocentre of the Heidelberg Basin, we applied multiple luminescence dating approaches, including quartz optically stimulated luminescence (OSL), two feldspar post‐IR IRSL protocols using second IR stimulation temperatures of 225 °C (pIRIR₂₂₅) and 290 °C (pIRIR₂₉₀), and two fading correction models. Relatively high anomalous fading was observed for both the pIRIR₂₂₅ and pIRIR₂₉₀ signals, with mean fading rates of 2.13±0.27 and 2.08±0.49%/decade, respectively. Poor dose recovery behaviour of the pIRIR₂₉₀ signal suggests that the pIRIR₂₉₀ ages are not reliable. The comparison of two fading correction methods for the K‐feldspar ages indicates that the correction method proposed by Kars et al. (2008) Radiation Measurements 43, 786, yields reliable ages, whereas the dose‐rate correction method proposed by Lamothe et al. (2003) Radiation Measurements 37, 493, does not. A chronology for the HDB is established using the quartz ages and reliable fading corrected feldspar pIRIR₂₂₅ ages. Our chronology shows that the sediments in the upper Mannheim Formation were deposited during Marine Isotope Stage (MIS) 4 (c. 70 ka), constrained by two quartz ages in the upper 20 m of the core. Four fading corrected pIRIR₂₂₅ ages of c. 400 ka show that the upper Ludwigshafen Formation was deposited during MIS 12–11, correlated with the Elsterian‐Holsteinian stage. Two ages of 491±76 and 487±79 ka indicate that the Middle and Upper Ludwigshafen Formation were probably deposited during the Cromerian Complex. This luminescence chronology is consistent with palynological results. It also indicates that the IR‐RF ages reported earlier are probably underestimated due to anomalous fading.     

Multiple and single aliquot luminescence dating techniques applied to quartz extracted from Middle and Upper Weichselian loess,Zemechy, Czech Republic

This paper reports the application of optically stimulated luminescence (OSL) dating to relatively coarse grains (100–200 μm) of quartz extracted from loess. Two approaches were tested – a multiple aliquot technique and a new single aliquot approach, which is especially suited to the dating of small quantities of such grains found in some loess. The results are compared with infra‐red stimulated luminescence and thermoluminescence (TL) measurements on the finer‐grained (4–11 μm) polymineral fraction and TL measurements on the relatively coarse grains of quartz. The advantages of the new single aliquot (OSL) approach are described and the iterating, computer‐controlled measurement procedure is given. The automated iterative single aliquot regeneration (AISAR) method corrects for changes in luminescence sensitivity during the measurement sequence by monitoring the response to a test dose. Some initial measurements are presented for the loess section at Zemechy, Czech Republic, and these show that the AISAR method gives more precise results than those using a multiple aliquot method. Copyright © 2000 John Wiley & Sons, Ltd.     

The chronostratigraphy of the latest Middle Pleistocene aeolian and alluvial activity on the Island of Hvar,eastern Adriatic,Croatia

Pleistocene aeolian sands and alluvial deposits can frequently be traced along the Mediterranean coast. Such deposits also exist along the eastern Adriatic coast and the nearby islands. Four stratigraphical sections of these deposits were studied on the Island of Hvar with the purpose of establishing a chronological framework of the aeolian–alluvial depositional system, using luminescence dating and magnetic susceptibility stratigraphy. Luminescence dating was applied on coarse‐grained feldspar and quartz grains separated from the sands. Both quartz optically stimulated luminescence (OSL) and feldspar post‐IR infrared stimulated luminescence (pIRIR) age estimates are in good agreement, with values ranging between 167±24 to 120±12 ka (OSL) and 179±18 to 131±18 ka (pIRIR measured at 290 °C) after a fading correction for the pIRIR signal. The results can be clearly correlated to around the end of oxygen isotope stage (OIS) 6 and the beginning of OSI 5, indicating that the aeolian accumulation of sands was a result of the Penultimate Glacial and climate fluctuations at the beginning of the Last Interglacial. Variations in magnetic susceptibility (MS) data can be interpreted alongside these dating results; several stronger peaks detected at the very end of the Penultimate Glacial and the initial stage of the Last Interglacial cycle most probably indicates more intensive pedogenesis resulting from a more favourable climate, probably because of climate changes. Breccias related to major bounding surfaces in association with evidence of soil formation and bioturbation could be the result of more favourable climate conditions and changes during the transition from OIS 6 to OIS 5 (Penultimate Glacial–Last Interglacial). These results are in agreement with similar data from the wider Mediterranean area.     

