岩矿测试

中文核心期刊

中国科技核心期刊

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文章摘要
陈岳,罗武干,穆青,赵学峰,王昌燧.河北临漳曹村窑址青釉器物工艺特征研究[J].岩矿测试,2013,32(1):64-69
CHEN Yue,LUO Wu-gan,MU Qing,ZHAO Xue-feng,WANG Chang-sui.Study on Firing Technique of Celadon Wares Excavated from Caocun Kiln in Linzhang, Hebei Province[J].Rock and Mineral Analysis,2013,32(1):64-69.DOI:
河北临漳曹村窑址青釉器物工艺特征研究
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Study on Firing Technique of Celadon Wares Excavated from Caocun Kiln in Linzhang, Hebei Province
投稿时间:2012-01-17  修订日期:2012-04-12
DOI:
中文关键词: 北朝青瓷  铅釉  X射线荧光光谱法  X射线衍射法  物性测试  二次烧成工艺
英文关键词: Celadon of Northern Dynasty  lead-glaze  X-ray Fluorescence Spectrometry  X-ray Diffraction  physical testing  secondary sintering process
基金项目:中国科学院知识创新工程重要方向项目(KZCX2-EW-QN607); 博士后科学基金项目(20090460567)
作者单位
陈岳 中国科学院研究生院, 北京 100049 
罗武干 中国科学院研究生院, 北京 100049 
穆青 河北省文物出境鉴定中心, 河北 石家庄 050011 
赵学峰 磁县文物保管所, 河北 磁县 056500 
王昌燧 中国科学院研究生院, 北京 100049 
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中文摘要:
      河北地区古代瓷窑产品的理化测试工作多集中于隋唐、宋金时期的器物,北朝等早期产品的分析数据则少有报道。本文运用X射线荧光光谱、X射线衍射、岩相、吸水率测试和烧成温度测定等分析方法,对曹村窑址出土青釉样品的工艺特征开展研究。结果表明,2件样品釉层氧化钙含量分别为17.86%和14.1%,烧成温度分别达到1150.1℃和1185.2℃,证明这2件样品属于青瓷,从而证实了曹村窑是已发现的我国北方早期烧制青瓷的窑口之一;其余样品釉层氧化铅含量大于42%,部分样品吸水率低于5%,X射线衍射结果显示胎体中出现莫来石相,证明曹村窑可以生产出瓷胎铅釉陶。结合样品烧成温度均在1000℃以上,远高于铅釉成熟温度,推断曹村窑的瓷胎铅釉陶在北朝时期已经使用了二次烧成工艺。这一复杂工艺的产生,有可能为唐三彩的出现作了技术铺垫。
英文摘要:
      Current research on ancient porcelain in Hebei province is focused mainly on samples of Sui, Tang, Song and Jin Dynasty, while porcelain of the Northern Dynasties attracts little attention. This paper reports a method using X-ray Fluorescence Spectrometry (XRF) analysis, X-ray Diffraction (XRD), lithofacies analysis, water absorption test and dilatometer were to study the celadon wares excavated from the Caocun Kiln. In two samples, the contents of CaO were found to be 17.86% and 14.1%, with sintering temperatures of 1150.1℃ and 1185.2℃. In the remaining samples, the contents of PbO were no less than 42%, the water absorptions of partial samples were less than 5%, and mullite was found in the X-ray diffraction pattern. In conclusion, both celadon porcelain and lead-glaze pottery were found in the excavated artifact, which provides evidence to support the hypothesis that the Caocun kiln was one of the earliest kilns, manufacturing celadon porcelain in the north of China. The lead-glaze potteries were secondary sintered based on the sintering temperature of more than 1000℃, which was much higher than that for lead-glaze pottery. This new production technique may pave the way for tricolored glazed pottery at the Tang Dynasty. Conducting experiments such as these is helpful in the understanding of the development process of porcelains in North China.
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