New Insights into the Evolution of an Intervalley Prehistoric Irrigation Canal System,North Coastal Peru

We present the results of combined AMS‐¹⁴C and single‐grain luminescence dating of pre‐Columbian irrigation canals that are part of the Racarumi Intervalley Canal System (RICS) in northern Peru. Archaeological and archival evidence suggest that the RICS was constructed during Middle Sicán (A.D. 900–1100) rule and continued to operate during Chimú and Inka conquests in the A.D. 1300s and 1400s, respectively, until finally succumbing to Spanish control of the area in the early A.D. 1500s. Detrital charcoal (AMS‐¹⁴C) and sand grains (OSL and IRSL) were collected from active, post‐abandonment, and clean out deposits in six earthen canals located within three separate alignments of the RICS. Resulting ages confirm operation during Middle Sicán, Late Sicán, Chimú, and Inka control, and possibly into the early part of the Spanish period. Placed within their hydroclimatological context, RICS canal deposits document recurrent El Niño flooding ∼A.D. 1300–1600 but indicate that damage to the system was repaired and the canals continued to operate despite periodic disruptions. This study demonstrates that single‐grain luminescence analysis conducted within a framework of geomorphology and formation processes has significant potential for detailed and accurate dating of ancient water‐control systems.     

Luminescence dating of Middle Pleistocene proglacial deposits from northern Switzerland: methodological aspects and stratigraphical conclusions

Optically stimulated luminescence (OSL) dating was applied to proglacial deposits from the Klettgau Valley in northern Switzerland, which is understood to record several phases of glaciation prior to the Last Interglacial. The aim was to provide an independent chronology for the different sedimentary units to understand better the complex depositional history of the region. This time range requires care when assessing the reliability of the luminescence protocols applied. Equivalent doses for fine‐ and coarse‐grain quartz remained below 300 Gy, while dose response curves for both fractions continued to display growth above 500 Gy. Dose recovery tests confirmed the ability of the single aliquot regenerative (SAR) protocol to recover laboratory doses of a similar size to burial doses, and isothermal decay measurements confirmed the stability of the quartz signal. Having passed rigorous testing criteria, quartz OSL ages of up to ～200 ka were considered reliable but significantly underestimated expected ages and prompt a reconsideration of earlier interpretations of the stratigraphy for this site. Rather than representing three separate glaciations, quartz luminescence ages instead suggest that these deposits record up to four independent ice advances during Marine Isotope Stage 6. For both single grain and single aliquot feldspar dating, it was not possible to separate the conflicting influences of anomalous fading and partial bleaching. However, uncorrected feldspar central age model ages were found to be in reasonable agreement with quartz age estimates, and suggest that feldspar ages may still offer useful additional information in this region.     

Thermoluminescence dating of St. Croix ceramics: Chronology building in Southwestern Nova Scotia

Using the classic thermoluminescence (TL) dating technique for fired ceramic materials, we have obtained the first direct ages for five ceramic artifacts recovered from BfDa-1, a prehistoric archaeological site located in St. Croix, southcentral Nova Scotia. BfDa-1 is the only archaeological site in Nova Scotia to produce the full range of ceramic styles associated with the Woodland or Ceramic Period (c. 1050 B.C. to A.D. 1500); thus our new chronology can be used to revise the current local and regional ceramic chronologies. The five sherds from the St. Croix site yielded absolute gas of 1.15 ± 0.15 ka to 2.62 ± 0.29 ka (1 ka = 1000 years). The oldest of these TL ages was obtained on a sherd decorated with a pseudoscallop shell design and is in excellent agreement with a ¹⁴C date of 2500 ± 120 B.P. associated with Early Ceramic artifacts at this site. The other TL ages are in agreement with the relative ceramic chronology deduced from their decorative attributes. All five TL dates are in the correct depth-age order. This demonstrates that the recent excavations explored a part of the site which remained undisturbed in spite of extensive agricultural and horticultural activities in the vicinity in recent centuries. The dates also indicate a high degree of compression for the cultural remains at the site. They suggest a sediment deposition rate of 1.3 cm/100 yr during the early stages of the occupation period (2000–2600 yr B.P.), and a decrease in the deposition rate to 0.5 cm/100 yr during the last 2000 years. These dates provide the first successful application of TL dating to ceramics of the Minas Basin area. They confirm an initial hypothesis based on the stylistic attributes of ceramics recovered from BfDa-1, that human occupation at the site must have been of long duration. The excellent quality of the analytical data indicates that the TL dating technique should be well suited to the study of ceramic technology in other parts of the province, and that local mineralogy is suitable for optical dating of sediments at the site and elsewhere in Nova Scotia. © 1997 John Wiley & Sons, Inc.     

Luminescence dating of lacustrine sediments from Tangra Yumco (southern Tibetan Plateau) using post‐IR IRSL signals from polymineral grains

Radiocarbon dating of bulk organic matter is the most commonly used method for establishing chronologies of lake sediments for palaeoclimate reconstructions on the Tibetan Plateau. However, this method is likely to be problematic because the dated material often suffers from old carbon contamination. Recently, advances in luminescence‐based chronological techniques have provided new options for dating lacustrine sediments. In the current study, we tested for the first time the applicability of a new post‐IR IRSL (pIRIR) measurement protocol for dating fine‐grained polymineral material from a deep‐lake sediment core from the central part of Tangra Yumco, on the southern Tibetan Plateau. Our results show that: (i) radioactive disequilibria in the uranium decay chain were observed in the studied lake sediments, and thus taken into account for dose rate calculation by using a dynamic modelling approach; (ii) the suitability and robustness of the pIRIR protocol measured at 150°C (pIRIR₁₅₀) for our samples are confirmed by a set of luminescence characteristic tests as well as the agreement with an independent age control; (iii) turbidite deposition partly caused an insufficient resetting of luminescence signals and thus apparent overestimation in luminescence dating; (iv) compared with the luminescence‐based age‐depth model, the ¹⁴C ages of bulk organic matter from the studied core generally yielded an age difference of ～2 ka, which is attributed to hardwater reservoir effects in Tangra Yumco. This study highlights the need for multi‐dating approaches of lake sedimentary archives on the Tibetan Plateau.     

北美五大湖区晚更新世劳伦泰德冰盖演化年代学综述及石英光释光测年的初步尝试

北美五大湖区的安大略湖北岸Don Valley Brickyard、Scarborough Bluffs、Bowmanville Bluffs剖面共同构成了北美东北部最长也是最厚的陆地第四纪沉积记录, 较完整地记录了晚更新世劳伦泰德冰盖(the Laurentide Ice Sheet)的演化. 晚更新世劳伦泰德冰盖演化的重建有赖于这些经典剖面中重要沉积地层单元的准确年代学控制. 传统的地层年代学主要是依靠少量¹⁴C年代, 将主要的混杂堆积单元(diamicton)解释为气候变冷环境下的冰川扩张, 并与指示全球冰量变化的深海氧同位素曲线一一比对建立起来的. 这样建立起来的年代学存在很大的不确定性. 20世纪80-90年代的少量热释光年代也不相吻合, 最近的13个长石红外释光定年则只集中于Bowmanville Bluffs的一个分层, 并未建立整个剖面的地层年代学, 使这些经典沉积剖面的年代学一直没有得到系统的建立. 应用石英光释光SAR-SGC法测试了Bowmanville Bluffs剖面Glaciofluvial Sand单元的2个冰水沉积样品, 年代结果分别为(41.6±3.8) ka、(48.1±4.4) ka, 分析表明这一年代结果偏老, 石英颗粒可能晒褪不完全. 由于大测片无法识别晒褪不完全的颗粒, 因此, 测试更多的剖面序列的光释光年代并尝试采用粗颗粒小测片或单颗粒技术解决样品颗粒晒褪不完全的问题将是必要的.     

Geoarchaeology of stratified paleoindian deposits at the Big Eddy site,Southwest Missouri,U.S.A.

The Big Eddy site (23CE426) in the Sac River valley of southwest Missouri is a rare recorded example of distinctly stratified Early through Late Paleoindian cultural deposits. Early point types recovered from the site include Gainey, Sedgwick, Dalton (fluted and unfluted), San Patrice, Wilson, and Packard. The Paleoindian record at Big Eddy represents only a fraction of the site's prehistoric cultural record; stratified cultural deposits in alluvium above the Paleoindian components span the entire known prehistoric sequence, and terminal Pleistocene alluvium may contain pre‐Early Paleoindian cultural deposits. This study focused on the paleogeomorphic setting, stratigraphy, depositional environments, pedology, geochronology, and history of landscape evolution of the late Pleistocene and early Holocene alluvium at the site. The Paleoindian sequence is associated with a complex buried soil 2.85 m below the modern surface (T1a) of the first terrace of the Sac River valley in the site vicinity. This soil formed at the top of the early submember of the Rodgers Shelter Member (underlying the T1c paleogeomorphic surface) and contains at least 70 cm of stratified Paleoindian cultural deposits, all in floodplain and upper point‐bar facies. A suite of 36 radiocarbon ages indicates that the alluvium hosting the Paleoindian sequence aggraded between ca. 13,250 and 11,870 cal yr B.P. (11,380 and 10,180 14C yr B.P.). Underlying deposits accumulated between ca. 15,300 and 13,250 cal yr B.P. (12,950 and 11,380 14C yr B.P.). By ca. 11,250 cal yr B.P. (9,840 14C yr B.P.) the T1c paleogeomorphic surface was buried by the earliest increment of a thick sequence of overbank sheetflood facies, ultimately resulting in deep burial and preservation of the Paleoindian record. The landform‐sediment assemblage that hosts the Paleoindian and possibly earlier cultural deposits at Big Eddy is both widespread and well preserved in the lower Sac River valley. Moreover, the terminal Pleistocene and early Holocene depositional environments were favorable for the preservation of the archaeological record. © 2007 Wiley Periodicals, Inc.